Description
Book SynopsisThe in-lab preparation of certain chemical reagents provides a number of advantages over purchasing various commercially prepared samples. This is especially true in isolated regions where acquiring the necessary substances from overseas can cause undue delay and inconvenience due to restrictions on the transportation of hazardous chemicals. An invaluable resource for chemists in a variety of environments, Small-Scale Synthesis of Laboratory Reagents with Reaction Modeling presents efficient, sensible, and versatile methods for the laboratory preparation of common chemical reagents.
Rapid, reliable synthesis
Designed to facilitate smooth experimentation in the lab, this volume presents preparations chosen for their short duration, availability of apparatus, high yield, and high purity of the product. Adding an educational component, the book also discusses fundamental processes in inorganic
Table of Contents
Safety in the Laboratory. Sodium. Potassium. Lithium. Cesium. Lithium Hydride and Sodium Hydride. Bromine. Aluminum Bromide. Lithium Aluminum Hydride. Triethylaluminum and Diethylaluminum Bromide. Hydrazine Sulfate and Alcoholic Hydrazine Hydrate. Sodium and Potassium Azide. Potassium t-Butoxide and Potassium Hydride. Carbon Disulfide. Chlorine. Carbon Tetrachloride. Bis-Trichloromethyl Carbonate (Triphosgene). Phosphorus Pentachloride. Phosphorus Oxychloride. Sulfur Trioxide and Oleum. Thionyl Chloride and Chlorosulfonic Acid. Appendix: Assay of Reagents.
