Description
Book SynopsisReflecting the increased pace of research and the many recent advances in organic chemistry, the Organic Syntheses series serves as a single source compendium of the most up-to-date procedures in use. Organic Syntheses consists of protocols for the synthesis of useful chemical compounds.
Table of ContentsPreparation of 1,4:5,8-Dimethano-1,2,3,4,5,6,7,8-Octahydro-9,10-Dimethaoxyanthracenium Hexachiloroantimonate(4
+Sbcl
6-): A Highly Robust Radical-Cation Salt.
Preparation of Optically Active (R,R)-Hydrobenzoin From Benxoin or Benzil.
2,2-Diethoxy-1-Isoxyanoethane.
Preparation of (S,S) -1,2--BIS(tert-Butylmethylphosphino)-Ethane ((S,S)-t-Bu-BISP) As a Rhodium Complex.
Preparation of Hexakis(4-Bromophenyl)Benzene (HBB).
An Efficient, Highly Diastereo- And Enantioselective Hetero-Diels-Alder Catalyst. Preparation of (2S, 6R)-6-(tert-Butyldimethylsilyloxymethyl)-2-Methoxy-2,5-Diyhdropyran.
Lipase-Catalyzed Resolution of 4-Trimethylsilyl-3-Butyn-2-OL and Conversion of the (R)-Enantiomer To (R)-3-Butyn-2-Yl Mesylate and ({)-1-tributylstannyl-1,2-Butadiene.
Iridium-Catalyzed Synthesis of Vinyl Ethers from Alcohols and Vinyl Acetate.
1-(tert-Butyliminomethyl)-1,3-Dimethylurea Hydrochloride.
Ortho-Formylation of Phenols: Preparation of 3-Bromosalicylaldehyde.
Preparation of 1-Methoxy-2-(4-Methoxyphenoxy)Benzene.
D-Ribonolactone and 2,3-Isopropylidene-(D-Ribonolactone)
Preparation of 4-Acetylamino-2,2,6,6-Tetramethyl-Piperidine-1-Oxoammonium Tetrafluoroborate, and the Oxidation of Geraniol to Geranial.
(2S)-(-)-3exo-(Morpholino)Isoborneol [(-)-MIB].
Conversion of Arylalkylketones Into Dichloroalkenes: 1-Chloro-4-(2,2-Dichloro-1-Methylvinyl)Benzene.
1,4,-Dioxene.
(R)-(+)-3,4-Dimethylcyclohex-2-EN-1-One.
A Practical and Safe Preparation of 3,5-BIS-(Trifluoromethyl)Acetophenone.
Asymmetric Alcoholysis of Meso-Anhydrides Mediated By Alkaloids.
Iridium-Catalyzed C-HBorylation of Arenes and Heteroarenes: 1-Chloro-3-Iodo-5-(4,4,5,5-Tetramethyl-1,3,2,-Dioxaborolan-2-YL)Benzene and 2-(4,4,5,5-Tetramethyl-1,3,2-Dioxaborolan-2-YL)Indole.
Asymmetric Rearrangement of Allylic Trichloroacetimidates: Preparation of (s)-2,2,2-Trichloro-N-(1-Propylallyl)Acetamide.
Preparation of (Triphenylphosphoranylidene)-Ketene From (Methoxycarbonylmethylene)-Triphenylphosphorane.
Preparation of [1-(Methoxymethylcarbamoyl)-Aethyl]Phosphonic Acid BIS(2,2,2-Trifluoroethyl)Ester: A Useful Intermediate in the Synthesis of Z-Unsaturated N-Methoxy-N-Methylamides.
(Rs)-(+)-2-Methyl-2-Propanesulfinamide.
Preparation of 1-Butyl-3-Methylimidazolium Tetrafluoroborate.
Catalytic Asymmetric Acyl Halide-Aldehyde Cyclocondensation reaction.
Alkyne via Solid-Liquid Phase-Transfer Catalyzed Dehydrohalogenation: Acetylene Dicarboxaldehyde Tetramethyl Acetal and Acetylene Dicarboxaldeyde Dimethyl Acetal.
Catalytic reduction of Amides to Amines with Hydrosilanes Using a Tributhenium Carbonyl Cluster as the Catalyst.
