Description

Book Synopsis
The content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the

Table of Contents

Contributors ix

Series Preface xiii

Volume Preface xv

Part A: Basic Principles 1

1 Quadrupolar Interactions
Pascal P. Man 3

2 Quadrupolar Nuclei in Solids
Alexander J. Vega 17

3 Quadrupolar Coupling: An Introduction and Crystallographic Aspects
Sharon E. Ashbrook, Stephen Wimperis 45

4 Quadrupolar Nuclei in Solids: Influence of Different Interactions on Spectra
David L. Bryce, Roderick E. Wasylishen 63

Part B: Advanced Techniques 75

5 Acquisition of Wideline Solid-State NMR Spectra of Quadrupolar Nuclei
Robert W. Schurko 77

6 Sensitivity and Resolution Enhancement of Half-Integer Quadrupolar Nuclei in Solid-State NMR
Thomas T. Nakashima, Roderick E. Wasylishen 95

7 Quadrupolar Nutation Spectroscopy
Arno P.M. Kentgens 107

8 Dynamic Angle Spinning
Philip J. Grandinetti 121

9 Double Rotation (DOR) NMR
Ray Dupree 133

10 MQMAS NMR: Experimental Strategies
Jean-Paul Amoureux, Marek Pruski 143

11 STMAS NMR: Experimental Advances
Sharon E. Ashbrook, Stephen Wimperis 163

12 Correlation Experiments Involving Half-Integer Quadrupolar Nuclei
Michael Deschamps, Dominique Massiot 179

13 Computing Electric Field Gradient Tensors
Josef W. Zwanziger 199

Part C: Applications 211

14 Quadrupolar NMR to Investigate Dynamics in Solid Materials
Luke A. O’Dell, Christopher I. Ratcliffe 213

15 Alkali Metal NMR of Biological Molecules
Gang Wu 233

16 Nitrogen-14 NMR Studies of Biological Systems
Luminita Duma 255

17 Oxygen-17 NMR Studies of Organic and Biological Molecules
Gang Wu 273

18 Oxygen-17 NMR of Inorganic Materials
Sharon E. Ashbrook, Mark E. Smith 291

19 Chlorine, Bromine, and Iodine Solid-State NMR
David L. Bryce, Cory M. Widdifield, Rebecca P. Chapman, Robert J. Attrell 321

20 Quadrupolar NMR of Ionic Conductors, Batteries, and other Energy-Related Materials
Frédéric Blanc, Leigh Spencer, Gillian R. Goward 349

21 Quadrupolar NMR of Nanoporous Materials
Mohamed Haouas, Charlotte Martineau, Francis Taulelle 371

22 Quadrupolar NMR in the Earth Sciences
Jonathan F. Stebbins 387

23 Quadrupolar NMR of Superconductors
Nicholas J. Curro 401

24 Quadrupolar NMR of Semiconductors
James P. Yesinowski 417

25 Quadrupolar NMR of Metal Nuclides in Biological Materials
Tatyana Polenova, Andrew S. Lipton, Paul D. Ellis 439

26 Nuclear Waste Glasses: Insights from Solid-State NMR
Scott Kroeker 453

27 Quadrupolar Metal NMR of Oxide Materials Including Catalysts
Olga B. Lapina, Victor V. Terskikh 467

28 Quadrupolar NMR of Intermetallic Compounds
Frank Haarmann 495

Index 511

NMR of Quadrupolar Nuclei in Solid Materials 3

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A Hardback by Roderick E. Wasylishen, Sharon E. Ashbrook, Stephen Wimperis

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    View other formats and editions of NMR of Quadrupolar Nuclei in Solid Materials 3 by Roderick E. Wasylishen

    Publisher: John Wiley & Sons Inc
    Publication Date: 15/06/2012
    ISBN13: 9780470973981, 978-0470973981
    ISBN10: 0470973986

    Description

    Book Synopsis
    The content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the

    Table of Contents

    Contributors ix

    Series Preface xiii

    Volume Preface xv

    Part A: Basic Principles 1

    1 Quadrupolar Interactions
    Pascal P. Man 3

    2 Quadrupolar Nuclei in Solids
    Alexander J. Vega 17

    3 Quadrupolar Coupling: An Introduction and Crystallographic Aspects
    Sharon E. Ashbrook, Stephen Wimperis 45

    4 Quadrupolar Nuclei in Solids: Influence of Different Interactions on Spectra
    David L. Bryce, Roderick E. Wasylishen 63

    Part B: Advanced Techniques 75

    5 Acquisition of Wideline Solid-State NMR Spectra of Quadrupolar Nuclei
    Robert W. Schurko 77

    6 Sensitivity and Resolution Enhancement of Half-Integer Quadrupolar Nuclei in Solid-State NMR
    Thomas T. Nakashima, Roderick E. Wasylishen 95

    7 Quadrupolar Nutation Spectroscopy
    Arno P.M. Kentgens 107

    8 Dynamic Angle Spinning
    Philip J. Grandinetti 121

    9 Double Rotation (DOR) NMR
    Ray Dupree 133

    10 MQMAS NMR: Experimental Strategies
    Jean-Paul Amoureux, Marek Pruski 143

    11 STMAS NMR: Experimental Advances
    Sharon E. Ashbrook, Stephen Wimperis 163

    12 Correlation Experiments Involving Half-Integer Quadrupolar Nuclei
    Michael Deschamps, Dominique Massiot 179

    13 Computing Electric Field Gradient Tensors
    Josef W. Zwanziger 199

    Part C: Applications 211

    14 Quadrupolar NMR to Investigate Dynamics in Solid Materials
    Luke A. O’Dell, Christopher I. Ratcliffe 213

    15 Alkali Metal NMR of Biological Molecules
    Gang Wu 233

    16 Nitrogen-14 NMR Studies of Biological Systems
    Luminita Duma 255

    17 Oxygen-17 NMR Studies of Organic and Biological Molecules
    Gang Wu 273

    18 Oxygen-17 NMR of Inorganic Materials
    Sharon E. Ashbrook, Mark E. Smith 291

    19 Chlorine, Bromine, and Iodine Solid-State NMR
    David L. Bryce, Cory M. Widdifield, Rebecca P. Chapman, Robert J. Attrell 321

    20 Quadrupolar NMR of Ionic Conductors, Batteries, and other Energy-Related Materials
    Frédéric Blanc, Leigh Spencer, Gillian R. Goward 349

    21 Quadrupolar NMR of Nanoporous Materials
    Mohamed Haouas, Charlotte Martineau, Francis Taulelle 371

    22 Quadrupolar NMR in the Earth Sciences
    Jonathan F. Stebbins 387

    23 Quadrupolar NMR of Superconductors
    Nicholas J. Curro 401

    24 Quadrupolar NMR of Semiconductors
    James P. Yesinowski 417

    25 Quadrupolar NMR of Metal Nuclides in Biological Materials
    Tatyana Polenova, Andrew S. Lipton, Paul D. Ellis 439

    26 Nuclear Waste Glasses: Insights from Solid-State NMR
    Scott Kroeker 453

    27 Quadrupolar Metal NMR of Oxide Materials Including Catalysts
    Olga B. Lapina, Victor V. Terskikh 467

    28 Quadrupolar NMR of Intermetallic Compounds
    Frank Haarmann 495

    Index 511

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