{"product_id":"the-organic-chem-lab-survival-manual-9781119608554","title":"The Organic Chem Lab Survival Manual","description":"\u003cb\u003eBook Synopsis\u003c\/b\u003e\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cb\u003eTable of Contents\u003c\/b\u003e\u003cbr\u003e\u003cp\u003e\u003cb\u003eChapter 1 Safety First, Last, and Always 1\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eAccidents Will Not Happen 5\u003c\/p\u003e \u003cp\u003eDisposing of Waste 5\u003c\/p\u003e \u003cp\u003eMixed Waste 7\u003c\/p\u003e \u003cp\u003eMaterial Safety Data Sheet (Msds) 8\u003c\/p\u003e \u003cp\u003eGreen Chemistry and Planning an Organic Synthesis 8\u003c\/p\u003e \u003cp\u003eAn iBag for Your iThing 10\u003c\/p\u003e \u003cp\u003eExercises 10\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 2 Keeping a Notebook 11\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eA Technique Experiment 12\u003c\/p\u003e \u003cp\u003eNotebook Notes 12\u003c\/p\u003e \u003cp\u003eA Synthesis Experiment 16\u003c\/p\u003e \u003cp\u003eNotebook Notes 17\u003c\/p\u003e \u003cp\u003eThe Six Maybe Seven Elements in Your Experimental Write-Up 20\u003c\/p\u003e \u003cp\u003eThe Acid Test 21\u003c\/p\u003e \u003cp\u003eNotebook Mortal Sin 21\u003c\/p\u003e \u003cp\u003eCalculation of Percent Yield (Not Yeild!) 22\u003c\/p\u003e \u003cp\u003eEstimation Is Your Friend 24\u003c\/p\u003e \u003cp\u003eExercises 24\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 3 Mining Your Own Data 25\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eGoogle and the Wiki 26\u003c\/p\u003e \u003cp\u003eThe Terphenyl Anomaly 29\u003c\/p\u003e \u003cp\u003eExercises 29\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 4 Jointware 30\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eStoppers With Only One Number 31\u003c\/p\u003e \u003cp\u003eAnother Episode of Love of Laboratory 33\u003c\/p\u003e \u003cp\u003eHall of Blunders and Things Not Quite Right 34\u003c\/p\u003e \u003cp\u003eRound-Bottom Flasks 34\u003c\/p\u003e \u003cp\u003eColumns and Condensers 34\u003c\/p\u003e \u003cp\u003eThe Adapter with Lots of Names 35\u003c\/p\u003e \u003cp\u003eForgetting the Glass 36\u003c\/p\u003e \u003cp\u003eInserting Adapter Upside Down 36\u003c\/p\u003e \u003cp\u003eInserting Adapter Upside Down \u003ci\u003esans \u003c\/i\u003eGlass 37\u003c\/p\u003e \u003cp\u003eThe O-Ring and Cap Branch Out 38\u003c\/p\u003e \u003cp\u003eGreasing the Joints 38\u003c\/p\u003e \u003cp\u003eTo Grease or Not to Grease 38\u003c\/p\u003e \u003cp\u003ePreparation of the Joints 39\u003c\/p\u003e \u003cp\u003eInto the Grease Pit 39\u003c\/p\u003e \u003cp\u003eStoring Stuff and Sticking Stoppers 40\u003c\/p\u003e \u003cp\u003eCorking a Vessel 40\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 5 Microscale Jointware 41\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eMicroscale: A Few Words 41\u003c\/p\u003e \u003cp\u003eUh-Oh Rings 42\u003c\/p\u003e \u003cp\u003eThe O-Ring Cap Seal 42\u003c\/p\u003e \u003cp\u003eSkinny Apparatus 42\u003c\/p\u003e \u003cp\u003eNot-So-Skinny Apparatus 43\u003c\/p\u003e \u003cp\u003eSizing Up the Situation 43\u003c\/p\u003e \u003cp\u003eWhy I Don’t Really Know How Vacuum-Tight These Seals Are 44\u003c\/p\u003e \u003cp\u003eThe Comical Vial (That’s \u003ci\u003eConical\u003c\/i\u003e!) 45\u003c\/p\u003e \u003cp\u003eThe Conical Vial as Vial 45\u003c\/p\u003e \u003cp\u003ePackaging Oops 46\u003c\/p\u003e \u003cp\u003eTare to the Analytical Balance 46\u003c\/p\u003e \u003cp\u003eThe Electronic Analytical Balance 46\u003c\/p\u003e \u003cp\u003eHeating These Vials 47\u003c\/p\u003e \u003cp\u003eThe Microscale Drying Tube 48\u003c\/p\u003e \u003cp\u003eGas Collection Apparatus 48\u003c\/p\u003e \u003cp\u003eGenerating the Gas 49\u003c\/p\u003e \u003cp\u003eIsolating the Product 51\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 6 Other Interesting Equipment 52\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eFunnels, and Beakers, and Flasks—Oh My! 53\u003c\/p\u003e \u003cp\u003eThe Flexible Double-Ended Stainless Steel Spatula 54\u003c\/p\u003e \u003cp\u003eTransferring a Powdered Solid with the Spatula 55\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 7 Pipet Tips 56\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003ePre-Preparing Pasteur Pipets 56\u003c\/p\u003e \u003cp\u003eCalibration 56\u003c\/p\u003e \u003cp\u003eOperation 57\u003c\/p\u003e \u003cp\u003eAmelioration 58\u003c\/p\u003e \u003cp\u003ePipet Cutting 58\u003c\/p\u003e \u003cp\u003ePipet Filtering—Liquids 60\u003c\/p\u003e \u003cp\u003ePipet Filtering—Solids 61\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 8 Syringes, Needles, and Septa 63\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eThe Rubber Septum 65\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 9 Clean and Dry 66\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eDrying Your Glassware When You Don’t Need To 67\u003c\/p\u003e \u003cp\u003eDrying Your Glassware When You Do Need To 67\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 10 Drying Agents 68\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eTypical Drying Agents 68\u003c\/p\u003e \u003cp\u003eUsing a Drying Agent 69\u003c\/p\u003e \u003cp\u003eFollowing Directions and Losing Product Anyway 70\u003c\/p\u003e \u003cp\u003eDrying Agents: Microscale 70\u003c\/p\u003e \u003cp\u003eDrying in Stages: The Capacity and Efficiency of Drying Agents 70\u003c\/p\u003e \u003cp\u003eExercises 71\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 11 On Products 72\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eSolid Product Problems 72\u003c\/p\u003e \u003cp\u003eLiquid Product Problems 72\u003c\/p\u003e \u003cp\u003eThe Sample Vial 73\u003c\/p\u003e \u003cp\u003eHold It! Don’t Touch That Vial 73\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 12 The Melting-Point Experiment 74\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eSample Preparation 75\u003c\/p\u003e \u003cp\u003eLoading the Melting-Point Tube 75\u003c\/p\u003e \u003cp\u003eClosing Off Melting-Point Tubes 76\u003c\/p\u003e \u003cp\u003eMelting-Point Hints 77\u003c\/p\u003e \u003cp\u003eThe Mel-Temp Apparatus 77\u003c\/p\u003e \u003cp\u003eOperation of the Mel-Temp Apparatus 79\u003c\/p\u003e \u003cp\u003eThe SRS DigiMelt 80\u003c\/p\u003e \u003cp\u003eThe Fisher-Johns Apparatus 82\u003c\/p\u003e \u003cp\u003eOperation of the Fisher-Johns Apparatus 83\u003c\/p\u003e \u003cp\u003eThe Thomas-Hoover Apparatus 84\u003c\/p\u003e \u003cp\u003eOperation of the Thomas-Hoover Apparatus 85\u003c\/p\u003e \u003cp\u003eUsing the Thiele Tube 88\u003c\/p\u003e \u003cp\u003eCleaning the Tube 89\u003c\/p\u003e \u003cp\u003eGetting the Sample Ready 89\u003c\/p\u003e \u003cp\u003eDunking the Melting-Point Tube 90\u003c\/p\u003e \u003cp\u003eHeating the Sample 91\u003c\/p\u003e \u003cp\u003eExercises 91\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 13 Recrystallization 92\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eFinding a Good Solvent 93\u003c\/p\u003e \u003cp\u003eGeneral Guidelines for a Recrystallization 94\u003c\/p\u003e \u003cp\u003eMy Product Disappeared 95\u003c\/p\u003e \u003cp\u003eGravity Filtration 95\u003c\/p\u003e \u003cp\u003eThe Buchner Funnel and Filter Flask 97\u003c\/p\u003e \u003cp\u003eJust a Note 100\u003c\/p\u003e \u003cp\u003eThe Hirsch Funnel and Friends 101\u003c\/p\u003e \u003cp\u003eActivated Charcoal 101\u003c\/p\u003e \u003cp\u003eThe Water Aspirator: A Vacuum Source 102\u003c\/p\u003e \u003cp\u003eThe Water Trap 102\u003c\/p\u003e \u003cp\u003eWorking with a Mixed-Solvent System—The Good Part 103\u003c\/p\u003e \u003cp\u003eThe Ethanol—Water System 103\u003c\/p\u003e \u003cp\u003eA Mixed-Solvent System—The Bad Part 104\u003c\/p\u003e \u003cp\u003eSalting Out 105\u003c\/p\u003e \u003cp\u003eWorld-Famous Fan-Folded Fluted Paper 105\u003c\/p\u003e \u003cp\u003eExercises 107\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 14 Recrystallization: Microscale 108\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eIsolating the Crystals 109\u003c\/p\u003e \u003cp\u003eCraig Tube Filtration 109\u003c\/p\u003e \u003cp\u003eCentrifuging the Craig Tube 113\u003c\/p\u003e \u003cp\u003eGetting the Crystals Out 113\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 15 Extraction and Washing 114\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eNever-Ever Land 115\u003c\/p\u003e \u003cp\u003eStarting an Extraction 115\u003c\/p\u003e \u003cp\u003eDutch Uncle Advice 116\u003c\/p\u003e \u003cp\u003eThe Separatory Funnel 117\u003c\/p\u003e \u003cp\u003eThe Stopper 117\u003c\/p\u003e \u003cp\u003eThe Teflon Stopcock 118\u003c\/p\u003e \u003cp\u003eHow to Extract and Wash What 119\u003c\/p\u003e \u003cp\u003eThe Road to Recovery—Back-Extraction 120\u003c\/p\u003e \u003cp\u003eA Sample Extraction 121\u003c\/p\u003e \u003cp\u003ePerforming an Extraction or Washing 123\u003c\/p\u003e \u003cp\u003eExtraction Hints 124\u003c\/p\u003e \u003cp\u003eTheory of Extraction 125\u003c\/p\u003e \u003cp\u003eExercises 127\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 16 Extraction and Washing: Microscale 128\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eMixing 128\u003c\/p\u003e \u003cp\u003eSeparation: Removing the Bottom Layer 128\u003c\/p\u003e \u003cp\u003eSeparation: Removing the Top Layer 129\u003c\/p\u003e \u003cp\u003eSeparation: Removing \u003ci\u003eBoth \u003c\/i\u003eLayers 130\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 17 Sources of Heat 131\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eBoiling Stones 131\u003c\/p\u003e \u003cp\u003eThe Steam Bath 132\u003c\/p\u003e \u003cp\u003eThe Bunsen Burner 133\u003c\/p\u003e \u003cp\u003eBurner Hints 134\u003c\/p\u003e \u003cp\u003eThe Heating Mantle 135\u003c\/p\u003e \u003cp\u003eProportional Heaters and Stepless Controllers 137\u003c\/p\u003e \u003cp\u003eExercise 139\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 18 Clamps and Clamping 140\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eClamping a Distillation Setup 142\u003c\/p\u003e \u003cp\u003eClipping a Distillation Setup 147\u003c\/p\u003e \u003cp\u003eCHAPTER 19 \u003ci\u003eDistillation \u003c\/i\u003e150\u003c\/p\u003e \u003cp\u003eDistillation Notes 151\u003c\/p\u003e \u003cp\u003eClass 1: Simple Distillation 151\u003c\/p\u003e \u003cp\u003eSources of Heat 151\u003c\/p\u003e \u003cp\u003eThe Three-Way Adapter 152\u003c\/p\u003e \u003cp\u003eThe Distilling Flask 152\u003c\/p\u003e \u003cp\u003eThe Thermometer Adapter 153\u003c\/p\u003e \u003cp\u003eThe Ubiquitous Clamp 153\u003c\/p\u003e \u003cp\u003eThe Thermometer 154\u003c\/p\u003e \u003cp\u003eThe Condenser 154\u003c\/p\u003e \u003cp\u003eThe Vacuum Adapter 154\u003c\/p\u003e \u003cp\u003eThe Receiving Flask 154\u003c\/p\u003e \u003cp\u003eThe Ice Bath 154\u003c\/p\u003e \u003cp\u003eThe Distillation Example 155\u003c\/p\u003e \u003cp\u003eThe Distillation Mistake 155\u003c\/p\u003e \u003cp\u003eClass 2: Vacuum Distillation 156\u003c\/p\u003e \u003cp\u003ePressure Measurement 157\u003c\/p\u003e \u003cp\u003eManometer Hints 158\u003c\/p\u003e \u003cp\u003eLeaks 158\u003c\/p\u003e \u003cp\u003ePressure and Temperature Corrections 159\u003c\/p\u003e \u003cp\u003eVacuum Distillation Notes 162\u003c\/p\u003e \u003cp\u003eClass 3: Fractional Distillation 164\u003c\/p\u003e \u003cp\u003eHow This Works 164\u003c\/p\u003e \u003cp\u003eFractional Distillation Notes 167\u003c\/p\u003e \u003cp\u003eAzeotropes 168\u003c\/p\u003e \u003cp\u003eClass 4: Steam Distillation 168\u003c\/p\u003e \u003cp\u003eExternal Steam Distillation 168\u003c\/p\u003e \u003cp\u003eInternal Steam Distillation 170\u003c\/p\u003e \u003cp\u003eSteam Distillation Notes 171\u003c\/p\u003e \u003cp\u003eSimulated Bulb-to-Bulb Distillation: Fakelrohr 172\u003c\/p\u003e \u003cp\u003eExercises 173\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 20 Microscale Distillation 175\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eLike the Big Guy 175\u003c\/p\u003e \u003cp\u003eClass 1: Simple Distillation 175\u003c\/p\u003e \u003cp\u003eClass 2: Vacuum Distillation 175\u003c\/p\u003e \u003cp\u003eClass 3: Fractional Distillation 176\u003c\/p\u003e \u003cp\u003eClass 4: Steam Distillation 176\u003c\/p\u003e \u003cp\u003eMicroscale Distillation II: The Hickman Still 176\u003c\/p\u003e \u003cp\u003eThe Hickman Still Setup 176\u003c\/p\u003e \u003cp\u003eHickman Still Heating 177\u003c\/p\u003e \u003cp\u003eRecovering Your Product 178\u003c\/p\u003e \u003cp\u003eA Port in a Storm 178\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 21 The Rotary Evaporator 179\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eExercises 182\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 22 Reflux and Addition 183\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eStandard Reflux 183\u003c\/p\u003e \u003cp\u003eA Dry Reflux 185\u003c\/p\u003e \u003cp\u003eAddition and Reflux 186\u003c\/p\u003e \u003cp\u003eFunnel Fun 186\u003c\/p\u003e \u003cp\u003eHow to Set Up 188\u003c\/p\u003e \u003cp\u003eExercise 189\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 23 Reflux: Microscale 190\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eAddition and Reflux: Microscale 190\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 24 Sublimation 192\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 25 Microscale Boiling Point 195\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eMicroscale Boiling Point 195\u003c\/p\u003e \u003cp\u003eUltramicroscale Boiling Point 197\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 26 Chromatography: Some Generalities 199\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eAdsorbents 199\u003c\/p\u003e \u003cp\u003eSeparation or Development 200\u003c\/p\u003e \u003cp\u003eThe Eluatropic Series 200\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 27 Thin-Layer Chromatography: TLC 202\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eWe Don’t Make Our Own TLC Plates Any More, But… 202\u003c\/p\u003e \u003cp\u003ePre-prepared TLC Plates 203\u003c\/p\u003e \u003cp\u003eThe Plate Spotter 203\u003c\/p\u003e \u003cp\u003eSpotting the Plates 204\u003c\/p\u003e \u003cp\u003eDeveloping a Plate 205\u003c\/p\u003e \u003cp\u003eVisualization 206\u003c\/p\u003e \u003cp\u003eInterpretation 207\u003c\/p\u003e \u003cp\u003eMultiple Spotting 209\u003c\/p\u003e \u003cp\u003eCospotting 210\u003c\/p\u003e \u003cp\u003eOther TLC Problems 210\u003c\/p\u003e \u003cp\u003ePreparative TLC 212\u003c\/p\u003e \u003cp\u003eExercises 212\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 28 Wet-Column Chromatography 214\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003ePreparing the Column 214\u003c\/p\u003e \u003cp\u003eCompounds on the Column 216\u003c\/p\u003e \u003cp\u003eVisualization and Collection 217\u003c\/p\u003e \u003cp\u003eWet-Column Chromatography: Microscale 218\u003c\/p\u003e \u003cp\u003eFlash Chromatography 219\u003c\/p\u003e \u003cp\u003eMicroscale Flash Chromatography 220\u003c\/p\u003e \u003cp\u003eExercises 221\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 29 Refractometry 222\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eThe Abbé Refractometer 223\u003c\/p\u003e \u003cp\u003eBefore Using the Abbé Refractometer: A Little Practice 224\u003c\/p\u003e \u003cp\u003eUsing the Abbé Refractometer 225\u003c\/p\u003e \u003cp\u003eRefractometry Hints 226\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 30 Gas Chromatography 227\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eThe Mobile Phase: Gas 227\u003c\/p\u003e \u003cp\u003eGC Sample Preparation 228\u003c\/p\u003e \u003cp\u003eGC Sample Introduction 228\u003c\/p\u003e \u003cp\u003eSample in the Column 230\u003c\/p\u003e \u003cp\u003eSample at the Detector 231\u003c\/p\u003e \u003cp\u003eElectronic Interlude 232\u003c\/p\u003e \u003cp\u003eSample on the Computer 233\u003c\/p\u003e \u003cp\u003eParameters, Parameters 234\u003c\/p\u003e \u003cp\u003eGas Flow Rate 234\u003c\/p\u003e \u003cp\u003eTemperature 234\u003c\/p\u003e \u003cp\u003eExercises 235\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 31 HP Liquid Chromatography 236\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eThe Mobile Phase: Liquid 237\u003c\/p\u003e \u003cp\u003eA Bubble Trap 238\u003c\/p\u003e \u003cp\u003eThe Pump and Pulse Dampener Module 239\u003c\/p\u003e \u003cp\u003eHPLC Sample Preparation 239\u003c\/p\u003e \u003cp\u003eHPLC Sample Introduction 241\u003c\/p\u003e \u003cp\u003eSample in the Column 242\u003c\/p\u003e \u003cp\u003eSample at the Detector 242\u003c\/p\u003e \u003cp\u003eSample on the Computer 243\u003c\/p\u003e \u003cp\u003eParameters, Parameters 243\u003c\/p\u003e \u003cp\u003eEluent Flow Rate 244\u003c\/p\u003e \u003cp\u003eTemperature 244\u003c\/p\u003e \u003cp\u003eEluent Composition 244\u003c\/p\u003e \u003cp\u003eExercises 244\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 32 Infrared Spectroscopy (and a bit of uv-vis, too ) 245\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eMolecules As Balls On Springs 245\u003c\/p\u003e \u003cp\u003eAh, Quantum Mechanics 247\u003c\/p\u003e \u003cp\u003eThe Dissonant Oscillator 247\u003c\/p\u003e \u003cp\u003eBut Wait! There’s More 248\u003c\/p\u003e \u003cp\u003eMore Complicated Molecules 248\u003c\/p\u003e \u003cp\u003eCorrelation Tables to the Rescue 250\u003c\/p\u003e \u003cp\u003eTroughs and Reciprocal Centimeters 254\u003c\/p\u003e \u003cp\u003eSome Functional Group Analysis 254\u003c\/p\u003e \u003cp\u003eA Systematic Interpretation 256\u003c\/p\u003e \u003cp\u003eInfrared Sample Preparation 258\u003c\/p\u003e \u003cp\u003eLiquid Samples 258\u003c\/p\u003e \u003cp\u003eSolid Samples 259\u003c\/p\u003e \u003cp\u003eRunning the Spectrum 262\u003c\/p\u003e \u003cp\u003eInterpreting IR Spectra—Finishing Touches 263\u003c\/p\u003e \u003cp\u003eThe Fourier Transform Infrared (FTIR) 264\u003c\/p\u003e \u003cp\u003eThe Optical System 264\u003c\/p\u003e \u003cp\u003eA Reflectance Attachment: Something to Think About 268\u003c\/p\u003e \u003cp\u003eAnd UV-VIS Too! 268\u003c\/p\u003e \u003cp\u003eElectrons Get to Jump 268\u003c\/p\u003e \u003cp\u003eInstrument Configuration 269\u003c\/p\u003e \u003cp\u003eSource 270\u003c\/p\u003e \u003cp\u003eSample (and Reference) Cells 270\u003c\/p\u003e \u003cp\u003eSolvents 270\u003c\/p\u003e \u003cp\u003eExercises 271\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 32 On The Dual -Beam Infra-Red Instrument (ONLINE)1\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eThe Perkin-Elmer 710B IR 2\u003c\/p\u003e \u003cp\u003eUsing the Perkin-Elmer 710B 4\u003c\/p\u003e \u003cp\u003eThe 100% Control: An Important Aside 5\u003c\/p\u003e \u003cp\u003eCalibration of the Spectrum 6\u003c\/p\u003e \u003cp\u003eIR Spectra: The Finishing Touches 7\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 33 Nuclear Magnetic Resonance 272\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eNuclei Have Spin, Too 272\u003c\/p\u003e \u003cp\u003eThe Magnetic Catch 273\u003c\/p\u003e \u003cp\u003eEverybody Line Up, Flip, and Relax 273\u003c\/p\u003e \u003cp\u003eA More Sensitive Census 274\u003c\/p\u003e \u003cp\u003eThe Chemical Shift 274\u003c\/p\u003e \u003cp\u003eT For One and Two 275\u003c\/p\u003e \u003cp\u003eBe It Better Resolved... 275\u003c\/p\u003e \u003cp\u003eIncredibly Basic Ft-Nmr 276\u003c\/p\u003e \u003cp\u003eNmr Sample Preparation 276\u003c\/p\u003e \u003cp\u003eSome Nmr Terms and Interpretations 280\u003c\/p\u003e \u003cp\u003eThe Chemical Shift and Tms Zero 280\u003c\/p\u003e \u003cp\u003eIntegration and Labeling 282\u003c\/p\u003e \u003cp\u003eThreaded Interpretations: Spectrum #1 (\u003ci\u003et\u003c\/i\u003e-butyl alcohol) 283\u003c\/p\u003e \u003cp\u003eThreaded Interpretations: Spectrum #2 (Toluene) and Spectrum #3 (\u003ci\u003ep\u003c\/i\u003e-Dichlorobenzene) 283\u003c\/p\u003e \u003cp\u003eThreaded Interpretations: Spectrum #4 (Ethylbenzene) and Spectrum #5 (A Double Resonance Experiment) 285\u003c\/p\u003e \u003cp\u003eUse a Correlation Chart 288\u003c\/p\u003e \u003cp\u003eExercises 290\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter 34 Theory of Distillation (Online) 1\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eClass 1: Simple Distillation 1\u003c\/p\u003e \u003cp\u003eClausius and Clapeyron 3\u003c\/p\u003e \u003cp\u003eClass 3: Fractional Distillation 5\u003c\/p\u003e \u003cp\u003eA Hint from Dalton 5\u003c\/p\u003e \u003cp\u003eDalton and Raoult 5\u003c\/p\u003e \u003cp\u003eA Little Algebra 6\u003c\/p\u003e \u003cp\u003eClausius and Clapeyron Meet Dalton and Raoult 7\u003c\/p\u003e \u003cp\u003eDalton Again 8\u003c\/p\u003e \u003cp\u003eWhat Does It All Mean? 10\u003c\/p\u003e \u003cp\u003eReality Intrudes I: Changing Composition 12\u003c\/p\u003e \u003cp\u003eReality Intrudes II: Nonequilibrium Conditions 12\u003c\/p\u003e \u003cp\u003eReality Intrudes III: Azeotropes 13\u003c\/p\u003e \u003cp\u003eOther Deviations 16\u003c\/p\u003e \u003cp\u003eClass 4: Steam Distillation 16\u003c\/p\u003e \u003cp\u003eIndex 291\u003c\/p\u003e","brand":"John Wiley \u0026 Sons Inc","offers":[{"title":"Default Title","offer_id":48866405450071,"sku":"9781119608554","price":56.85,"currency_code":"GBP","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0817\/1739\/5799\/files\/9781119608554.jpg?v=1722278490","url":"https:\/\/bookcurl.com\/products\/the-organic-chem-lab-survival-manual-9781119608554","provider":"Book Curl","version":"1.0","type":"link"}