{"product_id":"columns-for-gas-chromatography-performance-and-selection-9780471740438","title":"Columns for Gas Chromatography Performance and","description":"\u003cb\u003eBook Synopsis\u003c\/b\u003e\u003cbr\u003eChoosing the right column is key in Gas Chromatography  Gas Chromatography (GC) is the most widely used method for separating and analyzing a wide variety of organic compounds and gases. There have been many recent advancements in both packed column and capillary column GC.\u003cbr\u003e\u003cbr\u003e\u003cb\u003eTrade Review\u003c\/b\u003e\u003cbr\u003e\"This book provides the necessary guidance for column selection and type of column chosen with the injection system and detectors in mind.\" (\u003ci\u003eInternational Journal of Environmental and Analytical Chemistry\u003c\/i\u003e, January 2008)  \u003cp\u003e\"A very useful book for chromatographers and researchers.\" (\u003ci\u003eCHOICE\u003c\/i\u003e, September 2007)\u003c\/p\u003e \u003cp\u003e\"…a practical resource for scientists and technicians…\" (\u003ci\u003eJournal of the American Chemical Society\u003c\/i\u003e, August 15, 2007)\u003c\/p\u003e\u003cbr\u003e\u003cbr\u003e\u003cb\u003eTable of Contents\u003c\/b\u003e\u003cbr\u003e\u003cb\u003ePreface.\u003c\/b\u003e  \u003cp\u003e\u003cb\u003eAcknowledgments.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003e1 Introduction.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e1.1 Evolution of Gas Chromatographic Columns.\u003c\/p\u003e \u003cp\u003e1.2 Central Role Played by the Column.\u003c\/p\u003e \u003cp\u003e1.3 Justification for Column Selection and Care.\u003c\/p\u003e \u003cp\u003e1.4 Literature on Gas Chromatographic Columns.\u003c\/p\u003e \u003cp\u003e1.5 Gas Chromatographic Resources on the Internet.\u003c\/p\u003e \u003cp\u003eReferences.\u003c\/p\u003e \u003cp\u003e\u003cb\u003e2 Packed Column Gas Chromatography.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e2.1 Introduction.\u003c\/p\u003e \u003cp\u003e2.2 Solid Supports and Adsorbents.\u003c\/p\u003e \u003cp\u003eSupports for Gas–Liquid Chromatography.\u003c\/p\u003e \u003cp\u003eAdsorbents for Gas–Solid Chromatography.\u003c\/p\u003e \u003cp\u003e2.3 Stationary Phases.\u003c\/p\u003e \u003cp\u003eRequirements of a Stationary Phase.\u003c\/p\u003e \u003cp\u003eUSP Designation of Stationary Phases.\u003c\/p\u003e \u003cp\u003eKovats Retention Index.\u003c\/p\u003e \u003cp\u003eMcReynolds and Rohrschneider Classifications of Stationary Phases.\u003c\/p\u003e \u003cp\u003eEvaluation of Column Operation.\u003c\/p\u003e \u003cp\u003eOptimization of Packed Column Separations.\u003c\/p\u003e \u003cp\u003e2.4 Column Preparation.\u003c\/p\u003e \u003cp\u003eCoating Methods.\u003c\/p\u003e \u003cp\u003eTubing Materials and Dimensions.\u003c\/p\u003e \u003cp\u003eGlass Wool Plugs and Column Fittings.\u003c\/p\u003e \u003cp\u003eFilling the Column.\u003c\/p\u003e \u003cp\u003eConditioning the Column and Column Care.\u003c\/p\u003e \u003cp\u003e2.5 \u003ci\u003eUnited States Pharmacopeia\u003c\/i\u003e and \u003ci\u003eNational Formulary\u003c\/i\u003e Chromatographic Methods.\u003c\/p\u003e \u003cp\u003eReferences.\u003c\/p\u003e \u003cp\u003e\u003cb\u003e3 Capillary Column Gas Chromatography.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e3.1 Introduction.\u003c\/p\u003e \u003cp\u003eSignificance and Impact of Capillary Gas Chromatography.\u003c\/p\u003e \u003cp\u003eChronology of Achievements in Capillary Gas Chromatography.\u003c\/p\u003e \u003cp\u003eComparison of Packed and Capillary Columns.\u003c\/p\u003e \u003cp\u003e3.2 Capillary Column Technology.\u003c\/p\u003e \u003cp\u003eCapillary Column Materials.\u003c\/p\u003e \u003cp\u003eFused Silica and Other Glasses.\u003c\/p\u003e \u003cp\u003eExtrusion of a Fused-Silica Capillary Column.\u003c\/p\u003e \u003cp\u003eAluminum-Clad Fused-Silica Capillary Columns.\u003c\/p\u003e \u003cp\u003eFused-Silica-Lined Stainless Steel Capillary Columns.\u003c\/p\u003e \u003cp\u003e3.3 Preparation of Fused-Silica Capillary Columns.\u003c\/p\u003e \u003cp\u003eSilanol Deactivation Procedures.\u003c\/p\u003e \u003cp\u003eStatic Coating of Capillary Columns.\u003c\/p\u003e \u003cp\u003eCapillary Cages.\u003c\/p\u003e \u003cp\u003eTest Mixtures for Monitoring Column Performance.\u003c\/p\u003e \u003cp\u003eDiagnostic Role Played by Components of Test Mixtures.\u003c\/p\u003e \u003cp\u003e3.4 Chromatographic Performance of Capillary Columns.\u003c\/p\u003e \u003cp\u003eGolay Equation Versus the van Deemter Expression.\u003c\/p\u003e \u003cp\u003eChoice of Carrier Gas.\u003c\/p\u003e \u003cp\u003eMeasurement of Linear Velocity and Flow Rate.\u003c\/p\u003e \u003cp\u003eEffect of Carrier Gas Viscosity on Linear Velocity.\u003c\/p\u003e \u003cp\u003ePhase Ratio.\u003c\/p\u003e \u003cp\u003eCoating Efficiency.\u003c\/p\u003e \u003cp\u003e3.5 Stationary-Phase Selection for Capillary Gas Chromatography.\u003c\/p\u003e \u003cp\u003eRequirements.\u003c\/p\u003e \u003cp\u003eHistory.\u003c\/p\u003e \u003cp\u003eComparison of Columns from Manufacturers.\u003c\/p\u003e \u003cp\u003ePolysiloxane Phases.\u003c\/p\u003e \u003cp\u003ePolyethylene Glycol Phases.\u003c\/p\u003e \u003cp\u003eCross-Linked Versus Chemically Bonded Phase.\u003c\/p\u003e \u003cp\u003eChemical Bonding.\u003c\/p\u003e \u003cp\u003eMS-Grade Phases Versus Polysilarylene or Polysilphenylene Phases.\u003c\/p\u003e \u003cp\u003eSol-Gel Stationary Phases.\u003c\/p\u003e \u003cp\u003ePhenylpolycarborane–Siloxane Phases.\u003c\/p\u003e \u003cp\u003e3.6 Specialty Columns.\u003c\/p\u003e \u003cp\u003eEPA Methods.\u003c\/p\u003e \u003cp\u003eChiral Stationary Phases.\u003c\/p\u003e \u003cp\u003eGas–Solid Adsorption Capillary Columns: PLOT Columns.\u003c\/p\u003e \u003cp\u003e3.7 Capillary Column Selection.\u003c\/p\u003e \u003cp\u003ePractical Considerations of Column Diameter, Film Thickness, and Column Length.\u003c\/p\u003e \u003cp\u003eCapillary Columns of 0.53mm i.d.: Megabore Columns.\u003c\/p\u003e \u003cp\u003eCorrelation of Column Dimensions and Film Thickness with Parameters in the Fundamental Resolution Equation.\u003c\/p\u003e \u003cp\u003eColumn Selection for Gas Chromatography by Specifications.\u003c\/p\u003e \u003cp\u003e3.8 Column Installation and Care.\u003c\/p\u003e \u003cp\u003eCarrier Gas Purifiers.\u003c\/p\u003e \u003cp\u003eFerrule Materials and Fittings.\u003c\/p\u003e \u003cp\u003eColumn Installation.\u003c\/p\u003e \u003cp\u003eColumn Conditioning.\u003c\/p\u003e \u003cp\u003eColumn Bleed.\u003c\/p\u003e \u003cp\u003eRetention Gap and Guard Columns.\u003c\/p\u003e \u003cp\u003eColumn Fatigue and Regeneration.\u003c\/p\u003e \u003cp\u003e3.9 Special Gas Chromatographic Techniques.\u003c\/p\u003e \u003cp\u003eSimulated Distillation.\u003c\/p\u003e \u003cp\u003eMultidimensional Gas Chromatography.\u003c\/p\u003e \u003cp\u003eComputer Modeling of Stationary Phases.\u003c\/p\u003e \u003cp\u003eReferences.\u003c\/p\u003e \u003cp\u003e\u003cb\u003e4 Column Oven Temperature Control.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e4.1 Thermal Performance Variables and Electronic Considerations.\u003c\/p\u003e \u003cp\u003e4.2 Advantages of Temperature Programming over Isothermal Operation.\u003c\/p\u003e \u003cp\u003e4.3 Oven Temperature Profiles for Programmed-Temperature Gas Chromatography.\u003c\/p\u003e \u003cp\u003e4.4 Role of Computer Assistance in Optimizing Separations in Gas Chromatography.\u003c\/p\u003e \u003cp\u003eDryLab (LC Resources).\u003c\/p\u003e \u003cp\u003eProezGC (Restek Corporation).\u003c\/p\u003e \u003cp\u003eGC-SOS (Chem SW).\u003c\/p\u003e \u003cp\u003e4.5 Fast or High-Speed Gas Chromatography.\u003c\/p\u003e \u003cp\u003eSelectivity Tuning.\u003c\/p\u003e \u003cp\u003eResistively Heated Columns and Column Jackets.\u003c\/p\u003e \u003cp\u003e4.6 Subambient Oven Temperature Control.\u003c\/p\u003e \u003cp\u003eReferences.\u003c\/p\u003e \u003cp\u003e\u003cb\u003eSelected References.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eAppendix A: Guide to Selection of Packed Columns.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eAppendix B: Column Selection.\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e\u003cb\u003eIndex.\u003c\/b\u003e\u003c\/p\u003e","brand":"John Wiley \u0026 Sons Inc","offers":[{"title":"Default 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