{"product_id":"inorganic-syntheses-35-9780471682554","title":"Inorganic Syntheses 35","description":"\u003cb\u003eBook Synopsis\u003c\/b\u003e\u003cbr\u003eThe Inorganic Syntheses series provides all users of inorganic substances with detailed and foolproof procedures for the preparation of important and timely compounds.       * Includes complete, up-to-date procedures involving important inorganic substances    * Contains subject, contributor, and formula indexes   .\u003cbr\u003e\u003cbr\u003e\u003cb\u003eTable of Contents\u003c\/b\u003e\u003cbr\u003ePreface.  \u003cp\u003eContributors.\u003c\/p\u003e \u003cp\u003eDedication.\u003c\/p\u003e \u003cp\u003eNotice to Contributors and Checkers.\u003c\/p\u003e \u003cp\u003eToxic Substances and Laboratory Hazards.\u003c\/p\u003e \u003cp\u003eChapter One COMPLEXES OF BULKY ß-DIKETIMINATE LIGANDS.\u003c\/p\u003e \u003cp\u003e1. Introduction.\u003c\/p\u003e \u003cp\u003e2. ß-Diketiminate Precursors HL\u003csup\u003eMe,Me3\u003c\/sup\u003e and TlL\u003csup\u003eMe,Me3\u003c\/sup\u003e (L\u003csup\u003eMe,Me3\u003c\/sup\u003e = 2,4-Bis-(Mesitylimido)Pentyl).\u003c\/p\u003e \u003cp\u003e3. ß-Diketiminate Precursors L\u003csup\u003eMe,iPr2\u003c\/sup\u003eH, [\u003csup\u003eLMe,iPr2\u003c\/sup\u003eLi]x, and [L\u003csup\u003etBu,iPr2\u003c\/sup\u003eK]x (L\u003csup\u003eMe,iPr2\u003c\/sup\u003e = 2,4-Bis-(2,6-Diisopropylphenylimido)Pentyl; L\u003csup\u003etBu,iPr2\u003c\/sup\u003e = 2,2,6,6-\u003c\/p\u003e \u003cp\u003eTetramethyl-3,5-Bis-(2,6-Diisopropylphenylimido)Heptyl).\u003c\/p\u003e \u003cp\u003e4. ß-Diketiminate Precursors L\u003csup\u003etBu,iPr2\u003c\/sup\u003eH and L\u003csup\u003etBu,iPr2\u003c\/sup\u003eLi(THF) (L\u003csup\u003etBu,iPr2\u003c\/sup\u003e=2,2,6,6-Tetramethyl-3,5- Bis-(2,6-Diisopropylphenylimido)Heptyl).\u003c\/p\u003e \u003cp\u003e5. Scandium Trichloride Tris(Tetrahydrofuran) and ß-Diketiminate-Supported Scandium Chloride Complexes.\u003c\/p\u003e \u003cp\u003e6. ß-Diketiminate-Supported Titanium and Vanadium Dichloride Complexes.\u003c\/p\u003e \u003cp\u003e7. ß-Diketiminate-Supported Vanadium and Chromium Chloride Complexes.\u003c\/p\u003e \u003cp\u003e8. ß-Diketiminate-Supported Manganese and Zinc Complexes.\u003c\/p\u003e \u003cp\u003e9. Iron 2,4-Bis-(2,6-Diisopropylphenylimido)Pentyl Chloride (L\u003csup\u003eMe,iPr2\u003c\/sup\u003eFeCl).\u003c\/p\u003e \u003cp\u003e10. Iron 2,2,6,6-Tetramethyl-3,5-Bis-(2,6-Diisopropylphenylimido)Heptyl Chloride (L\u003csup\u003etBu,iPr2\u003c\/sup\u003eFeCl).\u003c\/p\u003e \u003cp\u003e11. Cobalt 2,2,6,6-Tetramethyl-3,5-Bis-(2,6-Diisopropylphenylimido) Heptyl Chloride (L\u003csup\u003etBu,iPr2\u003c\/sup\u003eCoCl).\u003c\/p\u003e \u003cp\u003e12. ß-Diketiminate-Supported Nickel(II) and Nickel(I) Complexes of L\u003csup\u003eMe,Me3\u003c\/sup\u003e (L\u003csup\u003eMe,Me3\u003c\/sup\u003e = 2,4-Bis-(Mesitylimido)Pentyl).\u003c\/p\u003e \u003cp\u003e13. Nickel 2,4-Bis-(2,6-Diisopropylphenylimido)Pentyl Chloride Dimer, [L\u003csup\u003eMe,iPr2\u003c\/sup\u003eNi(µ-Cl)]\u003csub\u003e2\u003c\/sub\u003e.\u003c\/p\u003e \u003cp\u003e14. Bis[Copper 2,4-Bis-(2,4,6-Trimethylphenylimido)Pentyl] Toluene, (L\u003csup\u003eMe,Me3\u003c\/sup\u003eCu)\u003csub\u003e2\u003c\/sub\u003e(µ-n\u003csup\u003e2\u003c\/sup\u003e:n\u003csup\u003e2\u003c\/sup\u003e-C\u003csub\u003e7\u003c\/sub\u003eH\u003csub\u003e8\u003c\/sub\u003e).\u003c\/p\u003e \u003cp\u003e15. Copper 2,4-Bis-(2,6-Diisopropylphenylimido)Pentyl Chloride (L\u003csup\u003eMe,iPr2\u003c\/sup\u003eCuCl).\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter Two BORON CLUSTER COMPOUNDS.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e16. Salts of Dodecamethylcarba-\u003ci\u003ecloso\u003c\/i\u003e-Dodecaborate(—) Anion, CB\u003csub\u003e11\u003c\/sub\u003eMe\u003csub\u003e12\u003c\/sub\u003e, and the Radical Dodecamethylcarba-\u003ci\u003ecloso\u003c\/i\u003e-Dodecaboranyl, CB\u003csub\u003e11\u003c\/sub\u003eMe\u003csub\u003e12\u003c\/sub\u003e.\u003c\/p\u003e \u003cp\u003e17. Cesium Dodecahydroxy-\u003ci\u003ecloso\u003c\/i\u003e-Dodecaborate, Cs\u003csub\u003e2\u003c\/sub\u003e[B\u003csub\u003e12\u003c\/sub\u003e(OH)\u003csub\u003e12\u003c\/sub\u003e].\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter Three COORDINATION COMPOUNDS.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e18. Pentaaquanitrosylchromium Sulfate.\u003c\/p\u003e \u003cp\u003e19. The Tetradentate Bispidine Ligand Dimethyl-(3,7-Dimethyl-9-oxo-2,4-bis(2-pyridyl)-3,7-Diazabicyclo[3.3.1]nonane)-1, 5-dicarboxylate and Its Copper(ll) Complex.\u003c\/p\u003e \u003cp\u003e20. Tris(2-Picolinyl)Methane and Its Copper(I) Complex.\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter Four CARBENE LIGANDS AND COMPLEXES.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e21. 1,3-Dialkyl-Imidazole-2-Ylidenes.\u003c\/p\u003e \u003cp\u003e22. A Chelating Rhodium \u003ci\u003eN\u003c\/i\u003e-Heterocyclic Carbene Complex by Transmetallation from a Silver–NHC Intermediate.\u003c\/p\u003e \u003cp\u003e23. Rhodium and Iridium \u003ci\u003eN\u003c\/i\u003e-Heterocyclic Carbene Complexes from Imidazolium Carboxylates.\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter Five FUNCTIONAL LIGANDS AND COMPLEXES.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e24. \u003ci\u003eN\u003c\/i\u003e-\u003ci\u003etert\u003c\/i\u003e-Butyl \u003ci\u003eortho\u003c\/i\u003e-Aminophenol, \u003ci\u003eortho\u003c\/i\u003e-Iminoquinone, and a Zirconium(IV) bis(Aminophenolate) Complex.\u003c\/p\u003e \u003cp\u003e25. Synthesis of the Water-Soluble Bidentate (P, N) Ligand PTN(Me) (PTN(Me) = 7-Phospha-3-methyl-1,3,5-triazabicyclo[3.3.1]nonane).\u003c\/p\u003e \u003cp\u003e26. Synthesis of Metal-Organic Frameworks: MOF-5 and MOF-177.\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter Six ORGANOMETALLIC REAGENTS.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e27. Tricarbonyl 1,3,5-Trimethyl-1,3,5-Triazacyclohexane Complexes of Chromium(0), Molybdenum(0), and Tungsten(0) [M(CO)\u003csub\u003e3\u003c\/sub\u003e(Me\u003csub\u003e3\u003c\/sub\u003eTACH) (M = Cr, Mo, W)].\u003c\/p\u003e \u003cp\u003e28. Manganese Tricarbonyl Transfer (MTT) Agents.\u003c\/p\u003e \u003cp\u003e29. Bis(1,5-Cyclooctadiene)Nickel(0).\u003c\/p\u003e \u003cp\u003e30. Sodium (n\u003csup\u003e5\u003c\/sup\u003e-Cyclopentadienyl)Tris(Dimethylphosphito-\u003ci\u003eP\u003c\/i\u003e) Cobaltate(III), Na[(C\u003csub\u003e5\u003c\/sub\u003eH\u003csub\u003e5\u003c\/sub\u003e)Co{P(O)(OMe)\u003csub\u003e2\u003c\/sub\u003e}\u003csub\u003e3\u003c\/sub\u003e].\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter Seven BIO-INSPIRED IRON AND NICKEL COMPLEXES.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e31. Iron–Cyanocarbonyl Complexes [PPN][Fe(CO)\u003csub\u003e4\u003c\/sub\u003e(CN)] and [PPN][FeBr(CO)\u003csub\u003e3\u003c\/sub\u003e(CN)\u003csub\u003e2\u003c\/sub\u003e].\u003c\/p\u003e \u003cp\u003e32. Nickel Complexes of Bis(Diethylphosphinomethyl) Methylamine.\u003c\/p\u003e \u003cp\u003e33. Monomeric Iron(II) Complexes Having Two Sterically Hindered Arylthiolates.\u003c\/p\u003e \u003cp\u003e34 (1,3-Propanedithiolato)-Hexacarbonyldiiron and Cyanide Derivatives.\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter Eight RUTHENIUM COMPLEXES.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e35. Ruthenium(II)-Chlorido Complexes of Dimethylsulfoxide.\u003c\/p\u003e \u003cp\u003e36. Synthesis of Chloride-Free Ruthenium(II) Hexaaqua Tosylate, [Ru(H\u003csub\u003e2\u003c\/sub\u003eO)\u003csub\u003e6\u003c\/sub\u003e]tos\u003csub\u003e2\u003c\/sub\u003e.\u003c\/p\u003e \u003cp\u003e37. Basic Ruthenium Acetate and Mixed Valence Derivatives.\u003c\/p\u003e \u003cp\u003e38. Di-µ-Chloro(Ethylbenzoate)Diruthenium(II), [(n\u003csup\u003e6\u003c\/sup\u003e-etb)RuCl\u003csub\u003e2\u003c\/sub\u003e]\u003csub\u003e2\u003c\/sub\u003e.\u003c\/p\u003e \u003cp\u003e\u003cb\u003eChapter Nine IRIDIUM COMPLEXES.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e39. The Diphosphine tfepma and its Diiridium Complex Ir\u003csub\u003e2\u003c\/sub\u003e\u003csup\u003e0,II\u003c\/sup\u003e(tfepma)\u003csub\u003e3\u003c\/sub\u003eCl\u003csub\u003e2\u003c\/sub\u003e.\u003c\/p\u003e \u003cp\u003e40. Heteroleptic Cyclometalated Iridium(III) Complexes.\u003c\/p\u003e \u003cp\u003e41. Oxygen and Carbon Bound Acetylacetonato Iridium(III) Complexes.\u003c\/p\u003e \u003cp\u003eContributor Index.\u003c\/p\u003e \u003cp\u003eSubject Index.\u003c\/p\u003e \u003cp\u003eFormula Index.\u003c\/p\u003e","brand":"John Wiley \u0026 Sons Inc","offers":[{"title":"Default Title","offer_id":49402652885335,"sku":"9780471682554","price":127.76,"currency_code":"GBP","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0817\/1739\/5799\/files\/9780471682554.jpg?v=1730481128","url":"https:\/\/bookcurl.com\/products\/inorganic-syntheses-35-9780471682554","provider":"Book Curl","version":"1.0","type":"link"}