Analytical chemistry Books

Book SynopsisProceedings of the NATO Advanced Research Workshop on Syntheses, Optical Properties and Applications of Near-Infrared (NIR) Dyes in High Technology Fields, Trest, Czech Republic, September 24-27, 1997Table of ContentsPreface. Advances in Methodology. Recent Developments in Fluorescence Spectroscopy: Three-Photon Excitation, Two-Color Two-Photon Excitation, Light Quenching and Development of Long-Lifetime Probes for Biophysics and Clinical Chemistry; J.R. Lakowicz, et al. Near-Infrared Fluorescence Instrumentation for DNA Analysis; L. Middendorf, et al. Highlights in Biochemistry and Biophysics. Ultrasensitive Detection and Identification of Biomolecules with Diode Lasers - from DYES to DNA; M. Sauer, et al. Incorporation of Dye in Resting and Stimulated Leukocytes; D. Frackowiak, et al. Application of Red Fluorescent Probes for the Measurement of Individual Cell Cytoplasmic pH Values; J. Slavik. Molecular Probes Based on Cyanine Dyes for Nucleic Acid Research; T.G. Deligeorgiev. New NIR Dyes: Synthesis, Spectral Properties and Applications in DNA Analyses; N. Narayanan, et al. Frontiers in Analytical Chemistry and Sensor Technology. Luminescent Probes for NIR Sensing Applications; E. Terpetschnig, O.S. Wolfbeis. NIR Fluorophores in Practical Analytical Chemistry; A.R. Swamy, et al. Long Wavelength Emitting Fluorescence Probes for Metal Ions; K. Rurack, et al. Advances in High Technology Applications. NIR Dyes for Information Recording, from Origin to Update; M. Matsuoka. Tuning of Color by Different Alignment of Dye Molecules; L. Dähne, E. Biller. Spectral Sensitization of Silver Halides in NIR Region; B.I. Shapiro. Optical Properties and Applications of Near Infrared Dyes in Polymeric Media; O.V. Przhonska. Insolubilisation and Fluorescence, Induced by Laser Diode Irradiation of IR-Dyes Embedded in Polymer Films. Thermally Induced Latex Coalescence and Acid Generation; C.D. Catry, et al. NIRPhotosensitizers in Photodynamic Therapy; E.A. Lukyanets. New Chromophores. Molecular Engineering of NIR Dyes; S. Daehne, M.L. Dekhtyar. New NIR Dyes Based on the Cyclopentadienylium Chromophore and Related Compounds; R. Gompper, et al. New Cyanine Dyes Absorbing in the NIR Region; A.I. Tolmachev, et al. Near-Infrared Cyanine Dyes: A New Approach to an Old Problem; Yu.L. Bricks, N.N. Romanov. Adventures in Search of New Dyes Absorbing in the Red or Near Infrared Region; H. Hartmann. Subject Index.

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Book SynopsisCalorimetry in Food Processing: Analysis and Design of Food Systems highlights various applications of calorimetry including characterization of moisture sorption, starch gelatinization and recrystallization, lipid polymorphism, protein gelation kinetics, and inactivation of microorganisms in a variety of food and biological materials.Table of ContentsPreface xiii Contributor List xvii Part 1 Analysis of Food and Biological Materials by Calorimetry 3 Chapter 1 Calorimetric Methods as Applied to Food: An Overview 5Gönül Kaletunç Chapter 2 Methods and Applications of Microcalorimetry in Food 15Pierre Le Parlouër and Luc Benoist Chapter 3 High-Pressure Differential Scanning Calorimetry 51Günther W.H. Höhne and Gönül Kaletunç Chapter 4 Calorimetry of Proteins in Dilute Solution 67G. Eric Plum Chapter 5 Thermal Analysis of Denaturation and Aggregation of Proteins and Protein Interactions in a Real Food System 87Valerij Y. Grinberg, Tatiana V. Burova, and Vladimir B. Tolstoguzov Chapter 6 Heat-Induced Phase Transformations of Protein Solutions and Fat Droplets in Oil-in-Water Emulsions: A Thermodynamic and Kinetic Study 119Perla Relkin Chapter 7 Analysis of Foodborne Bacteria by Differential Scanning Calorimetry 147Michael H. Tunick, John S. Novak, Darrell O. Bayles, Jaesung Lee, and Gönül Kaletunç Chapter 8 Coupling of Differential Scanning Calorimetry and X-Ray Diffraction to Study the Crystallization Properties and Polymorphism of Triacyglycerols 169Christelle Lopez, Daniel J.E. Kalnin, and Michel R. Ollivon Part 2 Calorimetry as a Tool for Process Design 199 Chapter 9 Overview of Calorimetry as a Tool for Efficient and Safe Food-Processing Design 201Alois Raemy, Corinne Appolonia Nouzille, Pierre Lambelet, and Alejandro Marabi Chapter 10 Shelf Life Prediction of Complex Food Systems by Quantitative Interpretation of Isothermal Calorimetric Data 237Simon Gaisford, Michael A.A. O’Neill, and Anthony E. Beezer Chapter 11 Use of Thermal Analysis to Design and Monitor Cereal Processing 265Alberto Schiraldi, Dimitrios Fessas, and Marco Signorelli Chapter 12 Importance of Calorimetry in Understanding Food Dehydration and Stability 289Yrjö H. Roos Chapter 13 High-Pressure Calorimetry and Transitiometry 311Stanislaw L. Randzio and Alain Le Bail Chapter 14 Calorimetric Analysis of Starch Gelatinization by High-Pressure Processing 341Kelley Lowe and Gönül Kaletunç Chapter 15 Use of Calorimetry to Evaluate Safety of Processing 351Hans Fierz Index 369

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Book SynopsisProvides comprehensive coverage of the structures, properties, and interactions of organo-clay complexes as well as their role in the origin of life. Presents current techniques in nuclear magnetic resonance, differential thermal analysis and thermogravimetry, visible spectroscopy, and infrared and thermal-infrared spectroscopy for the analysis of fine structures in organo-clay complexes.Table of ContentsStructure and surface acidity of clay minerals; introduction to organo-clay complexes and interactions; interactions of vermiculites with organic compounds; organophilicity and hydrophobicity of organo-clays; adsorption of organic cations on clays - experimental results and modelling; nuclear magnetic resonance spectroscopy; thermal analysis of organo-clay complexes; IR-spectroscopy and thermo-IR-spectroscopy in the study of the fine structure of organo-clay complexes; staining of clay minerals and visible-absorption spectroscopy of dye-dye complexes; clay catalysis in reactions of organic matter; organo-materials and organo-clay interactions and the origin of life on Earth.

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Book SynopsisElectrokinetic Phenomena emphasizes the impact of methods such as capillary zone electrophoresis, capillary electrochromatography, and capillary gel electrophoresis on the analysis of biomolecules. This reference reveals the electrokinetic phenomena that underlie high-performance electro-based analytical tools and vividly depicts how electrodriven analytical tools revolutionize and expedite chemical, pharmaceutical, and biotechnological analysis. An authoritative overview, the book provides effective pathways for large-scale biomedical applications and describes how microfabricated and automated devices enhance and accelerate the analysis of biologically important molecules.Table of Contents Migration of sample components in capillary analytical techniques - chromatography, electrophoresis, and electrochromatography, Anurag S. Rathore; methods development for capillary electrophoresis with emphasis on small molecules, Robert Weinberger; capillary isoelectric focusing, Ferenc Kilar; capillary gel electrophoresis and related microseparation techniques Andras Guttman; affinity capillary electrophoresis, Vadim M. Okun and Ernst Kenndler; electroosmotic mobility and conductivity in microchannels, Emily Wen, Anurag S. Rathore and Csaba Horvath; factors influencing performance in capillary electrochromatography on silica columns, Keith D. Bartle and Peter Myers; effects of pore flow on separation efficiency in capillary electrochromatography with porous particles, Remco Stol and Wim Th. Kok; ultrashort-column capillary electrochromatography, Takao Tsuda; microstructure and in-silico developments for high-sensitivity proteomics research, Thomas Laurell, Johan Nilsson and Gyorgy Marko-Varga; micro chemical processing on microchips, Yoshikuni Kikutani and Takehiko Kitamori; micropreparative applications and on-line sample treatment, Julia Khandurina; NMR detection in capillary electrophoresis and capillary electrochromatography, Dimuthu A. Jayawickrama, Andrew M. Wolters and Jonathan V. Sweedler; applications of capillary electrochromatography, V.T. Remcho, Gabriela S. Chirica, Stacey L. Clark and Angela Doneau; clinical applications of microfluidic devices, Joan M. Bienvenue, James Karlinsey, James P. Landers and Jerome P. Ferrance.

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Book SynopsisThis work introduces scientists of all disciplines to the chromatographic process and how it functions. The basic principles of chromatographic separation and specific chromatographic procedures, including gas, liquid and thin-layer chromatography, are covered. For each separation method the book details its characteristics, the instrumentation required, the procedures necessary for effective use, areas of application and examples of its use.;This work is intended for analytical chemists, laboratory technicians, and upper-level undergraduate and graduate students in analytical chemistry or separation science courses.Trade Review"Excellent discussions and practical advice are provided for the selection of stationary and mobile phases, as well as the exact type of chromatography needed to accomplish a separation. "---Analytical Chemistry News & Features ". . .a very readable and. . .informative book which is highly recommended for any scientist who needs to use separation techniques as part of their work but is not a separations expert. "---Bioseparation ". . .a[n]. . .instructive presentation of basic intermolecular forces and processes playing a substantial role in understanding the selectivity and resolution of separations, and a nice broad set of practical examples of applications. "---Journal of Chromatography ATable of ContentsThe chromatographic separation; the mechanism of retention; peak dispersion; qualitative analysis; quantitative analysis. Part 1 Gas chromatography: the gas chromatograph; gas chromatography detectors; gas chromatography columns; gas chromatography applications; the liquid chromatograph; liquid chromatography detectors; liquid chromatography columns; liquid chromatography applications. Part 2 Thin layer chromatography: TLC apparatus; thin-layer chromatography techniques.

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Book SynopsisDiscusses the latest techniques for integrating NMR spectroscopy in undergraduate courses.

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Book SynopsisThe book is intended for chemists entering medicinal chemistry research who have no knowledge of pharmacology. Pharmacological principles and concepts are emphasized, rather than a survey of large numbers of specific drugs. It is intended to serve as a tool to prepare the reader for further in-depth study in many areas of pharmacology.

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Book SynopsisSince the publication of the benchmark first edition of this book, chemical library and combinatorial chemistry methods have developed into mature technologies. There have also been significant shifts in emphasis in combinatorial synthesis. Reflecting the growth in the field and the heightened focus on select areas, Analytical Methods in Combinatorial Chemistry, Second Edition updates a classic text and captures the current state of these technologies.Written by leaders in the field, this second edition includes several enhancements. A chapter on high-throughput analytical methods and informatics reflects the demand for quality control of library members. A new chapter focuses on high-throughput purification methods. All chapters have been updated with new data.Topics discussed in this second edition include: Properties of solid-phase samples, analytical studies targeted to understand these properties, and resin swelling FTable of ContentsAnalytical issues in combinatorial chemistry. An examination of the analytical sample resin support. Solid-phase reaction optimization using FTIR. Reaction optimization using MS and NMR methods. Reaction optimization using spectrophotometric and other methods. Quality control of combinatorial libraries. High-throughput purification. Final Thoughts and Future Perspectives.

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Book SynopsisHandbook of Chromatography: Analysis of Lipids provides a valuable review of state-of-the-art applications of chromatographic techniques (TLC, GC, HPLC) and other analytical techniques. Much of this volume is devoted to applications of HPLC (including supercritical fluid chromatography) in the analysis of lipids such as fatty acids, oxygenated fatty acids, enantiomeric acyl- and alkylglycerols, and lipoproteins. The handbook also provides extensive coverage of applications of combinations of various chromatographic techniques used in the analysis of ozonides, anacardic acids, glycerophospholipids, products of lipolysis, artifacts and contaminants in edible fats, acylated proteins, non-caloric lipids, lipophilic vitamins, acyl-Coenzyme A thioesters, dolichols, mycolic acids, technical fats and fat products, and liposomes. Handbook of Chromatography: Analysis of Lipids will be a useful reference for oil chemists, biochemists, fat science technologists, and other scieTable of Contents: Obtaining and Handling Biological Materials and Prefractionating Extracts for Lipid Analysis. Analysis of Lipids by Planar Chromatography. Imaging Plate System for Radio Luminographic Detection of Lipids on Thin-Layer Plates. High Performance Liquid Chromatography as a Tool for the Lipid Chemist and Biochemist. High Performance Liquid Chromatography of Fatty Acids. Analysis of Lipids by On-Line Coupled Liquid Chromatography-Gas Chromatography. Supercritical Fluid Chromatographic Analysis of Lipids. High Performance Liquid Chromatography of Oxygenated Fatty Acids Including Enantiomer Separation. High Performance Liquid Chromatography of Lipoproteins. High Performance Liquid Chromatography of Acylglycerols and Alkylglycerols. Gas Chromatography of Triacylglycerols and Other Lipids in Packed Columns. Gas Chromatography of Fatty Acids and Acylglycerols in Capillary Columns. Radio-Gas Chromatography of Lipids. Ozonides and Ozonolysis of Lipids. Anacardic Acids. Glycerophospholipids. Artifacts, Contaminants and Autoxidation Products of Edible Fats and Oils. Acylated Proteins: Identification of the Attached Fatty Acids and Their Linkages. Non-Caloric Lipids. Lipophilic Vitamins. Acyl-CoA Thioesters. Dolichols and Dolichyl Derivatives. Mycolic Acids. Technical Fats and Oils and Products Derived Therefrom. Analysis of Natural Fats and Oils by Ammonia Negative Ion Tandem Mass Spectrometry. Characterization of Liposomes. Phospholipids from Pulmonary Surfactant and Amniotic Fluid. Large-Scale Chromatography of Lipids. Products of Lipolysis. Index. FEATURES:

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Book SynopsisThe knowledge of metal ion speciation is essential for predicting the exact toxicities of metal ion species in the environment. Metal ions can exist in various oxidation states, each of which possesses different physical and chemical properties as well as exhibit varying toxicities. Often, toxicity data is unreliable because it is based on metal ion concentration measurements that fail to identify a dominant species either more or less harmful than the average. Instrumental Methods in Metal Ion Speciation provides analytical techniques and experimental methodologies for determining the concentration of the different physicochemical forms of metal ions in environmental and biological samples, leading to more accurate measurements of actual toxicity.The authors introduce the principles of metal ion speciation and discuss important analytical techniques such as gas and liquid chromatography, capillary electrophoresis, and both electrochemical and radiochemical methods used to determine concentration and composition. They present a range of liquid chromatographic approaches, including capillary electrochromatography and high-performance, ion, ion pair, micellar electrokinetic, size exclusion, chiral, and supercritical fluid chromatographies for all metal ion species. Comprehensive in scope, the text covers the sources, distribution, toxicity, biotransformation, and biodegradation of each metal ions species as well as extraction methods, sample preparation, and experimental optimization techniques that can be useful in designing future experiments. Instrumental Methods in Metal Ion Speciation is a unique and valuable source of reference for scientists, academics, and researchers involved in analytical, biological, pharmaceutical, and environmental chemistries, as well as material industries, geochemistry, agriculture, biotechnology, and occupational safety and regulations.Trade Review“The book has been presented by well known scientists … presents very interesting material … The book as a whole will certainly be a useful source of information for numerous analytical chemists which are obliged to work in the timely important field of chemical analysis.” — Adam Hulanicki, in Chem. Anal, Vol. 52, No. 157, 2007Table of ContentsIntroduction. Metal Ion Species: Sources and Distribution. Metal Ion Species: Toxicities, Biotransformation, and Biodegradation. Sample Preparation. Speciation of Metal Ions by Gas Chromatography. Speciation of Metal Ions by Reversed Phase High Performance Liquid Chromatography. Speciation of Metal Ions by Ion Chromatography. Speciation of Metal Ions by Ion Pair, Micellar Electrokinetic, Size Exclusion, Chiral, Capillary Electro- and Supercritical Fluid Chromatographic Methods. Speciation of Metal Ions by Capillary Electrophoresis. Speciation of Metal Ions by Spectroscopic Methods. Speciation of Metal Ions by Electrochemical and Radiochemical Methods. Perspectives and Legislation of Metal Ion Speciation.

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Book SynopsisPreparative Layer Chromatography explains how this method is used for separating large quantities of mixtures containing a wide variety of important compounds. It offers a broad review of preparative layer chromatography (PLC) applications and adaptable working procedures for microseparations involving organic, inorganic, and organometallic compounds. The book contains theoretical background, chemical principles, and relevance of preparative layer chromatography (PLC) to a wide range of applications, particularly in the study of pharmaceuticals and biochemistry. Written by many of the best known and most knowledgeable specialists in the field, the chapters describe all the necessary techniques, current procedures, and superior strategies for selecting the most suitable eluents and designing application-specific PLC systems based on the data being sought. They provide comprehensive instructions, surrounding issues, and suggestions for optimizing optional working techniques withiTrade Review"...A valuable and important supplement to the existing vast chromatographic literature, [this book] demonstrates the potential of planar chromatography for separation and isolation of pure compounds, even from very complex mixtures."-Journal of Liquid Chromatography, August 2006"The contributor[s']...experience integrated in the monograph forms a good basis for the readers."-Instrumentation Science & Technology, August 2006"The [first] eight chapters provide sound theoretical and methodological foundations of PLC. Numerous applications of PLC are reviewed in the second section, based on extensive literature. ...The application reviews provide numerous examples of solving experimental difficulties for the separation of complex mixtures."-Preparative Biochemistry & Biotechnology, August 2006"The book is quite well produced and has a large number of illustrations . . . this volume is a worthy addition to the PLC literature, and a good place to start for the novice." – I.D. Wilson, in Chromatographia, January 2008, Vol. 67, No. 1/2Table of ContentsIntroduction. Adsorption Planar Chromatography in the Non-linear Range: Selected Drawbacks and Selected Guidelines. Sorbents and Precoated Layers in PLC. Selection and Optimization of the Mobile Phase for PLC. Sample Application and Development of Layers. On Methodical Possibilities of the Horizontal Chambers in PLC. Location of Separated Zones by Use of Visualization Reagents, UV Absorbance on Layers Containing a Fluorescent Indicator, and Densitometry. Additional Detection Methods for Separated Zones and Recovery of Substances from the Layer. Medical Applications of PLC. PLC of Hydrophobic Vitamins. PLC of Natural Mixtures. Application of PLC to Lipids. The Use of PLC for Separation of Natural Pigments. Application of PLC to Inorganics and Organometallics. PLC in a Clean-up and Group Fractionaction of Geochemical Samples: A Review of the Commonly Applied Techniques. The Use of PLC for Isolation and Identification of Unknown Compounds from the Frankincense Resin: Strategies for Finding Marker Substances.

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Book SynopsisPulse Radiolysis presents an in-depth discussion of the pulse radiolysis technique, one of the most important and powerful means for detecting transient and relaxation phenomena and following their behavior in irradiated systems. The book covers the principle of pulse radiolysis, identifies various kinds of pulse radiolysis techniques, and discusses recent advancements in the field. The text also discusses new experimental pulse radiolysis techniques (basic and applied) in broad scientific fields such as physics, chemistry, biology, and engineering. These techniques include picosecond pulse radiolysis, single particle radiolysis, and muon-induced transient phenomena. Pulse Radiolysis provides essential information for all professionals involved with pulse radiolysis research.Table of ContentsIntroduction-Pulse Radiolysis. Twin Linac Pulse Radiolysis System. Time-Resolved Single-Photon Counting Technique in Radiolysis of Hydrocarbons. Time-Resolved Magnetic Resonance Study. Time-Resolved Atmospheric Pressure Mass-Spectroscopy. Time-Resolved Conductivity Techniques, DC to Microwave. Time-Resolved Light-Scattering Study. Picosecond Ultraviolet Multiphoton Laser Photolysis Related to Radiolysis. Pulse Radiolysis in the Gas Phase. Studies of Gamma-, Alpha-, Positron- and Muon-Induced Spurs by Single-Particle Pulse Radiolysis Technique. Muon Spin Resonance Studies by Pulsed Muon Beam. Ion-Beam Pulse Radiolysis. Early Processes in Crystalline Alkali-Halides. Early Processes in Liquids. Geminate Ion Recombination in Non-Polar Liquid. Pulse Radiolysis in Glassy Solid. Pulse Radiolysis Studies of Aqueous Solutions. Pulse Radiolysis Study Related to Organic Synthesis. Pulse Radiolysis Macromolecules. Pulse Radiolysis Nucleic Acids in Aqueous Solution.

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Book SynopsisThe purpose of this volume is to emphasize the fact that biological trace element research is a multidisciplinary science which requires a prudent combination of biological insight and analytical awareness. The text frequently stresses that accurate measurements on biologically and analytically valid samples hold the key for success in future investigations. It reminds the analytical scientists and the life sciences researchers that their perceptions should extend beyond conventional limits - namely, the former as generators of data and the latter as interpreters of those findings. This book enables the reader to understand the intricacies of elemental composition studies in biological systems, and also provides a valuable source of information to biologists, biochemists, physicians, nutritionists and related scientific workers who intend to draw meaningful conclusions from the analytical findings.Table of ContentsVOLUME I: BIOLOGICAL, MEDICAL, ENVIRONMENTAL, COMPOSITIONAL, AND METHODOLOGICAL ASPECTS. Biological Trace Element Research. Chemical Elements in Biological Systems. Physiological and Anatomical Features of Biomedical Specimens. The Biological Basis for Selection of Specimens for Trace Element Research Studies. Problems in the Elemental Analysis of Biological Systems. Methods for Elemental Analysis of Biological Materials. Quality Assurance in Inorganic Bioanalytical Research. Presentation and Interpretation of Trace Element Data. Reference Values for Trace Elements in Human Tissues and Body Fluids. Biological and Dietary Reference Materials for Use in Bioinorganic Analytical Quality Control Programs. Index.

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Book SynopsisThe purpose of this book is to collect into one volume the research done on the mass spectrometry of peptides. It balances a range of topics including theory, instrumentation, analytical techniques, and biological applications. The scope of the work contains three major sections: ionization methods, instrumental developments, and analysis of peptides. It describes 252Cf plasma desorption and laser-induced multiphoton ionization methodology. This exciting resource covers many new areas, including continuous flow FAB, quantification of human neuropeptides, and peptide mapping. It also discusses Q-FTMS, cross-links, and metal ions.Table of ContentsINTRODUCTION. PREFACE. SECTION I: IONIZATION METHODS. 252Cf PLASMA DESORPTION METHODS. Fundamental Aspects of Protein Mass Spectrometry Using 252-Californium Plasma Desorption. Plasma Desorption Mass Spectrometry of Peptides and Peptide Conjugates. The Analysis of Synthetic Peptides and Proteins. Analysis of Peptides and Proteins by Plasma Desorption Mass Spectrometry. LASER-INDUCED MULTIPHOTON IONIZATION. Laser-Induced Multiphoton Ionization of Peptides in Supersonic Beam/Mass Spectrometry. SECTION II: INSTRUMENTAL DEVELOPMENTS. MAGNETIC SECTOR INSTRUMENTS. The Molecular Weight Determination of Large Peptides by Magnetic Sector Mass Spectrometry. Four-Sector Tandem Mass Spectrometry of Peptides. QUADRUPOLE FOURIER TRANSFORM. Peptide Sequence Analysis by Triple Quadrupole and Quadrupole Fourier Transform Mass Spectrometry. TIME-OF-FLIGHT INSTRUMENTS. Correlation Measurements in a Reflecting Time-of-Flight Mass Spectrometer. SECTION III: ANALYSIS OF PEPTIDES. SAMPLE PREPARATION. Sample Preparation and Matrix Selection for Analysis of Peptides by FAB and Liquid SIMS. LC-MS ANALYSIS. On-Line Methods for Peptide Analysis by Continuous-Flow FABMS. ANALYSIS OF PROTEIN PRODUCTS. Investigation of Amino Acid Mutation by High Resolution Mass Spectrometry. The Mass Spectral Analysis of Hemoglobin Variants. PROTEIN CROSS-LINKAGES. Detection and Location of Disulfide Bonds in Proteins by Mass Spectrometry. PEPTIDE INTERACTIONS WITH METAL IONS. Tandem Mass Spectrometry for Determining the Amino Acid Sequence of Cyclic Peptides and for Assessing Interactions of Peptides and Metal Ions. PERMETHYLATED PEPTIDES. Analysis of Permethylated Peptides by Mass Spectrometry. NEUROPEPTIDES. Applications of Mass Spectrometry for Characterization of Neuropeptides. Peptide-Charting Applied to Studies of Precursor Processing in Endocrine Tissues. QUANTIFICATION OF NEUROPEPTIDES. Mass Spectrometry of Biologically Important Neuropeptides

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