{"product_id":"application-of-icms-and-icicpms-in-environmental-research-9781118862001","title":"Application of ICMS and ICICPMS in Environmental","description":"\u003cb\u003eBook Synopsis\u003c\/b\u003e\u003cbr\u003eIntroduces the reader to the field of ion chromatography, species analysis and hyphenated methods IC-MS and IC-ICP-MS including the theory and theirs applications\u003cbr\u003e \u003cul\u003e \u003cli\u003eCovers the importance of species analysis and hyphenated methods in ion chromatography\u003c\/li\u003e \u003cli\u003eIncludes practical applications of IC-MS and IC-ICP-MS in environmental analysis\u003c\/li\u003e \u003cli\u003eDetails sample preparation methods for ion chromatography\u003c\/li\u003e \u003cli\u003eDiscusses hyphenated methods IC-MS and IC-ICP-MS used in determining both the total element contents and its elements\u003c\/li\u003e \u003cli\u003eDetails speciation analysis used in studying biochemical cycles of selected chemical compounds; determining toxicity and ecotoxicity of elements; food and pharmaceuticals quality control; and in technological process control and clinical analytics\u003c\/li\u003e \u003c\/ul\u003e\u003cbr\u003e\u003cbr\u003e\u003cb\u003eTable of Contents\u003c\/b\u003e\u003cbr\u003e\u003cp\u003eList of Contributors ix\u003c\/p\u003e \u003cp\u003ePreface xi\u003c\/p\u003e \u003cp\u003e\u003cb\u003e1 Principles and Applications of Ion Chromatography 1\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eRajmund Michalski\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e1.1 Principles of Ion Chromatography, 1\u003c\/p\u003e \u003cp\u003e1.1.1 Introduction, 1\u003c\/p\u003e \u003cp\u003e1.1.2 Stationary Phases, 6\u003c\/p\u003e \u003cp\u003e1.1.3 Eluents, 13\u003c\/p\u003e \u003cp\u003e1.1.4 Suppressors, 16\u003c\/p\u003e \u003cp\u003e1.1.5 Detection Methods, 18\u003c\/p\u003e \u003cp\u003e1.2 Ion Chromatography Applications, 23\u003c\/p\u003e \u003cp\u003e1.2.1 Speciation Analysis with the Hyphenated Methods of IC-ICP-MS and IC-MS, 29\u003c\/p\u003e \u003cp\u003e1.3 Sample Preparation for Ion Chromatography, 32\u003c\/p\u003e \u003cp\u003e1.4 Selected Methodological Aspects of Ion Determination with Ion Chromatography, 34\u003c\/p\u003e \u003cp\u003e1.5 Ion Chromatography Development Perspectives, 37\u003c\/p\u003e \u003cp\u003e1.6 References, 37\u003c\/p\u003e \u003cp\u003e\u003cb\u003e2 Mass Spectrometric Detectors for Environmental Studies 47\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eMaria Balcerzak\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e2.1 Introduction, 47\u003c\/p\u003e \u003cp\u003e2.2 Mass Spectrometric Detectors, 49\u003c\/p\u003e \u003cp\u003e2.2.1 Ionization Methods, 50\u003c\/p\u003e \u003cp\u003e2.2.2 Mass Analyzers, 58\u003c\/p\u003e \u003cp\u003eAcknowledgments, 62\u003c\/p\u003e \u003cp\u003e2.3 References, 62\u003c\/p\u003e \u003cp\u003e\u003cb\u003e3 High-Performance Liquid Chromatography Coupled to Inductively Coupled Plasma MS\/Electrospray Ionization MS 79\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eJürgen Mattusch\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e3.1 Separation Principles, 79\u003c\/p\u003e \u003cp\u003e3.1.1 Ion Chromatography (Anion\/Cation Exchange, Mixed Mode), 80\u003c\/p\u003e \u003cp\u003e3.1.2 High-Performance Liquid Chromatography (Reversed-Phase Mode, HILIC), 81\u003c\/p\u003e \u003cp\u003e3.1.3 Size Exclusion Chromatography (SEC) (Gel Filtration Chromatography, GFC), 82\u003c\/p\u003e \u003cp\u003e3.2 Detection Principles, 83\u003c\/p\u003e \u003cp\u003e3.2.1 Common Detection in IC: Conductivity, UV–Vis, Electrochemical Detection, 83\u003c\/p\u003e \u003cp\u003e3.2.2 Element Specific Detection, 83\u003c\/p\u003e \u003cp\u003e3.3 Hyphenated Techniques, 87\u003c\/p\u003e \u003cp\u003e3.3.1 HPLC(IC)–ICP-MS, 87\u003c\/p\u003e \u003cp\u003e3.4 HPLC(IC)–ICP-MS\/ESI-MS, 90\u003c\/p\u003e \u003cp\u003e3.4.1 Fundamentals, 90\u003c\/p\u003e \u003cp\u003e3.4.2 Methodology of Data Evaluation, 90\u003c\/p\u003e \u003cp\u003e3.4.3 Technical Requirements, 91\u003c\/p\u003e \u003cp\u003e3.5 Applications and Conclusion, 91\u003c\/p\u003e \u003cp\u003e3.6 References, 102\u003c\/p\u003e \u003cp\u003e\u003cb\u003e4 Application of IC-MS in Organic Environmental Geochemistry 109\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eKlaus Fischer\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e4.1 Introduction, 109\u003c\/p\u003e \u003cp\u003e4.2 Carboxylic Acids, 114\u003c\/p\u003e \u003cp\u003e4.2.1 Molecular Structure, Molecular Interaction Potential, and Chromatographic Retention, 114\u003c\/p\u003e \u003cp\u003e4.2.2 Environmental Analysis of Carboxylic Acids by Ion Exclusion Chromatography–Mass Spectrometry (HPICE-MS), 116\u003c\/p\u003e \u003cp\u003e4.2.3 Environmental Analysis of Carboxylic Acids by Ion-Exchange Chromatography–Mass Spectrometry (HPI-EC-MS), 124\u003c\/p\u003e \u003cp\u003e4.3 Carbohydrates, 135\u003c\/p\u003e \u003cp\u003e4.3.1 Structural Diversity and Ion Chromatographic Behavior, 135\u003c\/p\u003e \u003cp\u003e4.3.2 Environmental Analysis of Carbohydrates by Various IC-MS Methods, 136\u003c\/p\u003e \u003cp\u003e4.4 Amines and Amino Acids, 143\u003c\/p\u003e \u003cp\u003e4.5 Trends and Perspectives, 144\u003c\/p\u003e \u003cp\u003e4.6 References, 145\u003c\/p\u003e \u003cp\u003e\u003cb\u003e5 Analysis of Oxyhalides and Haloacetic Acids in Drinking Water Using IC-MS and IC-ICP-MS 152\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eKoji Kosaka\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e5.1 Introduction, 152\u003c\/p\u003e \u003cp\u003e5.2 Source of Oxyhalides and HAAs, 154\u003c\/p\u003e \u003cp\u003e5.3 Analysis of Oxyhalides and HAAs, 158\u003c\/p\u003e \u003cp\u003e5.3.1 Suppressed IC-MS, 158\u003c\/p\u003e \u003cp\u003e5.3.2 Nonsuppressed IC-MS and LC-MS, 162\u003c\/p\u003e \u003cp\u003e5.3.3 IC-ICP-MS, 165\u003c\/p\u003e \u003cp\u003e5.4 Application for Monitoring of Oxyhalides and HAAs in Drinking Water, 166\u003c\/p\u003e \u003cp\u003e5.4.1 Oxyhalides, 166\u003c\/p\u003e \u003cp\u003e5.4.2 HAAs, 171\u003c\/p\u003e \u003cp\u003eSummary, 171\u003c\/p\u003e \u003cp\u003e5.5 References, 172\u003c\/p\u003e \u003cp\u003e\u003cb\u003e6 Analysis of Various Anionic Metabolites in Plant and Animal Material by IC-MS 178\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eAdam Konrad Jagielski and Michal Usarek\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e6.1 Introduction, 178\u003c\/p\u003e \u003cp\u003e6.2 Optimization of HPIC and Ms Settings, 179\u003c\/p\u003e \u003cp\u003e6.2.1 HPIC Settings, 179\u003c\/p\u003e \u003cp\u003e6.2.2 MS Settings, 183\u003c\/p\u003e \u003cp\u003e6.2.3 HPIC-MS Settings, 185\u003c\/p\u003e \u003cp\u003e6.2.4 Extraction of Metabolites from Cells and Tissues, 189\u003c\/p\u003e \u003cp\u003e6.3 Application of the Method in Analysis of Metabolites in Plant and Animal Material, 191\u003c\/p\u003e \u003cp\u003e6.3.1 Analysis of Metabolites from Cell Cultures (Primary Cultures as well as Established Cell Lines), 192\u003c\/p\u003e \u003cp\u003e6.3.2 Analysis of Metabolites from Solid Tissues, 192\u003c\/p\u003e \u003cp\u003e6.3.3 Extraction of Metabolites from Plants, 194\u003c\/p\u003e \u003cp\u003e6.4 Conclusions, 196\u003c\/p\u003e \u003cp\u003e6.5 References, 197\u003c\/p\u003e \u003cp\u003e\u003cb\u003e7 Analysis of Perchlorate Ion in Various Matrices Using Ion Chromatography Hyphenated with Mass Spectrometry 199\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eJay Gandhi\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e7.1 Introduction, 199\u003c\/p\u003e \u003cp\u003e7.2 Precautions Unique to Ion Chromatography–Mass Spectrometry, 200\u003c\/p\u003e \u003cp\u003e7.2.1 Instrumental and Operating Parameters, 201\u003c\/p\u003e \u003cp\u003e7.3 Results and Discussion, 204\u003c\/p\u003e \u003cp\u003eAcknowledgment, 209\u003c\/p\u003e \u003cp\u003e7.4 References, 209\u003c\/p\u003e \u003cp\u003e\u003cb\u003e8 Sample Preparation Techniques for Ion Chromatography 210\u003cbr\u003e \u003c\/b\u003e\u003ci\u003eWolfgang Frenzel and Rajmund Michalski\u003c\/i\u003e\u003c\/p\u003e \u003cp\u003e8.1 Introduction, 210\u003c\/p\u003e \u003cp\u003e8.2 When and Why is Sample Preparation Required in Ion Chromatography? 213\u003c\/p\u003e \u003cp\u003e8.3 Automation of Sample Preparation (IN-LINE Techniques), 215\u003c\/p\u003e \u003cp\u003e8.4 Sample Preparation Methods, 217\u003c\/p\u003e \u003cp\u003e8.4.1 Filtration and Ultrafiltration, 219\u003c\/p\u003e \u003cp\u003e8.4.2 Solid-Phase Extraction (SPE), 220\u003c\/p\u003e \u003cp\u003e8.4.3 Liquid–Liquid Extraction, 225\u003c\/p\u003e \u003cp\u003e8.4.4 Gas-Phase Separations, 226\u003c\/p\u003e \u003cp\u003e8.4.5 Precipitation, 226\u003c\/p\u003e \u003cp\u003e8.4.6 Membrane-Based Separations and Sample Treatment, 227\u003c\/p\u003e \u003cp\u003e8.5 Trace Analysis and Preconcentration for Ion Chromatographic Analysis, 238\u003c\/p\u003e \u003cp\u003e8.5.1 Preconcentration Using SPE, 239\u003c\/p\u003e \u003cp\u003e8.5.2 Membrane-Based In-Line Preconcentration, 241\u003c\/p\u003e \u003cp\u003e8.6 In-Line Preseparations Using Two-Dimensional Ion Chromatography (2D-IC), 243\u003c\/p\u003e \u003cp\u003e8.7 Sample Preparation of Solid Samples, 244\u003c\/p\u003e \u003cp\u003e8.7.1 Dissolution and Aqueous or Acid Extraction, 246\u003c\/p\u003e \u003cp\u003e8.7.2 Wet-Chemical Acid Digestions, 247\u003c\/p\u003e \u003cp\u003e8.7.3 UV Photolytic Digestion, 248\u003c\/p\u003e \u003cp\u003e8.7.4 Fusion Methods, 249\u003c\/p\u003e \u003cp\u003e8.7.5 Dry Ashing and Combustion Methods, 249\u003c\/p\u003e \u003cp\u003e8.8 Air Analysis Using Ion Chromatography – Application to Gases and Particulate Matter, 251\u003c\/p\u003e \u003cp\u003e8.9 Postcolumn Eluent Treatment Prior to Ms Detection, 255\u003c\/p\u003e \u003cp\u003e8.10 Concluding Remarks, 257\u003c\/p\u003e \u003cp\u003e8.11 References, 258\u003c\/p\u003e \u003cp\u003eIndex 267\u003c\/p\u003e","brand":"John Wiley \u0026 Sons Inc","offers":[{"title":"Default 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