Description

Book Synopsis
Edited by key figures in 3D integration and written by top authors from high-tech companies and renowned research institutions, this book covers the intricate details of 3D process technology. As such, the main focus is on silicon via formation, bonding and debonding, thinning, via reveal and backside processing, both from a technological and a materials science perspective. The last part of the book is concerned with assessing and enhancing the reliability of the 3D integrated devices, which is a prerequisite for the large-scale implementation of this emerging technology.
Invaluable reading for materials scientists, semiconductor physicists, and those working in the semiconductor industry, as well as IT and electrical engineers.

Table of Contents

List of Contributors xvii

1 3D IC Integration Since 2008 1
Philip Garrou, Peter Ramm, and Mitsumasa Koyanagi

1.1 3D IC Nomenclature 1

1.2 Process Standardization 2

1.3 The Introduction of Interposers (2.5D) 4

1.4 The Foundries 6

1.4.1 TSMC 6

1.4.2 UMC 7

1.4.3 GlobalFoundries 7

1.5 Memory 7

1.5.1 Samsung 7

1.5.2 Micron 8

1.5.3 Hynix 9

1.6 The Assembly and Test Houses 9

1.7 3D IC Application Roadmaps 10

References 11

2 Key Applications and Market Trends for 3D Integration and Interposer Technologies 13
Rozalia Beica, Jean-Christophe Eloy, and Peter Ramm

2.1 Introduction 13

2.2 Advanced Packaging Importance in the Semiconductor Industry is Growing 16

2.3 3D Integration-Focused Activities – The Global IP Landscape 18

2.4 Applications, Technology, and Market Trends 22

References 32

3 Economic Drivers and Impediments for 2.5D/3D Integration 33
Philip Garrou

3.1 3D Performance Advantages 33

3.2 The Economics of Scaling 33

3.3 The Cost of Future Scaling 34

3.4 Cost Remains the Impediment to 2.5D and 3D Product Introduction 37

3.4.1 Required Economics for Interposer Use in Mobile Products 38

3.4.2 Silicon Interposer Pricing 38

References 40

4 Interposer Technology 41
Venky Sundaram and Rao R. Tummala

4.1 Definition of 2.5D Interposers 41

4.2 Interposer Drivers and Need 42

4.3 Comparison of Interposer Materials 44

4.4 Silicon Interposers with TSV 45

4.5 Lower Cost Interposers 48

4.5.1 Glass Interposers 48

4.5.1.1 Challenges in Glass Interposers 49

4.5.1.2 Small-Pitch Through-Package Via Hole Formation and Ultrathin Glass Handling 49

4.5.1.3 Metallization of Glass TPV 51

4.5.1.4 Reliability of Copper TPVs in Glass Interposers 52

4.5.1.5 Thermal Dissipation of Glass 53

4.5.1.6 Glass Interposer Fabrication with TPV and RDL 53

4.5.2 Low-CTE Organic Interposers 53

4.5.3 Polycrystalline Silicon Interposer 55

4.5.3.1 Polycrystalline Silicon Interposer Fabrication Process 56

4.6 Interposer Technical and Manufacturing Challenges 57

4.7 Interposer Application Examples 58

4.8 Conclusions 60

References 61

5 TSV Formation Overview 65
Dean Malta

5.1 Introduction 65

5.2 TSV Process Approaches 67

5.2.1 TSV-Middle Approach 68

5.2.2 Backside TSV-Last Approach 68

5.2.3 Front-Side TSV-Last Approach 69

5.3 TSV Fabrication Steps 70

5.3.1 TSV Etching 70

5.3.2 TSV Insulation 71

5.3.3 TSV Metallization 71

5.3.4 Overburden Removal by CMP 72

5.3.5 TSV Anneal 73

5.3.6 Temporary Carrier Wafer Bonding and Debonding 74

5.3.7 Wafer Thinning and TSV Reveal 74

5.4 Yield and Reliability 75

References 76

6 TSV Unit Processes and Integration 79
Sesh Ramaswami

6.1 Introduction 79

6.2 TSV Process Overview 80

6.3 TSV Unit Processes 82

6.3.1 Etching 82

6.3.2 Insulator Deposition with CVD 83

6.3.3 Metal Liner/Barrier Deposition with PVD 84

6.3.4 Via Filling by ECD of Copper 84

6.3.5 CMP of Copper 85

6.3.6 Temporary Bonding between Carrier and Device Wafer 86

6.3.7 Wafer Backside Thinning 86

6.3.8 Backside RDL 87

6.3.9 Metrology, Inspection, and Defect Review 87

6.4 Integration and Co-optimization of Unit Processes in Via Formation Sequence 88

6.5 Co-optimization of Unit Processes in Backside Processing and Via-Reveal Flow 89

6.6 Integration and Co-optimization of Unit Processes in Via-Last Flow 91

6.7 Integration with Packaging 92

6.8 Electrical Characterization of TSVs 92

6.9 Conclusions 96

References 97

7 TSV Formation at ASET 99
Hiroaki Ikeda

7.1 Introduction 99

7.2 Via-Last TSV for Both D2D and W2W Processes in ASET 103

7.3 TSV Process for D2D 105

7.3.1 Front-Side Bump Forming 106

7.3.2 Attach WSS and Thinning 106

7.3.3 Deep Si Etching from the Backside 107

7.3.4 Liner Deposition 107

7.3.5 Removal of SiO 2 at the Bottom of Via 107

7.3.6 Barrier Metal and Seed Layer Deposition by PVD 110

7.3.7 Cu Electroplating 110

7.3.8 Cmp 110

7.3.9 Backside Bump 111

7.3.10 Detach WSS 111

7.3.11 Dicing 112

7.4 TSV Process for W2W 113

7.4.1 Polymer Layer Coat and Development 114

7.4.2 Barrier Metal and Seed Layer Deposition 114

7.4.3 Cu Plating 114

7.4.4 CMP 115

7.4.5 First W2W Stacking (Face to Face) 116

7.4.6 Wafer Thinning and Deep Si Etching 116

7.4.7 TSV Liner Deposition and SiO2 Etching of Via Bottom 117

7.4.8 Barrier Metal and Seed Layer Deposition and Cu Plating 117

7.4.9 CMP 117

7.4.10 Next W2W Stacking 118

7.5 Conclusions 119

References 119

8 Laser-Assisted Wafer Processing: New Perspectives in Through-Substrate Via Drilling and Redistribution Layer Deposition 121
Marc B. Hoppenbrouwers, Gerrit Oosterhuis, Guido Knippels, and Fred Roozeboom

8.1 Introduction 121

8.2 Laser Drilling of TSVs 121

8.2.1 Cost of Ownership Comparison 121

8.2.2 Requirements for an Industrial TSV Laser Driller 123

8.2.3 Drilling Strategy 124

8.2.3.1 Mechanical 124

8.2.3.2 Optical 125

8.2.4 Experimental Drilling Results 126

8.3 Direct-Write Deposition of Redistribution Layers 126

8.3.1 Introduction on Redistribution Layers 126

8.3.2 Direct-Write Characteristics 127

8.3.3 Direct-Write Laser-Induced Forward Transfer 128

8.3.4 LIFT Results 130

8.4 Conclusions and Outlook 131

References 132

9 Temporary Bonding Material Requirements 135
Rama Puligadda

9.1 Introduction 135

9.2 Technology Options 136

9.2.1 Tapes and Waxes 136

9.2.2 Chemical Debonding 136

9.2.3 Thermoplastic Bonding Material and Slide Debonding 136

9.2.4 Debonding Using Release Layers 137

9.3 Requirements of a Temporary Bonding Material 138

9.4 Considerations for Successful Processing 139

9.4.1 Application of the Temporary Bonding Adhesive to the Device Wafer and Bonding to Carrier 139

9.4.2 Moisture and Contaminants on Surface 139

9.4.3 Total Thickness Variation 140

9.4.4 Squeeze Out 140

9.5 Surviving the Backside Process 141

9.5.1 Edge Trimming 142

9.5.2 Edge Cleaning 142

9.5.3 Temperature Excursions in Plasma Processes 143

9.5.4 Wafer Warpage due to CTE Mismatch 143

9.6 Debonding 144

9.6.1 Debonding Parameters in Slide-Off Debonding 144

9.6.2 Mechanical Damage to Interconnects 144

References 145

10 Temporary Bonding and Debonding – An Update on Materials and Methods 147
Wilfried Bair

10.1 Introduction 147

10.2 Carrier Selection for Temporary Bonding 148

10.3 Selection of Temporary Bonding Adhesives 151

10.4 Bonding and Debonding Processes 152

10.5 Equipment and Process Integration 155

References 156

11 ZoneBOND 1 : Recent Developments in Temporary Bonding and Room-Temperature Debonding 159
Thorsten Matthias, J€urgen Burggraf, Daniel Burgstaller, Markus Wimplinger, and Paul Lindner

11.1 Introduction 159

11.2 Thin Wafer Processing 159

11.2.1 Thin Wafer Total Thickness Variation 161

11.2.2 Wafer Alignment 163

11.3 ZoneBOND Room-Temperature Debonding 163

11.4 Conclusions 165

References 166

12 Temporary Bonding and Debonding at TOK 167
Shoji Otaka

12.1 Introduction 167

12.2 Zero Newton Technology 168

12.2.1 The Wafer Bonder 168

12.2.2 The Wafer Debonder 170

12.2.3 The Wafer Bonder and Debonder Equipment Lineups 170

12.2.4 Adhesives 170

12.2.5 Integration Process Performance 172

12.3 Conclusions 174

References 174

13 The 3MTM Wafer Support System (WSS) 175
Blake Dronen and Richard Webb

13.1 Introduction 175

13.2 System Description 175

13.3 General Advantages 177

13.4 High-Temperature Material Solutions 178

13.5 Process Considerations 180

13.5.1 Wafer and Adhesive Delamination 180

13.5.2 LTHC Glass Delamination 181

13.6 Future Directions 181

13.6.1 Thermal Stability 181

13.6.2 Elimination of Adhesion Control Agents 182

13.6.3 Laser-Free Release Layer 183

13.7 Summary 183

Reference 184

14 Comparison of Temporary Bonding and Debonding Process Flows 185
Matthew Lueck

14.1 Introduction 185

14.2 Studies of Wafer Bonding and Thinning 186

14.3 Backside Processing 186

14.4 Debonding and Cleaning 188

References 189

15 Thinning, Via Reveal, and Backside Processing – Overview 191
Eric Beyne, Anne Jourdain, and Alain Phommahaxay

15.1 Introduction 191

15.2 Wafer Edge Trimming 192

15.3 Thin Wafer Support Systems 194

15.3.1 Glass Carrier Support System with Laser Debonding Approach 196

15.3.2 Thermoplastic Glue Thin Wafer Support System – Thermal Slide Debondable System 196

15.3.3 Room-Temperature, Peel-Debondable Thin Wafer Support Systems 197

15.4 Wafer Thinning 198

15.5 Thin Wafer Backside Processing 202

15.5.1 Via-Middle Thin Wafer Backside Processing: “Via-Reveal” Process 202

15.5.1.1 Mechanical Via Reveal 202

15.5.1.2 “Soft” Via Reveal 202

15.5.2 Via-Last Thin Wafer Backside Processing 203

References 205

16 Backside Thinning and Stress-Relief Techniques for Thin Silicon Wafers 207
Christof Landesberger, Christoph Paschke, Hans-Peter Sp€ohrle, and Karlheinz Bock

16.1 Introduction 207

16.2 Thin Semiconductor Devices 207

16.3 Wafer Thinning Techniques 208

16.3.1 Wafer Grinding 209

16.3.2 Wet-Chemical Spin Etching 210

16.3.3 CMP Polishing 211

16.3.4 Plasma Dry Etching 212

16.3.5 Dry Polish 213

16.3.6 Chemical–Mechanical Grinding (CMG) 214

16.4 Fracture Tests for Thin Silicon Wafers 214

16.5 Comparison of Stress-Relief Techniques for Wafer Backside Thinning 216

16.6 Process Flow for Wafer Thinning and Dicing 220

16.7 Summary and Outlook on 3D Integration 222

References 223

17 Via Reveal and Backside Processing 227
Mitsumasa Koyanagi and Tetsu Tanaka

17.1 Introduction 227

17.2 Via Reveal and Backside Processing in Via-Middle Process 227

17.3 Backside Processing in Back-Via Process 232

17.4 Backside Processing and Impurity Gettering 234

17.5 Backside Processing for RDL Formation 237

References 239

18 Dicing, Grinding, and Polishing (Kiru Kezuru and Migaku) 241
Akihito Kawai

18.1 Introduction 241

18.2 Grinding and Polishing 241

18.2.1 Grinding General 241

18.2.1.1 Grinding Method 241

18.2.1.2 Rough Grinding and Fine Grinding 242

18.2.1.3 The Grinder Polisher 243

18.2.2 Thinning 243

18.2.2.1 Stress Relief 245

18.2.2.2 Die Attach Film 246

18.2.2.3 All-in-One System 246

18.2.2.4 Dicing Before Grinding 246

18.2.3 Grinding Topics for 3DIC Such as TSV Devices 246

18.2.3.1 Wafer Support System 246

18.2.3.2 Edge Trimming 247

18.2.3.3 Grinding to Improve Flatness 248

18.2.3.4 Higher Level of Cleanliness 248

18.2.3.5 Via Reveal 249

18.2.3.6 Planarization 249

18.3 Dicing 250

18.3.1 Blade Dicing General 250

18.3.1.1 Dicing Method 250

18.3.1.2 Blade Dicing Point 250

18.3.1.3 Blade 251

18.3.1.4 Optimization of Process Control 252

18.3.1.5 Dicer 252

18.3.1.6 Dual Dicing Applications 252

18.3.2 Thin Wafer Dicing 253

18.3.3 Low-k Dicing 254

18.3.4 Other Laser Dicing 254

18.3.4.1 Ablation 254

18.3.4.2 Laser Full Cut Application 255

18.3.4.3 Stealth Dicing (SD) 256

18.3.5 Dicing Topics for 3D-IC Such as TSV 257

18.3.5.1 Cutting of Chip on Chip (CoC) and Chip on Wafer (CoW) 258

18.3.5.2 Singulation of CoW and Wafer on Wafer (WoW) 259

18.4 Summary 260

Further Reading 260

19 Overview of Bonding and Assembly for 3D Integration 261
James J.-Q. Lu, Dingyou Zhang, and Peter Ramm

19.1 Introduction 261

19.2 Direct, Indirect, and Hybrid Bonding 262

19.3 Requirements for Bonding Process and Materials 263

19.4 Bonding Quality Characterization 267

19.5 Discussion of Specific Bonding and Assembly Technologies 269

19.6 Summary and Conclusions 273

References 274

20 Bonding and Assembly at TSMC 279
Douglas C.H. Yu

20.1 Introduction 279

20.2 Process Flow 280

20.3 Chip-on-Wafer Stacking 281

20.4 CoW-on-Substrate (CoWoS) Stacking 283

20.5 CoWoS Versus CoCoS 283

20.6 Testing and Known Good Stacks (KGS) 284

20.7 Future Perspectives 285

References 285

21 TSV Packaging Development at STATS ChipPAC 287
Rajendra D. Pendse

21.1 Introduction 287

21.2 Development of the 3DTSV Solution for Mobile Platforms 289

21.3 Alternative Approaches and Future Developments 293

References 294

22 Cu–SiO2 Hybrid Bonding 295
Léa Di Cioccio, S. Moreau, Loïc Sanchez, Floriane Baudin, Pierric Gueguen, Sebastien Mermoz, Yann Beilliard, and Rachid Taibi

22.1 Introduction 295

22.2 Blanket Cu–SiO2 Direct Bonding Principle 296

22.2.1 Chemical–Mechanical Polishing Parameters 296

22.3 Aligned Bonding 299

22.3.1 Wafer-to-Wafer Bonding 299

22.3.2 Die-to-Wafer Bonding in Pick-and-Place Equipment 299

22.3.3 Die-to-Wafer by the Self-Assembly Technique 300

22.4 Blanket Metal Direct Bonding Principle 302

22.5 Electrical Characterization 304

22.5.1 Wafer-to-Wafer and Die-to-Wafer Copper-Bonding Electrical Characterization 304

22.5.2 Reliability 307

22.5.3 Thermal Cycling 307

22.5.4 Stress Voiding (SIV) Test on 200 °C Postbonding Annealed Samples 308

22.5.5 Package-Level Electromigration Test 309

22.6 Conclusions 310

References 311

23 Bump Interconnect for 2.5D and 3D Integration 313
Alan Huffman

23.1 History 313

23.2 C4 Solder Bumps 315

23.3 Copper Pillar Bumps 316

23.4 Cu Bumps 319

23.5 Electromigration 320

References 322

24 Self-Assembly Based 3D and Heterointegration 325
Takafumi Fukushima and Jicheol Bea

24.1 Introduction 325

24.2 Self-Assembly Process 325

24.3 Key Parameters of Self-Assembly on Alignment Accuracies 327

24.4 How to Interconnect Self-Assembled Chips to Chips or Wafers 328

24.4.1 Flip-Chip-to-Wafer 3D Integration 329

24.4.2 Reconfigured-Wafer-to-Wafer 3D Integration 331

References 332

25 High-Accuracy Self-Alignment of Thin Silicon Dies on Plasma-Programmed Surfaces 335
Christof Landesberger, Mitsuru Hiroshima, Josef Weber, and Karlheinz Bock

25.1 Introduction 335

25.2 Principle of Fluidic Self-Alignment Process for Thin Dies 335

25.3 Plasma Programming of the Surface 336

25.4 Preparation of Materials for Self-Alignment Experiments 337

25.5 Self-Alignment Experiments 338

25.6 Results of Self-Alignment Experiments 339

25.7 Discussion 341

25.8 Conclusions 342

References 343

26 Challenges in 3D Fabrication 345
Douglas C.H. Yu

26.1 Introduction 345

26.2 High-Volume Manufacturing for 3D Integration 346

26.3 Technology Challenges 346

26.4 Front-Side and Backside Wafer Processes 346

26.5 Bonding and Underfills 350

26.6 Multitier Stacking 352

26.7 Wafer Thinning and Thin Die and Wafer Handling 353

26.8 Strata Packaging and Assembly 356

26.9 Yield Management 359

26.10 Reliability 360

26.11 Cost Management 362

26.12 Future Perspectives 362

References 364

27 Cu TSV Stress: Avoiding Cu Protrusion and Impact on Devices 365
Eric Beyne, Joke De Messemaeker, and Wei Guo

27.1 Introduction 365

27.2 Cu Stress in TSV 365

27.3 Mitigation of Cu Pumping 368

27.4 Impact of TSVs on FEOL Devices 371

References 378

28 Implications of Stress/Strain and Metal Contamination on Thinned Die 379
Kangwook Lee and Mariappan Murugesan

28.1 Introduction 379

28.2 Impacts of Cu Contamination on Device Reliabilities in Thinned 3DLSI 379

28.3 Impacts of Local Stress and Strain on Device Reliabilities in Thinned 3DLSI 386

28.3.1 Microbump-Induced Stresses in Stacked LSIs 387

28.3.2 Microbump-Induced TMS in LSI 388

28.3.3 Microbump-Induced LMS 389

References 391

29 Metrology Needs for 2.5D/3D Interconnects 393
Victor H. Vartanian, Richard A. Allen, Larry Smith, Klaus Hummler, Steve Olson, and Brian Sapp

29.1 Introduction: 2.5D and 3D Reference Flows 393

29.2 TSV Formation 394

29.2.1 TSV Etch Metrology 395

29.2.2 Liner, Barrier, and Seed Metrology 397

29.2.3 Copper Fill Metrology (TSV Voids) 399

29.2.4 Cross-Sectional SEM (Focused Ion Beam Milling Sample Preparation) 400

29.2.5 X-Ray Microscopy and CT Inspection 400

29.2.6 Stress Metrology in Cu and Si 402

29.3 MEOL Metrology 404

29.3.1 Edge Trim Inspection 405

29.3.2 Bond Voids and Bond Strength Metrology 406

29.3.2.1 Acoustic Microscopy: Operation 407

29.3.2.2 Acoustic Microscopy for Defect Inspection and Review 407

29.3.2.3 Other Bond Void Detection Techniques 408

29.3.3 Bond Strength Metrology 409

29.3.4 Bonded Wafer Thickness, Bow, and Warp 410

29.3.4.1 Chromatic White Light 411

29.3.4.2 Infrared Interferometry 412

29.3.4.3 White Light Interferometry (or Coherence Scanning Interferometry) 414

29.3.4.4 Laser Profiling 415

29.3.4.5 Capacitance Probes 416

29.3.4.6 Differential Backpressure Metrology 417

29.3.4.7 Acoustic Microscopy for Measuring Bonded Wafer Thickness 417

29.3.5 TSV Reveal Metrology 418

29.4 Assembly and Packaging Metrology 420

29.4.1 Wafer-Level C4 Bump and Microbump Metrology and Inspection 421

29.4.2 Package-Level Inspection: Scanning Acoustic Microscopy 422

29.4.3 Package-Level Inspection: X-Rays 424

29.5 Summary 426

References 427

Index 431

Handbook of 3D Integration, Volume 3: 3D Process

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      View other formats and editions of Handbook of 3D Integration, Volume 3: 3D Process by Philip Garrou

      Publisher: Wiley-VCH Verlag GmbH
      Publication Date: Publication Date: 04/06/2014
      ISBN13: 9783527334667, 978-3527334667
      ISBN10: 3527334661

      Description

      Book Synopsis
      Edited by key figures in 3D integration and written by top authors from high-tech companies and renowned research institutions, this book covers the intricate details of 3D process technology. As such, the main focus is on silicon via formation, bonding and debonding, thinning, via reveal and backside processing, both from a technological and a materials science perspective. The last part of the book is concerned with assessing and enhancing the reliability of the 3D integrated devices, which is a prerequisite for the large-scale implementation of this emerging technology.
      Invaluable reading for materials scientists, semiconductor physicists, and those working in the semiconductor industry, as well as IT and electrical engineers.

      Table of Contents

      List of Contributors xvii

      1 3D IC Integration Since 2008 1
      Philip Garrou, Peter Ramm, and Mitsumasa Koyanagi

      1.1 3D IC Nomenclature 1

      1.2 Process Standardization 2

      1.3 The Introduction of Interposers (2.5D) 4

      1.4 The Foundries 6

      1.4.1 TSMC 6

      1.4.2 UMC 7

      1.4.3 GlobalFoundries 7

      1.5 Memory 7

      1.5.1 Samsung 7

      1.5.2 Micron 8

      1.5.3 Hynix 9

      1.6 The Assembly and Test Houses 9

      1.7 3D IC Application Roadmaps 10

      References 11

      2 Key Applications and Market Trends for 3D Integration and Interposer Technologies 13
      Rozalia Beica, Jean-Christophe Eloy, and Peter Ramm

      2.1 Introduction 13

      2.2 Advanced Packaging Importance in the Semiconductor Industry is Growing 16

      2.3 3D Integration-Focused Activities – The Global IP Landscape 18

      2.4 Applications, Technology, and Market Trends 22

      References 32

      3 Economic Drivers and Impediments for 2.5D/3D Integration 33
      Philip Garrou

      3.1 3D Performance Advantages 33

      3.2 The Economics of Scaling 33

      3.3 The Cost of Future Scaling 34

      3.4 Cost Remains the Impediment to 2.5D and 3D Product Introduction 37

      3.4.1 Required Economics for Interposer Use in Mobile Products 38

      3.4.2 Silicon Interposer Pricing 38

      References 40

      4 Interposer Technology 41
      Venky Sundaram and Rao R. Tummala

      4.1 Definition of 2.5D Interposers 41

      4.2 Interposer Drivers and Need 42

      4.3 Comparison of Interposer Materials 44

      4.4 Silicon Interposers with TSV 45

      4.5 Lower Cost Interposers 48

      4.5.1 Glass Interposers 48

      4.5.1.1 Challenges in Glass Interposers 49

      4.5.1.2 Small-Pitch Through-Package Via Hole Formation and Ultrathin Glass Handling 49

      4.5.1.3 Metallization of Glass TPV 51

      4.5.1.4 Reliability of Copper TPVs in Glass Interposers 52

      4.5.1.5 Thermal Dissipation of Glass 53

      4.5.1.6 Glass Interposer Fabrication with TPV and RDL 53

      4.5.2 Low-CTE Organic Interposers 53

      4.5.3 Polycrystalline Silicon Interposer 55

      4.5.3.1 Polycrystalline Silicon Interposer Fabrication Process 56

      4.6 Interposer Technical and Manufacturing Challenges 57

      4.7 Interposer Application Examples 58

      4.8 Conclusions 60

      References 61

      5 TSV Formation Overview 65
      Dean Malta

      5.1 Introduction 65

      5.2 TSV Process Approaches 67

      5.2.1 TSV-Middle Approach 68

      5.2.2 Backside TSV-Last Approach 68

      5.2.3 Front-Side TSV-Last Approach 69

      5.3 TSV Fabrication Steps 70

      5.3.1 TSV Etching 70

      5.3.2 TSV Insulation 71

      5.3.3 TSV Metallization 71

      5.3.4 Overburden Removal by CMP 72

      5.3.5 TSV Anneal 73

      5.3.6 Temporary Carrier Wafer Bonding and Debonding 74

      5.3.7 Wafer Thinning and TSV Reveal 74

      5.4 Yield and Reliability 75

      References 76

      6 TSV Unit Processes and Integration 79
      Sesh Ramaswami

      6.1 Introduction 79

      6.2 TSV Process Overview 80

      6.3 TSV Unit Processes 82

      6.3.1 Etching 82

      6.3.2 Insulator Deposition with CVD 83

      6.3.3 Metal Liner/Barrier Deposition with PVD 84

      6.3.4 Via Filling by ECD of Copper 84

      6.3.5 CMP of Copper 85

      6.3.6 Temporary Bonding between Carrier and Device Wafer 86

      6.3.7 Wafer Backside Thinning 86

      6.3.8 Backside RDL 87

      6.3.9 Metrology, Inspection, and Defect Review 87

      6.4 Integration and Co-optimization of Unit Processes in Via Formation Sequence 88

      6.5 Co-optimization of Unit Processes in Backside Processing and Via-Reveal Flow 89

      6.6 Integration and Co-optimization of Unit Processes in Via-Last Flow 91

      6.7 Integration with Packaging 92

      6.8 Electrical Characterization of TSVs 92

      6.9 Conclusions 96

      References 97

      7 TSV Formation at ASET 99
      Hiroaki Ikeda

      7.1 Introduction 99

      7.2 Via-Last TSV for Both D2D and W2W Processes in ASET 103

      7.3 TSV Process for D2D 105

      7.3.1 Front-Side Bump Forming 106

      7.3.2 Attach WSS and Thinning 106

      7.3.3 Deep Si Etching from the Backside 107

      7.3.4 Liner Deposition 107

      7.3.5 Removal of SiO 2 at the Bottom of Via 107

      7.3.6 Barrier Metal and Seed Layer Deposition by PVD 110

      7.3.7 Cu Electroplating 110

      7.3.8 Cmp 110

      7.3.9 Backside Bump 111

      7.3.10 Detach WSS 111

      7.3.11 Dicing 112

      7.4 TSV Process for W2W 113

      7.4.1 Polymer Layer Coat and Development 114

      7.4.2 Barrier Metal and Seed Layer Deposition 114

      7.4.3 Cu Plating 114

      7.4.4 CMP 115

      7.4.5 First W2W Stacking (Face to Face) 116

      7.4.6 Wafer Thinning and Deep Si Etching 116

      7.4.7 TSV Liner Deposition and SiO2 Etching of Via Bottom 117

      7.4.8 Barrier Metal and Seed Layer Deposition and Cu Plating 117

      7.4.9 CMP 117

      7.4.10 Next W2W Stacking 118

      7.5 Conclusions 119

      References 119

      8 Laser-Assisted Wafer Processing: New Perspectives in Through-Substrate Via Drilling and Redistribution Layer Deposition 121
      Marc B. Hoppenbrouwers, Gerrit Oosterhuis, Guido Knippels, and Fred Roozeboom

      8.1 Introduction 121

      8.2 Laser Drilling of TSVs 121

      8.2.1 Cost of Ownership Comparison 121

      8.2.2 Requirements for an Industrial TSV Laser Driller 123

      8.2.3 Drilling Strategy 124

      8.2.3.1 Mechanical 124

      8.2.3.2 Optical 125

      8.2.4 Experimental Drilling Results 126

      8.3 Direct-Write Deposition of Redistribution Layers 126

      8.3.1 Introduction on Redistribution Layers 126

      8.3.2 Direct-Write Characteristics 127

      8.3.3 Direct-Write Laser-Induced Forward Transfer 128

      8.3.4 LIFT Results 130

      8.4 Conclusions and Outlook 131

      References 132

      9 Temporary Bonding Material Requirements 135
      Rama Puligadda

      9.1 Introduction 135

      9.2 Technology Options 136

      9.2.1 Tapes and Waxes 136

      9.2.2 Chemical Debonding 136

      9.2.3 Thermoplastic Bonding Material and Slide Debonding 136

      9.2.4 Debonding Using Release Layers 137

      9.3 Requirements of a Temporary Bonding Material 138

      9.4 Considerations for Successful Processing 139

      9.4.1 Application of the Temporary Bonding Adhesive to the Device Wafer and Bonding to Carrier 139

      9.4.2 Moisture and Contaminants on Surface 139

      9.4.3 Total Thickness Variation 140

      9.4.4 Squeeze Out 140

      9.5 Surviving the Backside Process 141

      9.5.1 Edge Trimming 142

      9.5.2 Edge Cleaning 142

      9.5.3 Temperature Excursions in Plasma Processes 143

      9.5.4 Wafer Warpage due to CTE Mismatch 143

      9.6 Debonding 144

      9.6.1 Debonding Parameters in Slide-Off Debonding 144

      9.6.2 Mechanical Damage to Interconnects 144

      References 145

      10 Temporary Bonding and Debonding – An Update on Materials and Methods 147
      Wilfried Bair

      10.1 Introduction 147

      10.2 Carrier Selection for Temporary Bonding 148

      10.3 Selection of Temporary Bonding Adhesives 151

      10.4 Bonding and Debonding Processes 152

      10.5 Equipment and Process Integration 155

      References 156

      11 ZoneBOND 1 : Recent Developments in Temporary Bonding and Room-Temperature Debonding 159
      Thorsten Matthias, J€urgen Burggraf, Daniel Burgstaller, Markus Wimplinger, and Paul Lindner

      11.1 Introduction 159

      11.2 Thin Wafer Processing 159

      11.2.1 Thin Wafer Total Thickness Variation 161

      11.2.2 Wafer Alignment 163

      11.3 ZoneBOND Room-Temperature Debonding 163

      11.4 Conclusions 165

      References 166

      12 Temporary Bonding and Debonding at TOK 167
      Shoji Otaka

      12.1 Introduction 167

      12.2 Zero Newton Technology 168

      12.2.1 The Wafer Bonder 168

      12.2.2 The Wafer Debonder 170

      12.2.3 The Wafer Bonder and Debonder Equipment Lineups 170

      12.2.4 Adhesives 170

      12.2.5 Integration Process Performance 172

      12.3 Conclusions 174

      References 174

      13 The 3MTM Wafer Support System (WSS) 175
      Blake Dronen and Richard Webb

      13.1 Introduction 175

      13.2 System Description 175

      13.3 General Advantages 177

      13.4 High-Temperature Material Solutions 178

      13.5 Process Considerations 180

      13.5.1 Wafer and Adhesive Delamination 180

      13.5.2 LTHC Glass Delamination 181

      13.6 Future Directions 181

      13.6.1 Thermal Stability 181

      13.6.2 Elimination of Adhesion Control Agents 182

      13.6.3 Laser-Free Release Layer 183

      13.7 Summary 183

      Reference 184

      14 Comparison of Temporary Bonding and Debonding Process Flows 185
      Matthew Lueck

      14.1 Introduction 185

      14.2 Studies of Wafer Bonding and Thinning 186

      14.3 Backside Processing 186

      14.4 Debonding and Cleaning 188

      References 189

      15 Thinning, Via Reveal, and Backside Processing – Overview 191
      Eric Beyne, Anne Jourdain, and Alain Phommahaxay

      15.1 Introduction 191

      15.2 Wafer Edge Trimming 192

      15.3 Thin Wafer Support Systems 194

      15.3.1 Glass Carrier Support System with Laser Debonding Approach 196

      15.3.2 Thermoplastic Glue Thin Wafer Support System – Thermal Slide Debondable System 196

      15.3.3 Room-Temperature, Peel-Debondable Thin Wafer Support Systems 197

      15.4 Wafer Thinning 198

      15.5 Thin Wafer Backside Processing 202

      15.5.1 Via-Middle Thin Wafer Backside Processing: “Via-Reveal” Process 202

      15.5.1.1 Mechanical Via Reveal 202

      15.5.1.2 “Soft” Via Reveal 202

      15.5.2 Via-Last Thin Wafer Backside Processing 203

      References 205

      16 Backside Thinning and Stress-Relief Techniques for Thin Silicon Wafers 207
      Christof Landesberger, Christoph Paschke, Hans-Peter Sp€ohrle, and Karlheinz Bock

      16.1 Introduction 207

      16.2 Thin Semiconductor Devices 207

      16.3 Wafer Thinning Techniques 208

      16.3.1 Wafer Grinding 209

      16.3.2 Wet-Chemical Spin Etching 210

      16.3.3 CMP Polishing 211

      16.3.4 Plasma Dry Etching 212

      16.3.5 Dry Polish 213

      16.3.6 Chemical–Mechanical Grinding (CMG) 214

      16.4 Fracture Tests for Thin Silicon Wafers 214

      16.5 Comparison of Stress-Relief Techniques for Wafer Backside Thinning 216

      16.6 Process Flow for Wafer Thinning and Dicing 220

      16.7 Summary and Outlook on 3D Integration 222

      References 223

      17 Via Reveal and Backside Processing 227
      Mitsumasa Koyanagi and Tetsu Tanaka

      17.1 Introduction 227

      17.2 Via Reveal and Backside Processing in Via-Middle Process 227

      17.3 Backside Processing in Back-Via Process 232

      17.4 Backside Processing and Impurity Gettering 234

      17.5 Backside Processing for RDL Formation 237

      References 239

      18 Dicing, Grinding, and Polishing (Kiru Kezuru and Migaku) 241
      Akihito Kawai

      18.1 Introduction 241

      18.2 Grinding and Polishing 241

      18.2.1 Grinding General 241

      18.2.1.1 Grinding Method 241

      18.2.1.2 Rough Grinding and Fine Grinding 242

      18.2.1.3 The Grinder Polisher 243

      18.2.2 Thinning 243

      18.2.2.1 Stress Relief 245

      18.2.2.2 Die Attach Film 246

      18.2.2.3 All-in-One System 246

      18.2.2.4 Dicing Before Grinding 246

      18.2.3 Grinding Topics for 3DIC Such as TSV Devices 246

      18.2.3.1 Wafer Support System 246

      18.2.3.2 Edge Trimming 247

      18.2.3.3 Grinding to Improve Flatness 248

      18.2.3.4 Higher Level of Cleanliness 248

      18.2.3.5 Via Reveal 249

      18.2.3.6 Planarization 249

      18.3 Dicing 250

      18.3.1 Blade Dicing General 250

      18.3.1.1 Dicing Method 250

      18.3.1.2 Blade Dicing Point 250

      18.3.1.3 Blade 251

      18.3.1.4 Optimization of Process Control 252

      18.3.1.5 Dicer 252

      18.3.1.6 Dual Dicing Applications 252

      18.3.2 Thin Wafer Dicing 253

      18.3.3 Low-k Dicing 254

      18.3.4 Other Laser Dicing 254

      18.3.4.1 Ablation 254

      18.3.4.2 Laser Full Cut Application 255

      18.3.4.3 Stealth Dicing (SD) 256

      18.3.5 Dicing Topics for 3D-IC Such as TSV 257

      18.3.5.1 Cutting of Chip on Chip (CoC) and Chip on Wafer (CoW) 258

      18.3.5.2 Singulation of CoW and Wafer on Wafer (WoW) 259

      18.4 Summary 260

      Further Reading 260

      19 Overview of Bonding and Assembly for 3D Integration 261
      James J.-Q. Lu, Dingyou Zhang, and Peter Ramm

      19.1 Introduction 261

      19.2 Direct, Indirect, and Hybrid Bonding 262

      19.3 Requirements for Bonding Process and Materials 263

      19.4 Bonding Quality Characterization 267

      19.5 Discussion of Specific Bonding and Assembly Technologies 269

      19.6 Summary and Conclusions 273

      References 274

      20 Bonding and Assembly at TSMC 279
      Douglas C.H. Yu

      20.1 Introduction 279

      20.2 Process Flow 280

      20.3 Chip-on-Wafer Stacking 281

      20.4 CoW-on-Substrate (CoWoS) Stacking 283

      20.5 CoWoS Versus CoCoS 283

      20.6 Testing and Known Good Stacks (KGS) 284

      20.7 Future Perspectives 285

      References 285

      21 TSV Packaging Development at STATS ChipPAC 287
      Rajendra D. Pendse

      21.1 Introduction 287

      21.2 Development of the 3DTSV Solution for Mobile Platforms 289

      21.3 Alternative Approaches and Future Developments 293

      References 294

      22 Cu–SiO2 Hybrid Bonding 295
      Léa Di Cioccio, S. Moreau, Loïc Sanchez, Floriane Baudin, Pierric Gueguen, Sebastien Mermoz, Yann Beilliard, and Rachid Taibi

      22.1 Introduction 295

      22.2 Blanket Cu–SiO2 Direct Bonding Principle 296

      22.2.1 Chemical–Mechanical Polishing Parameters 296

      22.3 Aligned Bonding 299

      22.3.1 Wafer-to-Wafer Bonding 299

      22.3.2 Die-to-Wafer Bonding in Pick-and-Place Equipment 299

      22.3.3 Die-to-Wafer by the Self-Assembly Technique 300

      22.4 Blanket Metal Direct Bonding Principle 302

      22.5 Electrical Characterization 304

      22.5.1 Wafer-to-Wafer and Die-to-Wafer Copper-Bonding Electrical Characterization 304

      22.5.2 Reliability 307

      22.5.3 Thermal Cycling 307

      22.5.4 Stress Voiding (SIV) Test on 200 °C Postbonding Annealed Samples 308

      22.5.5 Package-Level Electromigration Test 309

      22.6 Conclusions 310

      References 311

      23 Bump Interconnect for 2.5D and 3D Integration 313
      Alan Huffman

      23.1 History 313

      23.2 C4 Solder Bumps 315

      23.3 Copper Pillar Bumps 316

      23.4 Cu Bumps 319

      23.5 Electromigration 320

      References 322

      24 Self-Assembly Based 3D and Heterointegration 325
      Takafumi Fukushima and Jicheol Bea

      24.1 Introduction 325

      24.2 Self-Assembly Process 325

      24.3 Key Parameters of Self-Assembly on Alignment Accuracies 327

      24.4 How to Interconnect Self-Assembled Chips to Chips or Wafers 328

      24.4.1 Flip-Chip-to-Wafer 3D Integration 329

      24.4.2 Reconfigured-Wafer-to-Wafer 3D Integration 331

      References 332

      25 High-Accuracy Self-Alignment of Thin Silicon Dies on Plasma-Programmed Surfaces 335
      Christof Landesberger, Mitsuru Hiroshima, Josef Weber, and Karlheinz Bock

      25.1 Introduction 335

      25.2 Principle of Fluidic Self-Alignment Process for Thin Dies 335

      25.3 Plasma Programming of the Surface 336

      25.4 Preparation of Materials for Self-Alignment Experiments 337

      25.5 Self-Alignment Experiments 338

      25.6 Results of Self-Alignment Experiments 339

      25.7 Discussion 341

      25.8 Conclusions 342

      References 343

      26 Challenges in 3D Fabrication 345
      Douglas C.H. Yu

      26.1 Introduction 345

      26.2 High-Volume Manufacturing for 3D Integration 346

      26.3 Technology Challenges 346

      26.4 Front-Side and Backside Wafer Processes 346

      26.5 Bonding and Underfills 350

      26.6 Multitier Stacking 352

      26.7 Wafer Thinning and Thin Die and Wafer Handling 353

      26.8 Strata Packaging and Assembly 356

      26.9 Yield Management 359

      26.10 Reliability 360

      26.11 Cost Management 362

      26.12 Future Perspectives 362

      References 364

      27 Cu TSV Stress: Avoiding Cu Protrusion and Impact on Devices 365
      Eric Beyne, Joke De Messemaeker, and Wei Guo

      27.1 Introduction 365

      27.2 Cu Stress in TSV 365

      27.3 Mitigation of Cu Pumping 368

      27.4 Impact of TSVs on FEOL Devices 371

      References 378

      28 Implications of Stress/Strain and Metal Contamination on Thinned Die 379
      Kangwook Lee and Mariappan Murugesan

      28.1 Introduction 379

      28.2 Impacts of Cu Contamination on Device Reliabilities in Thinned 3DLSI 379

      28.3 Impacts of Local Stress and Strain on Device Reliabilities in Thinned 3DLSI 386

      28.3.1 Microbump-Induced Stresses in Stacked LSIs 387

      28.3.2 Microbump-Induced TMS in LSI 388

      28.3.3 Microbump-Induced LMS 389

      References 391

      29 Metrology Needs for 2.5D/3D Interconnects 393
      Victor H. Vartanian, Richard A. Allen, Larry Smith, Klaus Hummler, Steve Olson, and Brian Sapp

      29.1 Introduction: 2.5D and 3D Reference Flows 393

      29.2 TSV Formation 394

      29.2.1 TSV Etch Metrology 395

      29.2.2 Liner, Barrier, and Seed Metrology 397

      29.2.3 Copper Fill Metrology (TSV Voids) 399

      29.2.4 Cross-Sectional SEM (Focused Ion Beam Milling Sample Preparation) 400

      29.2.5 X-Ray Microscopy and CT Inspection 400

      29.2.6 Stress Metrology in Cu and Si 402

      29.3 MEOL Metrology 404

      29.3.1 Edge Trim Inspection 405

      29.3.2 Bond Voids and Bond Strength Metrology 406

      29.3.2.1 Acoustic Microscopy: Operation 407

      29.3.2.2 Acoustic Microscopy for Defect Inspection and Review 407

      29.3.2.3 Other Bond Void Detection Techniques 408

      29.3.3 Bond Strength Metrology 409

      29.3.4 Bonded Wafer Thickness, Bow, and Warp 410

      29.3.4.1 Chromatic White Light 411

      29.3.4.2 Infrared Interferometry 412

      29.3.4.3 White Light Interferometry (or Coherence Scanning Interferometry) 414

      29.3.4.4 Laser Profiling 415

      29.3.4.5 Capacitance Probes 416

      29.3.4.6 Differential Backpressure Metrology 417

      29.3.4.7 Acoustic Microscopy for Measuring Bonded Wafer Thickness 417

      29.3.5 TSV Reveal Metrology 418

      29.4 Assembly and Packaging Metrology 420

      29.4.1 Wafer-Level C4 Bump and Microbump Metrology and Inspection 421

      29.4.2 Package-Level Inspection: Scanning Acoustic Microscopy 422

      29.4.3 Package-Level Inspection: X-Rays 424

      29.5 Summary 426

      References 427

      Index 431

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