Description

Book Synopsis
Closely follows an actual structural determination. After some introductory material on the nature of x--rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x--ray data are covered, plus their reduction into a useable form.

Table of Contents
PRELIMINARY STAGES.

X-Rays.

Diffraction of X-Rays.

Crystals, Symmetry, and Space Groups.

Crystals and Their Properties.

Geometric Data Collection.

Intensity Data Collection.

Data Reduction.

Theory of Structure Factors and Fourier Syntheses.

Calculation of Structure Factors and Fourier Syntheses.

THE PHASE PROBLEM.

The Phase Problem.

Direct Methods.

Patterson Methods.

Heavy Atom Methods.

Search Methods.

Completing the Structure.

REFINEMENT AND RESULTS.

Refinement of Crystal Structures.

Random and Systematic Errors.

Derived Results.

Ambiguities and Uncertainties.

Appendices.

Index.

XRay Structure Determination A Practical Guide

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    A Hardback by George H. Stout, Lyle H. Jensen

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      Publisher: John Wiley & Sons Inc
      Publication Date: 21/06/1989
      ISBN13: 9780471607113, 978-0471607113
      ISBN10: 0471607118
      Also in:
      Chemistry

      Description

      Book Synopsis
      Closely follows an actual structural determination. After some introductory material on the nature of x--rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x--ray data are covered, plus their reduction into a useable form.

      Table of Contents
      PRELIMINARY STAGES.

      X-Rays.

      Diffraction of X-Rays.

      Crystals, Symmetry, and Space Groups.

      Crystals and Their Properties.

      Geometric Data Collection.

      Intensity Data Collection.

      Data Reduction.

      Theory of Structure Factors and Fourier Syntheses.

      Calculation of Structure Factors and Fourier Syntheses.

      THE PHASE PROBLEM.

      The Phase Problem.

      Direct Methods.

      Patterson Methods.

      Heavy Atom Methods.

      Search Methods.

      Completing the Structure.

      REFINEMENT AND RESULTS.

      Refinement of Crystal Structures.

      Random and Systematic Errors.

      Derived Results.

      Ambiguities and Uncertainties.

      Appendices.

      Index.

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