Description

Book Synopsis

Infrared spectroscopy is generally understood to mean the science of spectra relating to infrared radiation, namely electromagnetic waves, in the wavelength region occurring intermediately between visible light and microwaves. Measurements of infrared spectra have been providing useful information, for a variety of scientific research and industrial studies, for over half a century; this is set to continue in the foreseeable future.

Introduction to Experimental Infrared Spectroscopy is intended to be a handy guide for those who have no, or limited, experience in infrared spectroscopic measurements but are utilising infrared-related methods for their research or in practical applications.

Written by leading researchers and experienced practitioners, this work consists of 22 chapters and presents the basic theory, methodology and practical measurement methods, including ATR, photoacoustic, IR imaging, NIR, 2D-COS, and VCD. The six Appendices will aid readers in un

Trade Review

"If your next assignment incorporates any aspect of infrared spectroscopy, then Introduction to experimental infrared spectroscopy: fundamentals and practical methods is for you. This book integrates both theory and practice to offer a comprehensive and balanced textbook." (Chemistry in Australia 2016)



Table of Contents

List of Contributors ix

Preface xi

Part I Fundamentals of Infrared Spectroscopic Measurements 1

1. Introduction to Infrared Spectroscopy 3
Mitsuo Tasumi

2. Sample Handling and Related Matters in Infrared Spectroscopic Measurements 15
Akira Sakamoto

3. Quantitative Infrared Spectroscopic Analysis 29
Shukichi Ochiai

4. Principles of FT-IR Spectrometry 41
Koji Masutani

5. Hardware and Software in FT-IR Spectrometry 59
Koji Masutani

6. Computer Processing of Measured Infrared Spectra 83
Shukichi Ochiai

7. Chemometrics in Infrared Spectroscopic Analysis 97
Takeshi Hasegawa

Part II Practical Methods of Measurements 115

8. Reflection Measurements at Normal Incidence 117
Takeshi Hasegawa

9. External-Reflection Spectrometry for Thin Films and Surfaces 127
Takeshi Hasegawa

10. Reflection–Absorption Spectroscopy of Thin Layers on Metal Surfaces 141
Koji Masutani and Shukichi Ochiai

11. Polarization-Modulation Spectrometry and its Application to Reflection–Absorption Measurements 153
Koji Masutani

12. Diffuse-Reflection Measurements 169
Shukichi Ochiai

13. Attenuated Total Reflection Measurements 179
Shukichi Ochiai

14. Photoacoustic Spectrometry Measurements 199
Shukichi Ochiai

15. Emission Spectroscopic Measurements 209
Shukichi Ochiai

16. Infrared Microspectroscopic Measurements 223
Shukichi Ochiai and Hirofumi Seki

17. Infrared Microspectroscopic Imaging 241
Shigeru Shimada

18. Near-Infrared Spectroscopy 253
Masao Takayanagi

19. Far-Infrared Spectroscopy and Terahertz Time-Domain Spectroscopy 269
Seizi Nishizawa

20. Time-Resolved Infrared Absorption Measurements 287
Akira Sakamoto

21. Two-Dimensional Correlation Spectroscopy 307
Shigeaki Morita, Hideyuki Shinzawa, Isao Noda, and Yukihiro Ozaki

22. Vibrational Circular Dichroism 321
Yoshiaki Hamada

Part III Appendices 335

AppendixA The Speed, Frequency, Wavelength, and Wavenumber of an Electromagnetic Wave 337
Mitsuo Tasumi

Appendix B Formulae Expressing the Electric Field of an Electromagnetic Wave and Related Subjects 339
Mitsuo Tasumi

AppendixC Coherence of the Thermal Radiation 345
Mitsuo Tasumi

AppendixD Mathematical Methods in FT-IR Spectrometry 347
Mitsuo Tasumi

Appendix E Electromagnetic Pulse on the Time Axis and its Spectrum 359
Mitsuo Tasumi

Appendix F Basic Concept of Two-Dimensional Correlation Spectroscopy 363
Isao Noda

Index 375

Introduction to Experimental Infrared

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      Publisher: John Wiley & Sons Inc
      Publication Date: Publication Date: 31/10/2014
      ISBN13: 9780470665671, 978-0470665671
      ISBN10: 047066567X

      Description

      Book Synopsis

      Infrared spectroscopy is generally understood to mean the science of spectra relating to infrared radiation, namely electromagnetic waves, in the wavelength region occurring intermediately between visible light and microwaves. Measurements of infrared spectra have been providing useful information, for a variety of scientific research and industrial studies, for over half a century; this is set to continue in the foreseeable future.

      Introduction to Experimental Infrared Spectroscopy is intended to be a handy guide for those who have no, or limited, experience in infrared spectroscopic measurements but are utilising infrared-related methods for their research or in practical applications.

      Written by leading researchers and experienced practitioners, this work consists of 22 chapters and presents the basic theory, methodology and practical measurement methods, including ATR, photoacoustic, IR imaging, NIR, 2D-COS, and VCD. The six Appendices will aid readers in un

      Trade Review

      "If your next assignment incorporates any aspect of infrared spectroscopy, then Introduction to experimental infrared spectroscopy: fundamentals and practical methods is for you. This book integrates both theory and practice to offer a comprehensive and balanced textbook." (Chemistry in Australia 2016)



      Table of Contents

      List of Contributors ix

      Preface xi

      Part I Fundamentals of Infrared Spectroscopic Measurements 1

      1. Introduction to Infrared Spectroscopy 3
      Mitsuo Tasumi

      2. Sample Handling and Related Matters in Infrared Spectroscopic Measurements 15
      Akira Sakamoto

      3. Quantitative Infrared Spectroscopic Analysis 29
      Shukichi Ochiai

      4. Principles of FT-IR Spectrometry 41
      Koji Masutani

      5. Hardware and Software in FT-IR Spectrometry 59
      Koji Masutani

      6. Computer Processing of Measured Infrared Spectra 83
      Shukichi Ochiai

      7. Chemometrics in Infrared Spectroscopic Analysis 97
      Takeshi Hasegawa

      Part II Practical Methods of Measurements 115

      8. Reflection Measurements at Normal Incidence 117
      Takeshi Hasegawa

      9. External-Reflection Spectrometry for Thin Films and Surfaces 127
      Takeshi Hasegawa

      10. Reflection–Absorption Spectroscopy of Thin Layers on Metal Surfaces 141
      Koji Masutani and Shukichi Ochiai

      11. Polarization-Modulation Spectrometry and its Application to Reflection–Absorption Measurements 153
      Koji Masutani

      12. Diffuse-Reflection Measurements 169
      Shukichi Ochiai

      13. Attenuated Total Reflection Measurements 179
      Shukichi Ochiai

      14. Photoacoustic Spectrometry Measurements 199
      Shukichi Ochiai

      15. Emission Spectroscopic Measurements 209
      Shukichi Ochiai

      16. Infrared Microspectroscopic Measurements 223
      Shukichi Ochiai and Hirofumi Seki

      17. Infrared Microspectroscopic Imaging 241
      Shigeru Shimada

      18. Near-Infrared Spectroscopy 253
      Masao Takayanagi

      19. Far-Infrared Spectroscopy and Terahertz Time-Domain Spectroscopy 269
      Seizi Nishizawa

      20. Time-Resolved Infrared Absorption Measurements 287
      Akira Sakamoto

      21. Two-Dimensional Correlation Spectroscopy 307
      Shigeaki Morita, Hideyuki Shinzawa, Isao Noda, and Yukihiro Ozaki

      22. Vibrational Circular Dichroism 321
      Yoshiaki Hamada

      Part III Appendices 335

      AppendixA The Speed, Frequency, Wavelength, and Wavenumber of an Electromagnetic Wave 337
      Mitsuo Tasumi

      Appendix B Formulae Expressing the Electric Field of an Electromagnetic Wave and Related Subjects 339
      Mitsuo Tasumi

      AppendixC Coherence of the Thermal Radiation 345
      Mitsuo Tasumi

      AppendixD Mathematical Methods in FT-IR Spectrometry 347
      Mitsuo Tasumi

      Appendix E Electromagnetic Pulse on the Time Axis and its Spectrum 359
      Mitsuo Tasumi

      Appendix F Basic Concept of Two-Dimensional Correlation Spectroscopy 363
      Isao Noda

      Index 375

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