Description
Book SynopsisThe content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the
Table of ContentsContributors ix
Series Preface xiii
Volume Preface xv
Part A: Basic Principles 1
1 Quadrupolar Interactions
Pascal P. Man 3
2 Quadrupolar Nuclei in Solids
Alexander J. Vega 17
3 Quadrupolar Coupling: An Introduction and Crystallographic Aspects
Sharon E. Ashbrook, Stephen Wimperis 45
4 Quadrupolar Nuclei in Solids: Influence of Different Interactions on Spectra
David L. Bryce, Roderick E. Wasylishen 63
Part B: Advanced Techniques 75
5 Acquisition of Wideline Solid-State NMR Spectra of Quadrupolar Nuclei
Robert W. Schurko 77
6 Sensitivity and Resolution Enhancement of Half-Integer Quadrupolar Nuclei in Solid-State NMR
Thomas T. Nakashima, Roderick E. Wasylishen 95
7 Quadrupolar Nutation Spectroscopy
Arno P.M. Kentgens 107
8 Dynamic Angle Spinning
Philip J. Grandinetti 121
9 Double Rotation (DOR) NMR
Ray Dupree 133
10 MQMAS NMR: Experimental Strategies
Jean-Paul Amoureux, Marek Pruski 143
11 STMAS NMR: Experimental Advances
Sharon E. Ashbrook, Stephen Wimperis 163
12 Correlation Experiments Involving Half-Integer Quadrupolar Nuclei
Michael Deschamps, Dominique Massiot 179
13 Computing Electric Field Gradient Tensors
Josef W. Zwanziger 199
Part C: Applications 211
14 Quadrupolar NMR to Investigate Dynamics in Solid Materials
Luke A. O’Dell, Christopher I. Ratcliffe 213
15 Alkali Metal NMR of Biological Molecules
Gang Wu 233
16 Nitrogen-14 NMR Studies of Biological Systems
Luminita Duma 255
17 Oxygen-17 NMR Studies of Organic and Biological Molecules
Gang Wu 273
18 Oxygen-17 NMR of Inorganic Materials
Sharon E. Ashbrook, Mark E. Smith 291
19 Chlorine, Bromine, and Iodine Solid-State NMR
David L. Bryce, Cory M. Widdifield, Rebecca P. Chapman, Robert J. Attrell 321
20 Quadrupolar NMR of Ionic Conductors, Batteries, and other Energy-Related Materials
Frédéric Blanc, Leigh Spencer, Gillian R. Goward 349
21 Quadrupolar NMR of Nanoporous Materials
Mohamed Haouas, Charlotte Martineau, Francis Taulelle 371
22 Quadrupolar NMR in the Earth Sciences
Jonathan F. Stebbins 387
23 Quadrupolar NMR of Superconductors
Nicholas J. Curro 401
24 Quadrupolar NMR of Semiconductors
James P. Yesinowski 417
25 Quadrupolar NMR of Metal Nuclides in Biological Materials
Tatyana Polenova, Andrew S. Lipton, Paul D. Ellis 439
26 Nuclear Waste Glasses: Insights from Solid-State NMR
Scott Kroeker 453
27 Quadrupolar Metal NMR of Oxide Materials Including Catalysts
Olga B. Lapina, Victor V. Terskikh 467
28 Quadrupolar NMR of Intermetallic Compounds
Frank Haarmann 495
Index 511