{"product_id":"organic-syntheses-volume-96-9781119707769","title":"Organic Syntheses Volume 96","description":"\u003cb\u003eBook Synopsis\u003c\/b\u003e\u003cbr\u003eThe current volume continues the tradition of the Organic Syntheses series, providing carefully checked and edited experimental procedures that describe important synthetic methods, transformations, reagents, and synthetic building blocks or intermediates with demonstrated utility in organic synthesis. These significant and interesting procedures should prove worthwhile to many synthetic chemists working in increasingly diverse areas. A trusted guide for professionals in organic and medicinal chemistry in academia, government, and industries, including pharmaceuticals, fine chemicals, agrochemicals, and biotechnological products.\u003cbr\u003e\u003cbr\u003e\u003cb\u003eTable of Contents\u003c\/b\u003e\u003cbr\u003e\u003cp\u003eDiscussion Addendum for: 4-Nonylbenzoic Acid 1\u003cbr\u003e\u003ci\u003eAlois Fürstner\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eLate-Stage Deoxyfluorination of Phenols with PhenoFluorMix 16\u003cbr\u003e\u003ci\u003eJunting Chen and Tobias Ritter\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eNickel-Catalyzed Cross-Coupling of 2-Methoxynaphthalene with Methyl 4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzoate 36\u003cbr\u003e\u003ci\u003eYuki Kawashima, Takayuki Furukawa, Naoto Chatani and Mamoru Tobisu\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eDiscussion Addendum for: Lithium Amides as Homochiral Ammonia Equivalents for Conjugate Additions to α,β-Unsaturated Esters: Asymmetric Synthesis of (\u003ci\u003eS\u003c\/i\u003e)-β-Leucine 53\u003cbr\u003e\u003ci\u003eStephen G. Davies, Ai M. Fletcher, Paul M. Roberts, and James E. Thomson\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eSynthesis of 2,3-Diaryl-2\u003ci\u003eH\u003c\/i\u003e-azirines via Cs2CO3-Mediated Cyclization of Ketoxime Acetates 66\u003cbr\u003e\u003ci\u003eMi-Na Zhao and Zheng-Hui Guan\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eDiscussion Addendum for: The Direct Acyl-Alkylation of Arynes. Preparation of Methyl 2- (2-acetylphenyl)acetate 80\u003cbr\u003e\u003ci\u003eAustin C. Wright and Brian M. Stoltz\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eDiscussion Addendum for: Convenient Preparation of 3-Ethoxycarbonyl Benzofurans from Salicylaldehydes and Ethyl Diazoacetate 98\u003cbr\u003e\u003ci\u003eMizzanoor Rahaman and M. Mahmun Hossain\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eDiscussion Addendum for: Phosphine-Catalyzed [4 + 2] Annulation: Synthesis of Ethyl 6-Phenyl-1-tosyl-1,2,5,6-tetrahydropyridine-3-carboxylate 110\u003cbr\u003e\u003ci\u003eAslam C. Shaikh and Ohyun Kwon\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eDiscussion Addendum for: Protection of Alcohols using 2-Benzyloxy-1-methylpyridinium Trifluoromethanesulfonate: Methyl (\u003ci\u003eR\u003c\/i\u003e)-(-)-3-Benzyloxy-2-methyl Propanoate 124\u003cbr\u003e\u003ci\u003eHarvey F. Fulo, Philip A. Albiniak, and Gregory B. Dudley\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eSynthesis of 4-Methylbenzoate(2′,4′,6′-trimethoxy-phenyl)iodonium Tosylate 137\u003cbr\u003e\u003ci\u003eThomas L. Seidl, Aaron Moment, Charles Orella, Thomas Vickery, and David R. Stuart\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eGold-Catalyzed Oxidative Coupling of Arenes and Arylsilanes 150\u003cbr\u003e\u003ci\u003eChris Nottingham, Verity Barber, and Guy C. Lloyd-Jones\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eDiscussion Addendum for: Preparation of Enantioenriched Homoallylic Primary Amines 179\u003cbr\u003e\u003ci\u003eMiguel Yus\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eDiscussion Addendum for: Synthesis of Ynamides by Copper-Mediated Coupling of 1,1-Dibromo-1-alkenes with Nitrogen Nucleophiles. Preparation of 4-Methyl-\u003ci\u003eN\u003c\/i\u003e-(2-phenylethynyl)-\u003ci\u003eN\u003c\/i\u003e-(phenylmethyl)benzenesulfonamide 195\u003cbr\u003e\u003ci\u003eCédric Theunissen, Pierre Thilmany, Mounsef Lahboubi, Nicolas Blanchard, and Gwilherm Evano\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eDiscussion Addendum for: Phosphine-Catalyzed [3 + 2] Annulation: Synthesis of Ethyl 5-(\u003ci\u003etert\u003c\/i\u003e-Butyl)-2-phenyl-1-tosyl-3-pyrroline-3-carboxylate 214\u003cbr\u003e\u003ci\u003eAslam C. Shaikh and Ohuyn Kwon\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eDiscussion Addendum for: Synthesis of Highly Enantiomerically Enriched Amines by Asymmetric Transfer Hydrogenation of \u003ci\u003eN\u003c\/i\u003e-(\u003ci\u003etert\u003c\/i\u003e-Butylsulfinyl) Imines 232\u003cbr\u003e\u003ci\u003eMiguel Yus\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eSynthesis of Chiral Diamine Ligands for Nickel-catalyzed Asymmetric Cross-couplings of Alkylchloroboronate Esters with Alkylzincs: 1R,2R)-\u003ci\u003eN\u003c\/i\u003e,\u003ci\u003eN\u003c\/i\u003e\u003ci\u003e’\u003c\/i\u003e-Dimethyl-1,2-bis(2-methylphenyl)-1,2-diaminoethane 245\u003cbr\u003e\u003ci\u003eYusuke Masuda and Gregory C. Fu\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003ePreparation of 5-(Triisopropylalkynyl) dibenzo[\u003ci\u003eb\u003c\/i\u003e,\u003ci\u003ed\u003c\/i\u003e] thiophenium triflate 258\u003cbr\u003e\u003ci\u003eBernd Waldecker, Kevin Kafuta, and Manuel Alcarazo\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eThree-Step Synthesis of 2-(Diiodomethyl)-4,4,5,5-tetramethyl- 1,3,2-dioxaborolane from Dichloromethane 277\u003cbr\u003e\u003ci\u003eMorgane Sayes, Guillaume Benoit, and André B. Charette\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eDiscussion Addendum for: Allylic Oxidation Catalyzed by Dirhodium(II) Tetrakis[ε-caprolactamate] of tert-Butyldimethylsilylprotected \u003ci\u003etrans\u003c\/i\u003e-Dehydroandrosterone 300\u003cbr\u003e\u003ci\u003eYong-Liang Su, Luca De Angelis and Michael P. Doyle\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003ePreparation of (\u003ci\u003eR\u003c\/i\u003e)-3-(3,5-Bistrifluoromethylphenyl)-1,1’-bi-2-naphthol 312\u003cbr\u003e\u003ci\u003eYusuke Kobayashi, Atsushi Matsuda, Tomoya Ushimaru, and Toshiro Harada\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eCatalytic Enantioselective Addition of an In-Situ Prepared Aryltitanium Reagent to \u003ci\u003ep\u003c\/i\u003e-Chloroacetophenone: (R)-(+)-1-(4-Chlorophenyl)-1-\u003ci\u003em\u003c\/i\u003e-tolylethanol 333\u003cbr\u003e\u003ci\u003eYusuke Kobayashi, Atsushi Matsuda, Tomoya Ushimaru, and Toshiro Harada\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eStereoselective Synthesis of (\u003ci\u003eR\u003c\/i\u003e)-((\u003ci\u003eR\u003c\/i\u003e)-1-Phenyl-2,2,2-trichloroethyl)-2-(2-bromophenyl)aziridine-1-carboxylate 351\u003cbr\u003e\u003ci\u003eHélène Lebel and Henri Piras\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eDiscussion Addendum for: Preparation of (\u003ci\u003eR\u003c\/i\u003e,\u003ci\u003eR\u003c\/i\u003e)-1,2:4,5-Diepoxypentane 361\u003cbr\u003e\u003ci\u003eNicholas Sizemore and Scott D. Rychnovsky\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e(\u003ci\u003eR\u003c\/i\u003e)-\u003ci\u003eN\u003c\/i\u003e,\u003ci\u003eN\u003c\/i\u003e’-Dimethyl-1,1’-binaphthyldiamine 382\u003cbr\u003e\u003ci\u003eScott E. Denmark and Pavel Ryabchuk\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003ePreparation of a Diisopropylselenophosphoramide Catalyst and its Use in Enantioselective Sulfenoetherification 400\u003cbr\u003e\u003ci\u003eScott E. Denmark, Pavel Ryabchuk, Hyung Min Chi, and Anastassia Matviitsuk\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003ea\u003ci\u003enti\u003c\/i\u003e-1,2,2,3,4,4-Hexamethylphosphetane 1-Oxide 418\u003cbr\u003e\u003ci\u003eTrevor V. Nykaza, Julian C. Cooper, and Alexander T. Radosevich\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eFacile Reduction of Amides Using Nickel Catalysis: Reduction of 12-Aminododecanolactam 436\u003cbr\u003e\u003ci\u003eBryan J. Simmons, Melissa Ramirez, and Neil K. Garg\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003ePreparation of 2,4,5,6-Tetra(9H-carbazol-9-yl)isophthalonitrile 455\u003cbr\u003e\u003ci\u003eSaskia M. Engle, Takisha R. Kirkner, and Christopher B. Kelly\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eDiscussion Addendum for: Fluorobis(phenylsulfonyl)methane (FBSM) 474\u003cbr\u003e\u003ci\u003eXanath Ispizua-Rodriguez, Vinayak Krishnamurti, Mathew Coe, and G. K. Surya Prakash\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eSynthesis of 5-Hydroxy-4-methoxy-2-methylpyrylium Trifluoromethanesulfonate from Kojic Acid 494\u003cbr\u003e\u003ci\u003eNana B. Agyemang and Ryan P. Murelli\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eIridium-Catalyzed Reductive Coupling of Grignard Reagents and Tertiary Amides 511\u003cbr\u003e\u003ci\u003ePablo Gabriel, Lan-Gui Xie, and Darren J. Dixon\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eSynthesis of Chiral Tetramic Acids: Preparation of (\u003ci\u003eS\u003c\/i\u003e)-5-Benzylpyrrolidine-2,4-dione from L-Phenylalanine Methyl Ester Hydrochloride 528\u003cbr\u003e\u003ci\u003eKyle M. Lambert, Austin W. Medley, Amy C. Jackson, Lauren E. Markham, and John L. Wood\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003eSynthesis of 8-Hydroxygeraniol 586\u003cbr\u003e\u003ci\u003eFrancesca M. Ippoliti, Joyann S. Barber, and Neil K. Garg\u003c\/i\u003e\u003c\/p\u003e","brand":"John Wiley \u0026 Sons Inc","offers":[{"title":"Default Title","offer_id":49407126667607,"sku":"9781119707769","price":139.45,"currency_code":"GBP","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0817\/1739\/5799\/files\/9781119707769.jpg?v=1730498272","url":"https:\/\/bookcurl.com\/products\/organic-syntheses-volume-96-9781119707769","provider":"Book Curl","version":"1.0","type":"link"}