{"product_id":"nuclear-magnetic-resonance-spectroscopy-9781119295235","title":"Nuclear Magnetic Resonance Spectroscopy","description":"\u003cb\u003eBook Synopsis\u003c\/b\u003e\u003cbr\u003e\u003cp\u003e\u003cb\u003eCombines clear and concise discussions of key NMR concepts with succinct and illustrative examples\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eDesigned to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more.\u003c\/p\u003e \u003cp\u003e\u003ci\u003eNuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition\u003c\/i\u003e begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology t\u003cbr\u003e\u003cbr\u003e\u003cb\u003eTable of Contents\u003c\/b\u003e\u003cbr\u003e\u003c\/p\u003e\u003cp\u003ePreface to First Edition\u003c\/p\u003e \u003cp\u003ePreface to Second Edition\u003c\/p\u003e \u003cp\u003eSymbols\u003c\/p\u003e \u003cp\u003eAbbreviations\u003c\/p\u003e \u003cp\u003e\u003cb\u003e1. Introduction\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e1.1. Magnetic Properties of Nuclei\u003c\/p\u003e \u003cp\u003e1.2. The Chemical Shift\u003c\/p\u003e \u003cp\u003e1.3. Excitation and Relaxation\u003c\/p\u003e \u003cp\u003e1.4. Pulsed Experiments\u003c\/p\u003e \u003cp\u003e1.5. The Coupling Constant\u003c\/p\u003e \u003cp\u003e1.6. Quantitation and Complex Splitting\u003c\/p\u003e \u003cp\u003e1.7. Commonly Studied Nuclides\u003c\/p\u003e \u003cp\u003e1.8. Dynamic Effects\u003c\/p\u003e \u003cp\u003e1.9. Spectra of Solids\u003c\/p\u003e \u003cp\u003eProblems\u003c\/p\u003e \u003cp\u003eTips on Solving NMR Problems\u003c\/p\u003e \u003cp\u003eBibliography\u003c\/p\u003e \u003cp\u003e\u003cb\u003e2. Introductory Experimental Methods\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e2.1. The Spectrometer\u003c\/p\u003e \u003cp\u003e2.2. Sample Preparation\u003c\/p\u003e \u003cp\u003e2.3. Optimizing the Signal\u003c\/p\u003e \u003cp\u003e2.3a. Sample Tube Placement\u003c\/p\u003e \u003cp\u003e2.3b. Probe Tuning\u003c\/p\u003e \u003cp\u003e2.3c. Field\/Frequency Locking\u003c\/p\u003e \u003cp\u003e2.3d. Spectrometer Shimming\u003c\/p\u003e \u003cp\u003e2.4. Determination of NMR Spectra-Acquisition Parameters\u003c\/p\u003e \u003cp\u003e2.4a. Number of Data Points\u003c\/p\u003e \u003cp\u003e2.4b. Spectral Width\u003c\/p\u003e \u003cp\u003e2.4c. Filter Bandwidth\u003c\/p\u003e \u003cp\u003e2.4d. Acquisition Time\u003c\/p\u003e \u003cp\u003e2.4e. Transmitter Offset\u003c\/p\u003e \u003cp\u003e2.4f. Flip Angle\u003c\/p\u003e \u003cp\u003e2.4g. Receiver Gain\u003c\/p\u003e \u003cp\u003e2.4h. Number of Scans\u003c\/p\u003e \u003cp\u003e2.4i. Steady-State Scans\u003c\/p\u003e \u003cp\u003e2.4j. Oversampling and Digital Filtration\u003c\/p\u003e \u003cp\u003e2.4k. Decoupling for X Nuclei\u003c\/p\u003e \u003cp\u003e2.4l. Typical NMR Experiments\u003c\/p\u003e \u003cp\u003e2.5. Determination of NMR Spectral-Processing Parameters\u003c\/p\u003e \u003cp\u003e2.5a. Exponential Weighting\u003c\/p\u003e \u003cp\u003e2.5b. Zero Filling\u003c\/p\u003e \u003cp\u003e2.5c. FID Truncation and Spectral Artifacts\u003c\/p\u003e \u003cp\u003e2.5d. Resolution\u003c\/p\u003e \u003cp\u003e2.6. Determination of NMR Spectra:  Spectral Presentation\u003c\/p\u003e \u003cp\u003e2.6a. Signal Phasing and Baseline Correction\u003c\/p\u003e \u003cp\u003e2.6b. Zero Referencing\u003c\/p\u003e \u003cp\u003e2.6c. Determination of Certain NMR Parameters\u003c\/p\u003e \u003cp\u003e2.7. Calibrations\u003c\/p\u003e \u003cp\u003e2.7a. Pulse Width (Flip Angle)\u003c\/p\u003e \u003cp\u003e2.8b. Decoupler Field Strength\u003c\/p\u003e \u003cp\u003eProblems\u003c\/p\u003e \u003cp\u003eBibliography\u003c\/p\u003e \u003cp\u003e\u003cb\u003e3. The Chemical Shift\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e3.1. Factors That Influence Proton Shifts\u003c\/p\u003e \u003cp\u003e3.2. Proton Chemical Shifts and Structure\u003c\/p\u003e \u003cp\u003e3.2a. Saturated Aliphatics\u003c\/p\u003e \u003cp\u003e3.2b. Unsaturated Aliphatics\u003c\/p\u003e \u003cp\u003e3.2c. Aromatics\u003c\/p\u003e \u003cp\u003e3.2d. Protons on Oxygen and Nitrogen\u003c\/p\u003e \u003cp\u003e3.2e. Programs for Empirical Calculations\u003c\/p\u003e \u003cp\u003e3.3. Medium and Isotope Effects\u003c\/p\u003e \u003cp\u003e3.4. Factors That Influence Carbon Shifts\u003c\/p\u003e \u003cp\u003e3.5. Carbon Chemical Shifts and Structure\u003c\/p\u003e \u003cp\u003e3.5a. Saturated Aliphatics\u003c\/p\u003e \u003cp\u003e3.5b. Unsaturated Compounds\u003c\/p\u003e \u003cp\u003e3.5c. Carbonyl Groups\u003c\/p\u003e \u003cp\u003e3.5d. Programs for Empirical Calculation\u003c\/p\u003e \u003cp\u003e3.6. Tables of Chemical Shifts\u003c\/p\u003e \u003cp\u003eProblems\u003c\/p\u003e \u003cp\u003eFurther Tips on Solving NMR Problems\u003c\/p\u003e \u003cp\u003eBibliography\u003c\/p\u003e \u003cp\u003e\u003cb\u003e4. The Coupling Constant\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e4.1. First- and Second-Order Effects\u003c\/p\u003e \u003cp\u003e4.2. Chemical and Magnetic Equivalence\u003c\/p\u003e \u003cp\u003e4.3. Signs and Mechanisms of Coupling\u003c\/p\u003e \u003cp\u003e4.4. Couplings over One Bond\u003c\/p\u003e \u003cp\u003e4.5. Geminal Couplings\u003c\/p\u003e \u003cp\u003e4.6. Vicinal Couplings\u003c\/p\u003e \u003cp\u003e4.7. Long-Range Couplings\u003c\/p\u003e \u003cp\u003e4.8. Spectral Analysis\u003c\/p\u003e \u003cp\u003e4.9. Tables of Coupling Constants\u003c\/p\u003e \u003cp\u003eProblems\u003c\/p\u003e \u003cp\u003eBibliography\u003c\/p\u003e \u003cp\u003e\u003cb\u003e5. Further Topics in One-Dimensional NMR Spectroscopy\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e5.1. Spin-Lattice and Spin-Spin Relaxation\u003c\/p\u003e \u003cp\u003e5.2. Reactions on the NMR Time Scale\u003c\/p\u003e \u003cp\u003e5.3. Multiple Resonance\u003c\/p\u003e \u003cp\u003e5.4. The Nuclear Overhauser Effect\u003c\/p\u003e \u003cp\u003e5.5. Spectral Editing\u003c\/p\u003e \u003cp\u003e5.6. Sensitivity Enhancement\u003c\/p\u003e \u003cp\u003e5.7. Carbon Connectivity\u003c\/p\u003e \u003cp\u003e5.8. Phase Cycling, Composite Pulses, and Shaped Pulses\u003c\/p\u003e \u003cp\u003eProblems\u003c\/p\u003e \u003cp\u003eBibliography\u003c\/p\u003e \u003cp\u003e\u003cb\u003e6. Two-Dimensional NMR Spectroscopy\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e6.1. Proton-Proton Correlation Through \u003ci\u003eJ\u003c\/i\u003e Coupling\u003c\/p\u003e \u003cp\u003e6.2. Proton-Heteronucleus Correlation\u003c\/p\u003e \u003cp\u003e6.3. Proton-Proton Correlation Through Space or Chemical Exchange\u003c\/p\u003e \u003cp\u003e6.4. Carbon-Carbon Correlation\u003c\/p\u003e \u003cp\u003e6.5. Higher Dimensions\u003c\/p\u003e \u003cp\u003e6.6. Pulsed Field Gradients\u003c\/p\u003e \u003cp\u003e6.7. Diffusion-Ordered Spectroscopy\u003c\/p\u003e \u003cp\u003e6.7. Summary of Two-Dimensional Methods\u003c\/p\u003e \u003cp\u003eProblems\u003c\/p\u003e \u003cp\u003eBibliography\u003c\/p\u003e \u003cp\u003e\u003cb\u003e7. Advanced Experimental Methods\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003ePart A. One-Dimensional Techniques\u003c\/p\u003e \u003cp\u003e7.1. \u003ci\u003eT\u003c\/i\u003e\u003csub\u003e1\u003c\/sub\u003e Measurements\u003c\/p\u003e \u003cp\u003e7.2. \u003csup\u003e13\u003c\/sup\u003eC Spectral Editing Experiments\u003c\/p\u003e \u003cp\u003e7.2a. The APT Experiment\u003c\/p\u003e \u003cp\u003e7.2b. The DEPT Experiment\u003c\/p\u003e \u003cp\u003e7.3. NOE Experiments\u003c\/p\u003e \u003cp\u003e7.3a. The NOE Difference Experiment\u003c\/p\u003e \u003cp\u003e7.3b. The Double-Pulse, Field-Gradient, Spin-Echo NOE Experiment\u003c\/p\u003e \u003cp\u003ePart B. Two-Dimensional Techniques\u003c\/p\u003e \u003cp\u003e7.4. Two-Dimensional NMR Data-Acquisition Parameters\u003c\/p\u003e \u003cp\u003e7.4a. Number of Data Points\u003c\/p\u003e \u003cp\u003e7.4b. Number of Time Increments\u003c\/p\u003e \u003cp\u003e7.4c. Spectral Widths\u003c\/p\u003e \u003cp\u003e7.4d. Acquisition Time\u003c\/p\u003e \u003cp\u003e7.4e. Transmitter Offset\u003c\/p\u003e \u003cp\u003e7.4f. Flip Angle\u003c\/p\u003e \u003cp\u003e7.4g. Relaxation Delay\u003c\/p\u003e \u003cp\u003e7.4h. Receiver Gain\u003c\/p\u003e \u003cp\u003e7.4i. Number of Scans per Time Increment\u003c\/p\u003e \u003cp\u003e7.4j. Steady-State Scans\u003c\/p\u003e \u003cp\u003e7.5. Two-Dimensional NMR Data-Processing Parameters\u003c\/p\u003e \u003cp\u003e7.5a. Weighting Functions\u003c\/p\u003e \u003cp\u003e7.5b. Zero Filling\u003c\/p\u003e \u003cp\u003e7.5c. Digital Resolution\u003c\/p\u003e \u003cp\u003e7.5d. Linear Prediction\u003c\/p\u003e \u003cp\u003e7.6. Two-Dimensional NMR Data Display\u003c\/p\u003e \u003cp\u003e7.6a. Phasing and Zero Referencing\u003c\/p\u003e \u003cp\u003e7.6b. Symmetrization\u003c\/p\u003e \u003cp\u003e7.6c. Use of Cross Sections in Analysis\u003c\/p\u003e \u003cp\u003ePart C. Two-Dimensional Techniques:  The Experiments\u003c\/p\u003e \u003cp\u003e7.7. Homonuclear Chemical-Shift Correlation Experiments via Scalar Coupling\u003c\/p\u003e \u003cp\u003e7.7a. The COSY Family:  COSY-90°, COSY-45°, Long-Range COSY, and DQF-COSY\u003c\/p\u003e \u003cp\u003e7.7b. The TOCSY Experiment\u003c\/p\u003e \u003cp\u003e7.8. Direct Heteronuclear Chemical-Shift Correlation via Scalar Coupling\u003c\/p\u003e \u003cp\u003e7.8a. The HMQC Experiment\u003c\/p\u003e \u003cp\u003e7.8b. The HSQC Experiment\u003c\/p\u003e \u003cp\u003e7.8c. The HETCOR Experiment\u003c\/p\u003e \u003cp\u003e7.9. Indirect Heteronuclear Chemical-Shift Correlation via Scalar Coupling\u003c\/p\u003e \u003cp\u003e7.9a. The HMBC Experiment\u003c\/p\u003e \u003cp\u003e7.9b. The FLOCK Experiment\u003c\/p\u003e \u003cp\u003e7.9c. The HSQC-TOCSY Experiment\u003c\/p\u003e \u003cp\u003e7.10. Homonuclear Chemical-Shift Correlation via Dipolar Coupling\u003c\/p\u003e \u003cp\u003e7.10a. The NOESY Experiment\u003c\/p\u003e \u003cp\u003e7.10b. The ROESY Experiment\u003c\/p\u003e \u003cp\u003e7.11. 1D and Advanced 2D Experiments\u003c\/p\u003e \u003cp\u003e7.11a. The 1D TOCSY Experiment\u003c\/p\u003e \u003cp\u003e7.11b. The 1D NOESY and ROESY Experiments\u003c\/p\u003e \u003cp\u003e7.11c. The Multiplicity-Edited HSQC Experiment\u003c\/p\u003e \u003cp\u003e7.11d. The H2BC Experiment\u003c\/p\u003e \u003cp\u003e7.11e. Nonuniform Sampling\u003c\/p\u003e \u003cp\u003e7.11f. Pure Shift NMR\u003c\/p\u003e \u003cp\u003e7.11g. Covariance NMR\u003c\/p\u003e \u003cp\u003e7.12. Pure Shift-Covariance NMR\u003c\/p\u003e \u003cp\u003eBibliography\u003c\/p\u003e \u003cp\u003e\u003cb\u003e8. Structural Elucidation:  An Example\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003ePart A. Spectral Analysis\u003c\/p\u003e \u003cp\u003e8.1. \u003csup\u003e1\u003c\/sup\u003eH NMR Data\u003c\/p\u003e \u003cp\u003e8.2. \u003csup\u003e13\u003c\/sup\u003eC NMR Data\u003c\/p\u003e \u003cp\u003e8.3. The DEPT Experiment\u003c\/p\u003e \u003cp\u003e8.4. The HSQC Experiment\u003c\/p\u003e \u003cp\u003e8.5. The COSY Experiment\u003c\/p\u003e \u003cp\u003e8.6. The HMBC Experiment\u003c\/p\u003e \u003cp\u003e8.7. General Molecular Assembly Strategy\u003c\/p\u003e \u003cp\u003e8.8. A Specific Molecular Assembly Procedure\u003c\/p\u003e \u003cp\u003e8.9. The NOESY Experiment\u003c\/p\u003e \u003cp\u003ePart B Computer-Assisted Structure Elucidation\u003c\/p\u003e \u003cp\u003e8.10. CASE Procedures\u003c\/p\u003e \u003cp\u003e8.11. T-2 Toxin\u003c\/p\u003e \u003cp\u003eAppendix 1 Derivation of the NMR Equation\u003c\/p\u003e \u003cp\u003eAppendix 2 The Bloch Equations\u003c\/p\u003e \u003cp\u003eAppendix 3 Quantum Mechanical Treatment of the Two-Spin System\u003c\/p\u003e \u003cp\u003eAppendix 4 Analysis of Second-Order, Three- and Four-Spin Systems by Inspection\u003c\/p\u003e \u003cp\u003eAppendix 5 Relaxation\u003c\/p\u003e \u003cp\u003eAppendix 6 Product-Operator Formalism and Coherence-Level Diagrams\u003c\/p\u003e \u003cp\u003eBibliography\u003c\/p\u003e \u003cp\u003eAppendix 7 Stereochemical Considerations\u003c\/p\u003e \u003cp\u003eA7.1. Homotopic Groups\u003c\/p\u003e \u003cp\u003eA7.2. Enantiotopic Groups\u003c\/p\u003e \u003cp\u003eA7.3. Diastereotopic Groups\u003c\/p\u003e \u003cp\u003eBibliography\u003c\/p\u003e \u003cp\u003eIndex\u003c\/p\u003e","brand":"John Wiley \u0026 Sons Inc","offers":[{"title":"Default Title","offer_id":48866391916887,"sku":"9781119295235","price":67.4,"currency_code":"GBP","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0817\/1739\/5799\/files\/9781119295235.jpg?v=1722278432","url":"https:\/\/bookcurl.com\/products\/nuclear-magnetic-resonance-spectroscopy-9781119295235","provider":"Book Curl","version":"1.0","type":"link"}