Description

Book Synopsis
The content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the

Table of Contents

Contributors ix

Series Preface xiii

Volume Preface xv

Part A: Basic Principles 1

1 Quadrupolar Interactions
Pascal P. Man 3

2 Quadrupolar Nuclei in Solids
Alexander J. Vega 17

3 Quadrupolar Coupling: An Introduction and Crystallographic Aspects
Sharon E. Ashbrook, Stephen Wimperis 45

4 Quadrupolar Nuclei in Solids: Influence of Different Interactions on Spectra
David L. Bryce, Roderick E. Wasylishen 63

Part B: Advanced Techniques 75

5 Acquisition of Wideline Solid-State NMR Spectra of Quadrupolar Nuclei
Robert W. Schurko 77

6 Sensitivity and Resolution Enhancement of Half-Integer Quadrupolar Nuclei in Solid-State NMR
Thomas T. Nakashima, Roderick E. Wasylishen 95

7 Quadrupolar Nutation Spectroscopy
Arno P.M. Kentgens 107

8 Dynamic Angle Spinning
Philip J. Grandinetti 121

9 Double Rotation (DOR) NMR
Ray Dupree 133

10 MQMAS NMR: Experimental Strategies
Jean-Paul Amoureux, Marek Pruski 143

11 STMAS NMR: Experimental Advances
Sharon E. Ashbrook, Stephen Wimperis 163

12 Correlation Experiments Involving Half-Integer Quadrupolar Nuclei
Michael Deschamps, Dominique Massiot 179

13 Computing Electric Field Gradient Tensors
Josef W. Zwanziger 199

Part C: Applications 211

14 Quadrupolar NMR to Investigate Dynamics in Solid Materials
Luke A. O’Dell, Christopher I. Ratcliffe 213

15 Alkali Metal NMR of Biological Molecules
Gang Wu 233

16 Nitrogen-14 NMR Studies of Biological Systems
Luminita Duma 255

17 Oxygen-17 NMR Studies of Organic and Biological Molecules
Gang Wu 273

18 Oxygen-17 NMR of Inorganic Materials
Sharon E. Ashbrook, Mark E. Smith 291

19 Chlorine, Bromine, and Iodine Solid-State NMR
David L. Bryce, Cory M. Widdifield, Rebecca P. Chapman, Robert J. Attrell 321

20 Quadrupolar NMR of Ionic Conductors, Batteries, and other Energy-Related Materials
Frédéric Blanc, Leigh Spencer, Gillian R. Goward 349

21 Quadrupolar NMR of Nanoporous Materials
Mohamed Haouas, Charlotte Martineau, Francis Taulelle 371

22 Quadrupolar NMR in the Earth Sciences
Jonathan F. Stebbins 387

23 Quadrupolar NMR of Superconductors
Nicholas J. Curro 401

24 Quadrupolar NMR of Semiconductors
James P. Yesinowski 417

25 Quadrupolar NMR of Metal Nuclides in Biological Materials
Tatyana Polenova, Andrew S. Lipton, Paul D. Ellis 439

26 Nuclear Waste Glasses: Insights from Solid-State NMR
Scott Kroeker 453

27 Quadrupolar Metal NMR of Oxide Materials Including Catalysts
Olga B. Lapina, Victor V. Terskikh 467

28 Quadrupolar NMR of Intermetallic Compounds
Frank Haarmann 495

Index 511

NMR of Quadrupolar Nuclei in Solid Materials 3

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    A Hardback by Roderick E. Wasylishen, Sharon E. Ashbrook, Stephen Wimperis

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      Publisher: John Wiley & Sons Inc
      Publication Date: Publication Date: 15/06/2012
      ISBN13: 9780470973981, 978-0470973981
      ISBN10: 0470973986

      Description

      Book Synopsis
      The content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the

      Table of Contents

      Contributors ix

      Series Preface xiii

      Volume Preface xv

      Part A: Basic Principles 1

      1 Quadrupolar Interactions
      Pascal P. Man 3

      2 Quadrupolar Nuclei in Solids
      Alexander J. Vega 17

      3 Quadrupolar Coupling: An Introduction and Crystallographic Aspects
      Sharon E. Ashbrook, Stephen Wimperis 45

      4 Quadrupolar Nuclei in Solids: Influence of Different Interactions on Spectra
      David L. Bryce, Roderick E. Wasylishen 63

      Part B: Advanced Techniques 75

      5 Acquisition of Wideline Solid-State NMR Spectra of Quadrupolar Nuclei
      Robert W. Schurko 77

      6 Sensitivity and Resolution Enhancement of Half-Integer Quadrupolar Nuclei in Solid-State NMR
      Thomas T. Nakashima, Roderick E. Wasylishen 95

      7 Quadrupolar Nutation Spectroscopy
      Arno P.M. Kentgens 107

      8 Dynamic Angle Spinning
      Philip J. Grandinetti 121

      9 Double Rotation (DOR) NMR
      Ray Dupree 133

      10 MQMAS NMR: Experimental Strategies
      Jean-Paul Amoureux, Marek Pruski 143

      11 STMAS NMR: Experimental Advances
      Sharon E. Ashbrook, Stephen Wimperis 163

      12 Correlation Experiments Involving Half-Integer Quadrupolar Nuclei
      Michael Deschamps, Dominique Massiot 179

      13 Computing Electric Field Gradient Tensors
      Josef W. Zwanziger 199

      Part C: Applications 211

      14 Quadrupolar NMR to Investigate Dynamics in Solid Materials
      Luke A. O’Dell, Christopher I. Ratcliffe 213

      15 Alkali Metal NMR of Biological Molecules
      Gang Wu 233

      16 Nitrogen-14 NMR Studies of Biological Systems
      Luminita Duma 255

      17 Oxygen-17 NMR Studies of Organic and Biological Molecules
      Gang Wu 273

      18 Oxygen-17 NMR of Inorganic Materials
      Sharon E. Ashbrook, Mark E. Smith 291

      19 Chlorine, Bromine, and Iodine Solid-State NMR
      David L. Bryce, Cory M. Widdifield, Rebecca P. Chapman, Robert J. Attrell 321

      20 Quadrupolar NMR of Ionic Conductors, Batteries, and other Energy-Related Materials
      Frédéric Blanc, Leigh Spencer, Gillian R. Goward 349

      21 Quadrupolar NMR of Nanoporous Materials
      Mohamed Haouas, Charlotte Martineau, Francis Taulelle 371

      22 Quadrupolar NMR in the Earth Sciences
      Jonathan F. Stebbins 387

      23 Quadrupolar NMR of Superconductors
      Nicholas J. Curro 401

      24 Quadrupolar NMR of Semiconductors
      James P. Yesinowski 417

      25 Quadrupolar NMR of Metal Nuclides in Biological Materials
      Tatyana Polenova, Andrew S. Lipton, Paul D. Ellis 439

      26 Nuclear Waste Glasses: Insights from Solid-State NMR
      Scott Kroeker 453

      27 Quadrupolar Metal NMR of Oxide Materials Including Catalysts
      Olga B. Lapina, Victor V. Terskikh 467

      28 Quadrupolar NMR of Intermetallic Compounds
      Frank Haarmann 495

      Index 511

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