{"product_id":"nmr-spectroscopy-basic-principles-concepts-and-applications-in-chemistry-9783527330041","title":"NMR Spectroscopy: Basic Principles, Concepts and Applications in Chemistry","description":"\u003cb\u003eBook Synopsis\u003c\/b\u003e\u003cbr\u003eNuclear magnetic resonance (NMR) spectroscopy is one of the most powerful and widely used techniques in chemical research for investigating structures and dynamics of molecules. Advanced methods can even be utilized for structure determinations of biopolymers, for example proteins or nucleic acids. NMR is also used in medicine for magnetic resonance imaging (MRI). The method is based on spectral lines of different atomic nuclei that are excited when a strong magnetic field and a radiofrequency transmitter are applied. The method is very sensitive to the features of molecular structure because also the neighboring atoms influence the signals from individual nuclei and this is\u003cbr\u003e important for determining the 3D-structure of molecules.\u003cbr\u003e \u003cbr\u003e This new edition of the popular classic has a clear style and a highly practical, mostly non-mathematical approach. Many examples are taken from organic and organometallic chemistry, making this book an invaluable guide to undergraduate and graduate students of organic chemistry, biochemistry, spectroscopy or physical chemistry, and to researchers using this well-established and extremely important technique. Problems and solutions are included.\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cb\u003eTrade Review\u003c\/b\u003e\u003cbr\u003e\u003cp\u003e“Few good textbooks on NMR Spectroscopy are available at either the undergraduate or graduate levels.  For those who want to go beyond elementary organic chemistry but without delving into all the mathematics Friebolin’s book is probably the best among this category.”  (\u003ci\u003eJournal of Chemical Education\u003c\/i\u003e, 5 June 2014)\u003c\/p\u003e\u003cbr\u003e\u003cbr\u003e\u003cb\u003eTable of Contents\u003c\/b\u003e\u003cbr\u003ePREFACE \u003cbr\u003e \u003cbr\u003e INTRODUCTION \u003cbr\u003e Literature \u003cbr\u003e Units and Constants \u003cbr\u003e \u003cbr\u003e PART I: Basic Principles and Applications \u003cbr\u003e \u003cbr\u003e THE PHYSICAL BASIS OF THE NUCLEAR MAGNETIC RESONANCE EXPERIMENT\u003cbr\u003e The Quantum Mechanical Model for the Isolated Proton \u003cbr\u003e Classical Description of the NMR Experiment \u003cbr\u003e Experimental Verification of Quantized Angular Momentum and of the Resonance Equation \u003cbr\u003e The NMR Experiment on Compact Matter and the Principle of the NMR Spectrometer \u003cbr\u003e Magnetic Properties of Nuclei beyond the Proton \u003cbr\u003e \u003cbr\u003e THE PROTON MAGNETIC RESONANCE SPECTRA OF ORGANIC MOLECULES  -  CHEMICAL SHIFT AND SPIN -\u003cbr\u003e SPIN COUPLING \u003cbr\u003e The Chemical Shift \u003cbr\u003e Spin -\u003cbr\u003e Spin Coupling \u003cbr\u003e \u003cbr\u003e GENERAL EXPERIMENTAL ASPECTS OF NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY \u003cbr\u003e Sample Preparation and Sample Tubes\u003cbr\u003e Internal and External Standards;\u003cbr\u003e Solvent Effects \u003cbr\u003e Tuning the Spectrometer \u003cbr\u003e Increasing the Sensitivity \u003cbr\u003e Measurement of Spectra at Different Temperatures \u003cbr\u003e \u003cbr\u003e PROTON CHEMICAL SHIFTS AND SPIN -\u003cbr\u003e SPIN COUPLING CONSTANTS AS FUNCTIONS OF STRUCTURE \u003cbr\u003e Origin of Proton Chemical Shifts \u003cbr\u003e Proton -\u003cbr\u003e Proton Spin -\u003cbr\u003e Spin Coupling and Chemical Structure \u003cbr\u003e \u003cbr\u003e THE ANALYSIS OF HIGH-RESOLUTION NUCLEAR MAGNETIC RESONANCE SPECTRA \u003cbr\u003e Notation for Spin Systems \u003cbr\u003e Quantum Mechanical Formalism \u003cbr\u003e The Hamilton Operator for High-Resolution Nuclear Magnetic Resonance Spectroscopy \u003cbr\u003e Calculation of Individual Spin Systems \u003cbr\u003e \u003cbr\u003e THE INFLUENCE OF MOLECULAR SYMMETRY AND CHIRALITY ON PROTON MAGNETIC RESONANCE SPECTRA \u003cbr\u003e Spectral Types and Structural Isomerism \u003cbr\u003e Influence of Chirality on the NMR Spectrum \u003cbr\u003e Analysis of Degenerate Spin Systems by Means of 13C Satellites and H\/D Substitution \u003cbr\u003e \u003cbr\u003e PART II: Advanced Methods and Applications \u003cbr\u003e \u003cbr\u003e THE PHYSICAL BASIS OF THE NUCLEAR MAGNETIC RESONANCE EXPERIMENT.\u003cbr\u003e The NMR Signal by Pulse Excitation \u003cbr\u003e Relaxation Effects \u003cbr\u003e Pulse Fourier-Transform (FT) NMR Spectroscopy \u003cbr\u003e Experimental Aspects of Pulse Fourier-Transform Spectroscopy \u003cbr\u003e Double Resonance Experiments \u003cbr\u003e \u003cbr\u003e TWO-DIMENSIONAL NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY \u003cbr\u003e Principles of Two-Dimensional NMR Spectroscopy \u003cbr\u003e The Spin Echo Experiment in Modern NMR Spectroscopy \u003cbr\u003e Homonuclear Two-Dimensional Spin Echo Spectroscopy: Separation of the Parameters J and d for Proton NMR Spectra \u003cbr\u003e The COSY Experiment  -  Two-Dimensional 1H,1H Shift Correlations \u003cbr\u003e The Product Operator Formalism \u003cbr\u003e Phase Cycles \u003cbr\u003e Gradient Enhanced Spectroscopy \u003cbr\u003e Universal Building Blocks for Pulse Sequences \u003cbr\u003e Homonuclear Shift Correlation by Double Quantum Selection of AX Systems  -  the 2D-INADEQUATE Experiment \u003cbr\u003e Single-Scan 2D NMR \u003cbr\u003e \u003cbr\u003e MORE 1D AND 2D NMR EXPERIMENTS: THE NUCLEAR OVERHAUSER EFFECT  -  POLARIZATION TRANSFER  -  SPIN LOCK EXPERIMENTS  -  3D NMR \u003cbr\u003e The Overhauser Effect \u003cbr\u003e Polarization Transfer Experiments \u003cbr\u003e Rotating Frame Experiments \u003cbr\u003e Multidimensional NMR Experiments \u003cbr\u003e \u003cbr\u003e CARBON-13 NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY \u003cbr\u003e Historical Development and the Most Important Areas of Application \u003cbr\u003e Experimental Aspects of Carbon-13 Nuclear Magnetic Resonance Spectroscopy \u003cbr\u003e Carbon-13 Chemical Shifts \u003cbr\u003e Carbon-13 Spin -\u003cbr\u003e Spin Coupling Constants \u003cbr\u003e Carbon-13 Spin -\u003cbr\u003e Lattice Relaxation Rates \u003cbr\u003e \u003cbr\u003e SELECTED HETERONUCLEI \u003cbr\u003e Semimetals and Non-metals with the Exception of Hydrogen and Carbon \u003cbr\u003e Main Group Metals \u003cbr\u003e Transition Metals \u003cbr\u003e \u003cbr\u003e INFLUENCE OF DYNAMIC EFFECTS ON NUCLEAR MAGNETIC RESONANCE SPECTRA \u003cbr\u003e Exchange of Protons between Positions with Different Larmor Frequencies \u003cbr\u003e Internal Dynamics of Organic Molecules \u003cbr\u003e Intermolecular Exchange Processes \u003cbr\u003e Line Broadening by Fast Relaxing Neighboring Nuclei \u003cbr\u003e \u003cbr\u003e NUCLEAR MAGNETIC RESONANCE OF PARTIALLY ORIENTED MOLECULES AND SOLID STATE NMR\u003cbr\u003e Nuclear Magnetic Resonance of Partially Oriented Molecules \u003cbr\u003e High-Resolution Solid State Nuclear Magnetic Resonance Spectroscopy \u003cbr\u003e \u003cbr\u003e SELECTED TOPICS OF NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY \u003cbr\u003e Isotope Effects in Nuclear Magnetic Resonance \u003cbr\u003e Nuclear Magnetic Resonance Spectroscopy of Paramagnetic Materials \u003cbr\u003e Chemically Induced Dynamic Nuclear Polarization (CIDNP) \u003cbr\u003e Diffusion-Controlled Nuclear Magnetic Resonance Spectroscopy  -  DOSY \u003cbr\u003e Unconventional Methods for Sensitivity Enhancement  -  Hyperpolarization \u003cbr\u003e Nuclear Magnetic Resonance in Biochemistry and Medicine \u003cbr\u003e \u003cbr\u003e INDEX \u003cbr\u003e","brand":"Wiley-VCH Verlag GmbH","offers":[{"title":"Default Title","offer_id":53196947095895,"sku":"9783527330041","price":125.35,"currency_code":"GBP","in_stock":false}],"url":"https:\/\/bookcurl.com\/products\/nmr-spectroscopy-basic-principles-concepts-and-applications-in-chemistry-9783527330041","provider":"Book Curl","version":"1.0","type":"link"}