{"product_id":"neutrons-and-synchrotron-radiation-in-engineering-materials-science-from-fundamentals-to-applications-9783527335923","title":"Neutrons and Synchrotron Radiation in Engineering Materials Science: From Fundamentals to Applications","description":"\u003cb\u003eBook Synopsis\u003c\/b\u003e\u003cbr\u003eRetaining its proven concept, the second edition of this ready reference specifically addresses the need of materials engineers for reliable, detailed information on modern material characterization methods.\u003cbr\u003e \u003cbr\u003e As such, it provides a systematic overview of the increasingly important field of characterization of engineering materials with the help of neutrons and synchrotron radiation. The first part introduces readers to the fundamentals of structure-property relationships in materials and the radiation sources suitable for materials characterization.\u003cbr\u003e \u003cbr\u003e The second part then focuses on such characterization techniques as diffraction and scattering methods, as well as direct imaging and tomography. The third part presents new and emerging methods of materials characterization in the field of 3D characterization techniques like three-dimensional X-ray diffraction microscopy. The fourth and final part is a collection of examples that demonstrate the application of the methods introduced in the first parts to problems in materials science.\u003cbr\u003e \u003cbr\u003e With thoroughly revised and updated chapters and now containing about 20%\u003cbr\u003e new material, this is the must-have, in-depth resource on this highly relevant topic.\u003cbr\u003e\u003cbr\u003e\u003cbr\u003e\u003cb\u003eTable of Contents\u003c\/b\u003e\u003cbr\u003e\u003cp\u003eList of Contributor XVII\u003c\/p\u003e \u003cp\u003ePreface to Second Edition XXIII\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePart I General 1\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e1 Microstructure and Properties of Engineering Materials 3\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eHelmut Clemens, Svea Mayer, and Christina Scheu\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e1.1 Introduction 3\u003c\/p\u003e \u003cp\u003e1.2 Microstructure 4\u003c\/p\u003e \u003cp\u003e1.3 Microstructure and Properties 10\u003c\/p\u003e \u003cp\u003e1.4 Microstructural Characterization 12\u003c\/p\u003e \u003cp\u003e\u003cb\u003e2 Internal Stresses in Engineering Materials 21\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eAnke Kaysser-Pyzalla\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e2.1 Definition 21\u003c\/p\u003e \u003cp\u003e2.2 Origin of Residual Macro- and Microstresses 25\u003c\/p\u003e \u003cp\u003e2.3 Relevance 45\u003c\/p\u003e \u003cp\u003e\u003cb\u003e3 Textures in Engineering Materials 55\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eHeinz G. Brokmeier and Sangbong Yi\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e3.1 Introduction 55\u003c\/p\u003e \u003cp\u003e3.2 Measurement of Preferred Orientations 58\u003c\/p\u003e \u003cp\u003e3.3 Presentation of Preferred Orientations 59\u003c\/p\u003e \u003cp\u003e3.4 Interpretation of Textures 62\u003c\/p\u003e \u003cp\u003e3.5 Errors 67\u003c\/p\u003e \u003cp\u003e\u003cb\u003e4 Physical Properties of Photons and Neutrons 73\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eAndreas Schreyer\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e4.1 Introduction 73\u003c\/p\u003e \u003cp\u003e4.2 Interaction of X-ray Photons and Neutrons with Individual Atoms 74\u003c\/p\u003e \u003cp\u003e4.3 Scattering of X-ray Photons and Neutrons from Ensembles of Atoms 79\u003c\/p\u003e \u003cp\u003e\u003cb\u003e5 Radiation Sources 83\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e5.1 Generation and Properties of Neutrons 83\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eIna Lommatzsch,Wolfgang Knop, Philipp K. Pranzas, and Peter Schreiner\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e5.2 Production and Properties of Synchrotron Radiation 90\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eRolf Treusch\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePart II Methods 105\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e6 Stress Analysis by Angle-Dispersive Neutron Diffraction 107\u003c\/b\u003e\u003cbr\u003e\u003ci\u003ePeter Staron\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e6.1 Introduction 107\u003c\/p\u003e \u003cp\u003e6.2 Diffractometer for Residual Stress Analysis 108\u003c\/p\u003e \u003cp\u003e6.3 Measurement and Data Analysis 112\u003c\/p\u003e \u003cp\u003e6.4 Examples 116\u003c\/p\u003e \u003cp\u003e6.5 Summary and Outlook 120\u003c\/p\u003e \u003cp\u003e\u003cb\u003e7 Stress Analysis by Energy-Dispersive Neutron Diffraction 123\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eJavier Santisteban\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e7.1 Introduction 123\u003c\/p\u003e \u003cp\u003e7.2 Time-of-Flight Neutron Diffraction 123\u003c\/p\u003e \u003cp\u003e7.3 TOF Strain Scanners 126\u003c\/p\u003e \u003cp\u003e7.4 A Virtual Laboratory for Strain Scanning 131\u003c\/p\u003e \u003cp\u003e7.5 Type II Stresses: Evolution of Intergranular Stresses 134\u003c\/p\u003e \u003cp\u003e7.6 Type III Stresses: Dislocation Densities 135\u003c\/p\u003e \u003cp\u003e7.7 Strain Imaging by Energy-Dispersive Neutron Transmission 138\u003c\/p\u003e \u003cp\u003e7.8 Conclusions 140\u003c\/p\u003e \u003cp\u003e\u003cb\u003e8 Residual Stress Analysis by Monochromatic High-Energy X-rays 145\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eRené V. Martins\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e8.1 Basic Setups 145\u003c\/p\u003e \u003cp\u003e8.2 Principle of Slit Imaging and Data Reconstruction 148\u003c\/p\u003e \u003cp\u003e8.3 The Conical Slit 149\u003c\/p\u003e \u003cp\u003e8.4 The Spiral Slit 152\u003c\/p\u003e \u003cp\u003e8.5 Simultaneous Strain Measurements in Individual Bulk Grains 155\u003c\/p\u003e \u003cp\u003e8.6 Coarse Grain Effects 156\u003c\/p\u003e \u003cp\u003e8.7 Analysis of Diffraction Data from Area Detectors 157\u003c\/p\u003e \u003cp\u003e8.8 Matrix for Comparison and Decision Taking Which Technique to Use for a Specific Problem 158\u003c\/p\u003e \u003cp\u003e\u003cb\u003e9 Residual Stress Analysis by Energy-Dispersive Synchrotron X-ray Diffraction 161\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eChristoph Genzel and Manuela Klaus\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e9.1 Introduction 161\u003c\/p\u003e \u003cp\u003e9.2 Fundamentals of Energy-Dispersive X-ray Diffraction Stress Analysis 162\u003c\/p\u003e \u003cp\u003e9.3 Experimental Setup 167\u003c\/p\u003e \u003cp\u003e9.4 Examples for Energy-Dispersive Stress Analysis 168\u003c\/p\u003e \u003cp\u003e9.5 Final Remarks 173\u003c\/p\u003e \u003cp\u003e\u003cb\u003e10 Texture Analyses by Synchrotron X-rays and Neutrons 179\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eSangbong Yi, Weimin Gan, and Heinz G. Brokmeier\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e10.1 Texture Measurements on Laboratory Scale 179\u003c\/p\u003e \u003cp\u003e10.2 Texture Measurements at Large Scale Facilities 182\u003c\/p\u003e \u003cp\u003e10.3 Conclusion 193\u003c\/p\u003e \u003cp\u003e\u003cb\u003e11 Basics of Small-Angle Scattering Methods 197\u003c\/b\u003e\u003cbr\u003e\u003ci\u003ePhilipp K. Pranzas\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e11.1 Introduction 197\u003c\/p\u003e \u003cp\u003e11.2 Common Features of a SAS Instrument 197\u003c\/p\u003e \u003cp\u003e11.3 Contrast 198\u003c\/p\u003e \u003cp\u003e11.4 Scattering Curve 198\u003c\/p\u003e \u003cp\u003e11.5 Power Law\/Scattering by Fractal Systems 200\u003c\/p\u003e \u003cp\u003e11.6 Guinier and Porod Approximations 201\u003c\/p\u003e \u003cp\u003e11.7 Macroscopic Differential Scattering Cross-section 202\u003c\/p\u003e \u003cp\u003e11.8 Model Calculation of Size Distributions 202\u003c\/p\u003e \u003cp\u003e11.9 Magnetic Structures 203\u003c\/p\u003e \u003cp\u003e\u003cb\u003e12 Small-Angle Neutron Scattering 207\u003c\/b\u003e\u003cbr\u003e\u003ci\u003ePhilipp K. Pranzas and André Heinemann\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e12.1 Introduction 207\u003c\/p\u003e \u003cp\u003e12.2 Nanocrystalline Magnesium Hydride for the Reversible Storage of Hydrogen 208\u003c\/p\u003e \u003cp\u003e12.3 Precipitates in Steel 210\u003c\/p\u003e \u003cp\u003e12.4 SiO2 Nanoparticles in a Polymer Matrix – An Industrial Application 213\u003c\/p\u003e \u003cp\u003e12.5 Green Surfactants 213\u003c\/p\u003e \u003cp\u003e\u003cb\u003e13 Anomalous Small-Angle X-ray Scattering 217\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eUlla Vainio\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e13.1 Introduction 217\u003c\/p\u003e \u003cp\u003e13.2 Theory 218\u003c\/p\u003e \u003cp\u003e13.3 Experiments 223\u003c\/p\u003e \u003cp\u003e13.4 Example: ASAXS on Catalyst Nanoparticles 223\u003c\/p\u003e \u003cp\u003e13.5 Summary and Outlook 223\u003c\/p\u003e \u003cp\u003e\u003cb\u003e14 Imaging 227\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eWolfgang Treimer\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e14.1 Radiography 227\u003c\/p\u003e \u003cp\u003e14.2 Tomography 240\u003c\/p\u003e \u003cp\u003e14.3 New Developments in Neutron Tomography 244\u003c\/p\u003e \u003cp\u003e\u003cb\u003e15 Neutron and Synchrotron-Radiation-Based Imaging for Applications in Materials Science – From Macro- to Nanotomography 253\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eFelix Beckmann\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e15.1 Introduction 253\u003c\/p\u003e \u003cp\u003e15.2 Parallel-Beam Tomography 256\u003c\/p\u003e \u003cp\u003e15.3 Macrotomography Using Neutrons 258\u003c\/p\u003e \u003cp\u003e15.4 Microtomography Using Synchrotron Radiation 264\u003c\/p\u003e \u003cp\u003e15.5 Summary and Outlook 271\u003c\/p\u003e \u003cp\u003e\u003cb\u003e16 Mu-Tomography of Engineering Materials 275\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eAstrid Haibel and Julia Herzen\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e16.1 Introduction 275\u003c\/p\u003e \u003cp\u003e16.2 Advantage of Synchrotron Tomography 275\u003c\/p\u003e \u003cp\u003e16.3 Applications and 3D Image Analysis 276\u003c\/p\u003e \u003cp\u003e16.4 Image Artifacts 282\u003c\/p\u003e \u003cp\u003e16.5 Summary 286\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePart III New and Emerging Methods 291\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e17 3D X-ray Diffraction Microscope 293\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eHenning F. Poulsen,Wolfgang Ludwig, and Søren Schmidt\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e17.1 Basic Setup and Strategy 294\u003c\/p\u003e \u003cp\u003e17.2 Indexing and Characterization of Average Properties of Each Grain 296\u003c\/p\u003e \u003cp\u003e17.3 Mapping of Grains and Orientations 300\u003c\/p\u003e \u003cp\u003e17.4 Combining 3DXRD and Tomography 304\u003c\/p\u003e \u003cp\u003e17.5 Outlook 305\u003c\/p\u003e \u003cp\u003e\u003cb\u003e18 3D Micron-Resolution Laue Diffraction 309\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eGene E. Ice\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e18.1 Introduction 309\u003c\/p\u003e \u003cp\u003e18.2 The Need for Polychromatic Microdiffraction 309\u003c\/p\u003e \u003cp\u003e18.3 Theoretical Basis for Advanced Polychromatic Microdiffraction 311\u003c\/p\u003e \u003cp\u003e18.4 Technical Developments for an Automated 3D Probe 313\u003c\/p\u003e \u003cp\u003e18.5 Research Examples 318\u003c\/p\u003e \u003cp\u003e18.6 Future Prospects and Opportunities 324\u003c\/p\u003e \u003cp\u003e\u003cb\u003ePart IV Applications 327\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e19 The Use of Neutron and Synchrotron Research for Aerospace and Automotive Materials and Components 329\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eWolfgang Kaysser, Jörg Eßlinger, Volker Abetz, Norbert Huber, Karl U. Kainer, Thomas Klassen, Florian Pyczak, Andreas Schreyer, and Peter Staron\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e19.1 Introduction 329\u003c\/p\u003e \u003cp\u003e19.2 Commercial Passenger Aircraft 331\u003c\/p\u003e \u003cp\u003e19.3 The Light-Duty Automotive Vehicle 341\u003c\/p\u003e \u003cp\u003e19.4 Other Transport Systems 352\u003c\/p\u003e \u003cp\u003e\u003cb\u003e20 In situ Experiments with Synchrotron High-Energy X-rays and Neutrons 365\u003c\/b\u003e\u003cbr\u003e\u003ci\u003ePeter Staron, Torben Fischer, Thomas Lippmann, Andreas Stark, Shahrokh \u003c\/i\u003eDaneshpour, \u003ci\u003eDirk Schnubel, Eckart Uhlmann, Robert Gerstenberger, Bettina Camin, Walter Reimers, Elisabeth Eidenberger-Schober, Helmut Clemens, Norbert Huber, and Andreas Schreyer\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e20.1 Introduction 365\u003c\/p\u003e \u003cp\u003e20.2 In situ Dilatometry 366\u003c\/p\u003e \u003cp\u003e20.3 In situ Study on Single Overload of Fatigue-Cracked Specimens 368\u003c\/p\u003e \u003cp\u003e20.4 In situ Cutting Experiment 370\u003c\/p\u003e \u003cp\u003e20.5 In situ Study of Precipitation Kinetics Using Neutrons 372\u003c\/p\u003e \u003cp\u003e20.6 Conclusions 373\u003c\/p\u003e \u003cp\u003e\u003cb\u003e21 Application of Photons and Neutrons for the Characterization and Development of Advanced Steels 377\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eElisabeth Eidenberger-Schober, Ronald Schnitzer, Gerald A. Zickler, Michael Eidenberger-Schober,Michael Bischof, Peter Staron, Harald Leitner, Andreas Schreyer, and Helmut Clemens\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e21.1 Introduction 377\u003c\/p\u003e \u003cp\u003e21.2 Characterization Using Synchrotron Radiation 378\u003c\/p\u003e \u003cp\u003e21.3 Characterization Using Small-Angle Neutron Scattering (SANS) 382\u003c\/p\u003e \u003cp\u003e21.4 Conclusions 388\u003c\/p\u003e \u003cp\u003e\u003cb\u003e22 The Contribution of High-Energy X-rays and Neutrons to Characterization and Development of Intermetallic Titanium Aluminides 395\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eThomas Schmoelzer, Klaus-Dieter Liss, Peter Staron, Andreas Stark, Emanuel Schwaighofer, Thomas Lippmann, Helmut Clemens, and Svea Mayer\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e22.1 Introduction 395\u003c\/p\u003e \u003cp\u003e22.2 High-Energy X-rays and Neutrons 396\u003c\/p\u003e \u003cp\u003e22.3 In situ Investigation of Phase Evolution 398\u003c\/p\u003e \u003cp\u003e22.4 Atomic Order and Disorder in TiAl Alloys 409\u003c\/p\u003e \u003cp\u003e22.5 Recovery and Recrystallization during Deformation of TiAl 412\u003c\/p\u003e \u003cp\u003e22.6 Lattice Parameter and Thermal Expansion 418\u003c\/p\u003e \u003cp\u003e22.7 Conclusions 419\u003c\/p\u003e \u003cp\u003e\u003cb\u003e23 In situ Mu-Laue: Instrumental Setup for the Deformation of Micron Sized Samples 425\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eChristoph Kirchlechner, Jozef Keckes, Jean S.Micha, and Gerhard Dehm\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e23.1 Introduction 425\u003c\/p\u003e \u003cp\u003e23.2 Experimental Instrumentation 427\u003c\/p\u003e \u003cp\u003e23.3 Discussion 433\u003c\/p\u003e \u003cp\u003e23.4 Conclusion 436\u003c\/p\u003e \u003cp\u003e\u003cb\u003e24 Residual Stresses in Thin Films and Coated Tools: Challenges and Strategies for Their Nondestructive Analysis by X-ray Diffraction Methods 439\u003c\/b\u003e\u003cbr\u003e\u003ci\u003eManuela Klaus and Christoph Genzel\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e24.1 Introduction 439\u003c\/p\u003e \u003cp\u003e24.2 Compilation of Approaches to Meet the Challenges in Thin Film X-ray Stress Analysis (XSA) 441\u003c\/p\u003e \u003cp\u003e24.3 Final Remarks and Recommendations 447\u003c\/p\u003e \u003cp\u003eIndex 451\u003c\/p\u003e","brand":"Wiley-VCH Verlag GmbH","offers":[{"title":"Default Title","offer_id":53196948242775,"sku":"9783527335923","price":138.56,"currency_code":"GBP","in_stock":false}],"url":"https:\/\/bookcurl.com\/products\/neutrons-and-synchrotron-radiation-in-engineering-materials-science-from-fundamentals-to-applications-9783527335923","provider":"Book Curl","version":"1.0","type":"link"}