{"product_id":"aiche-equipment-testing-procedure-trayed-and-packed-columns-9781118627716","title":"AIChE Equipment Testing Procedure  Trayed and","description":"\u003cb\u003eBook Synopsis\u003c\/b\u003e\u003cbr\u003e\u003cp\u003e\u003cb\u003eAIChE manual updates and consolidates procedures for testing performance of distillation columns\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003eFrom classic distillation operations to air stripping to other separations processes, selecting the correct column for appropriate efficient, safe, and environmentally-sound operations can be an important step. The newest updated volume in AIChE's long-running Equipment Testing Procedures series, \u003ci\u003eTrayed and Packed Columns: A Guide to Performance Evaluation, Third Edition\u003c\/i\u003e provides chemical engineers, plant managers, and other professionals with helpful advice to assess and measure performance of a variety of distillation columns, including those that utilize bubble cap, sieve, valve trays, or packing material.\u003c\/p\u003e \u003cp\u003eThe new book combines and updates into one user-friendly volume the best available field knowledge from previous publications on both types of distillation columns. Designed not as a single set of compulsory steps, but as a compilation of techniques, it w\u003cbr\u003e\u003cbr\u003e\u003cb\u003eTable of Contents\u003c\/b\u003e\u003cbr\u003e\u003c\/p\u003e\u003cp\u003e\u003cb\u003e100.0 PURPOSE \u0026amp; SCOPE\u003c\/b\u003e \u003cb\u003e1\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e101.0 Purpose 1\u003c\/p\u003e \u003cp\u003e102.0 Scope 1\u003c\/p\u003e \u003cp\u003e\u003cb\u003e200.0 DEFINITION AND DESCRIPTION OF TERMS\u003c\/b\u003e \u003cb\u003e2\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e201.0 Flow Quantities 2\u003c\/p\u003e \u003cp\u003e202.0 Key Components 3\u003c\/p\u003e \u003cp\u003e203.0 Mass Transfer Efficiency 4\u003c\/p\u003e \u003cp\u003e203.1 Theoretical Trays or Plates or Stages 4\u003c\/p\u003e \u003cp\u003e203.2 Overall Column Efficiency 4\u003c\/p\u003e \u003cp\u003e203.3 Apparent Murphree Tray Efficiency 4\u003c\/p\u003e \u003cp\u003e203.4 Ideal Murphree Tray Efficiency 4\u003c\/p\u003e \u003cp\u003e203.5 Murphree Point Efficiency 4\u003c\/p\u003e \u003cp\u003e203.6 HETP 4\u003c\/p\u003e \u003cp\u003e203.7 HTU 4\u003c\/p\u003e \u003cp\u003e203.8 NTU 4\u003c\/p\u003e \u003cp\u003e204.0 Operating Lines 5\u003c\/p\u003e \u003cp\u003e205.0 Pinch 5\u003c\/p\u003e \u003cp\u003e206.0 Maximum Throughput 5\u003c\/p\u003e \u003cp\u003e206.1 Maximum Hydraulic Throughput 5\u003c\/p\u003e \u003cp\u003e206.2 Maximum Operational Capacity 5\u003c\/p\u003e \u003cp\u003e206.3 Maximum Efficient Capacity 5\u003c\/p\u003e \u003cp\u003e207.0 Minimum Operating Rate 5\u003c\/p\u003e \u003cp\u003e208.0 Operating Section 5\u003c\/p\u003e \u003cp\u003e209.0 Hardware 6\u003c\/p\u003e \u003cp\u003e209.1 Components of a Trayed Column 6\u003c\/p\u003e \u003cp\u003e209.2 Components of a Packed Column 7\u003c\/p\u003e \u003cp\u003e\u003cb\u003e300.0 TEST PLANNING 9\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e301.0 Preliminary Preparation 9\u003c\/p\u003e \u003cp\u003e301.1 Safety 10\u003c\/p\u003e \u003cp\u003e301.2 Environmental Considerations 10\u003c\/p\u003e \u003cp\u003e301.3 Test Objectives 10\u003c\/p\u003e \u003cp\u003e301.4 Organizational Resources 10\u003c\/p\u003e \u003cp\u003e301.5 Schedule 10\u003c\/p\u003e \u003cp\u003e301.6 Review of Historic Operating Data 10\u003c\/p\u003e \u003cp\u003e302.0 Column Control and Instrumentation 11\u003c\/p\u003e \u003cp\u003e303.0 Peripheral Equipment 11\u003c\/p\u003e \u003cp\u003e304.0 Pre-test Calculations 11\u003c\/p\u003e \u003cp\u003e304.1 Process Simulation 11\u003c\/p\u003e \u003cp\u003e304.2 Dry Run 11\u003c\/p\u003e \u003cp\u003e305.0 Types of Tests 12\u003c\/p\u003e \u003cp\u003e305.1 Performance Tests 12\u003c\/p\u003e \u003cp\u003e305.2 Acceptance Tests 12\u003c\/p\u003e \u003cp\u003e306.0 Specific Areas of Interest 12\u003c\/p\u003e \u003cp\u003e306.1 Packing Efficiencies 12\u003c\/p\u003e \u003cp\u003e306.2 Tray Efficiencies 12\u003c\/p\u003e \u003cp\u003e306.3 Overall Column Efficiency 13\u003c\/p\u003e \u003cp\u003e306.4 Capacity Limitations 13\u003c\/p\u003e \u003cp\u003e307.0 Energy Consumption 14\u003c\/p\u003e \u003cp\u003e308.0 Pressure Drop Restrictions 15\u003c\/p\u003e \u003cp\u003e309.0 Data Collection Requirements 15\u003c\/p\u003e \u003cp\u003e309.1 Process Operating Data 15\u003c\/p\u003e \u003cp\u003e309.2 Gamma Scan Data 15\u003c\/p\u003e \u003cp\u003e310.0 Conditions of External Streams 18\u003c\/p\u003e \u003cp\u003e310.1 Overall and Component Material Balances 18\u003c\/p\u003e \u003cp\u003e310.2 Overall Enthalpy Balances 18\u003c\/p\u003e \u003cp\u003e311.0 Internal Temperatures 18\u003c\/p\u003e \u003cp\u003e311.1 Heat Balances 18\u003c\/p\u003e \u003cp\u003e311.2 Internal Profiles 18\u003c\/p\u003e \u003cp\u003e312.0 Internal Samples 20\u003c\/p\u003e \u003cp\u003e312.1 Internal Samples for Efficiency Checks 20\u003c\/p\u003e \u003cp\u003e312.2 Internal Samples for Overall Performance 20\u003c\/p\u003e \u003cp\u003e313.0 Pressure Profiles 20\u003c\/p\u003e \u003cp\u003e314.0 Data Requirements-Physical Properties 20\u003c\/p\u003e \u003cp\u003e314.1 Test Mixtures 20\u003c\/p\u003e \u003cp\u003e314.2 Essential Data 21\u003c\/p\u003e \u003cp\u003e315.0 Auxiliary Data 21\u003c\/p\u003e \u003cp\u003e316.0 Test Procedure Documentation 21\u003c\/p\u003e \u003cp\u003e\u003cb\u003e400.0 METHODS OF MEASUREMENT AND SAMPLING 22\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e401.0 System Controls and Operating Stability 22\u003c\/p\u003e \u003cp\u003e402.0 Measurement of Temperatures 22\u003c\/p\u003e \u003cp\u003e402.1 Accuracy 22\u003c\/p\u003e \u003cp\u003e402.2 Errors 22\u003c\/p\u003e \u003cp\u003e403.0 Measurement of Flow Rates 24\u003c\/p\u003e \u003cp\u003e403.1 Orifice Meters 24\u003c\/p\u003e \u003cp\u003e403.2 Rotameters 25\u003c\/p\u003e \u003cp\u003e403.3 Vortex Flow Meters 25\u003c\/p\u003e \u003cp\u003e403.4 Coriolis Flow Meters 25\u003c\/p\u003e \u003cp\u003e403.5 Magnetic Flow Meters 25\u003c\/p\u003e \u003cp\u003e403.6 Pitot Tube (or Annubar) 25\u003c\/p\u003e \u003cp\u003e403.7 Direct Volume or Weight Measurement 26\u003c\/p\u003e \u003cp\u003e404.0 Measurement of Column Pressure Drop 26\u003c\/p\u003e \u003cp\u003e404.1 Instrument 26\u003c\/p\u003e \u003cp\u003e404.2 Pressure Taps 26\u003c\/p\u003e \u003cp\u003e404.3 Seal Pots 33\u003c\/p\u003e \u003cp\u003e404.4 Leakage Check 33\u003c\/p\u003e \u003cp\u003e404.5 Accuracy 33\u003c\/p\u003e \u003cp\u003e405.0 Sampling Procedure 34\u003c\/p\u003e \u003cp\u003e405.1 General 34\u003c\/p\u003e \u003cp\u003e405.2 Selection of Sampling Points 34\u003c\/p\u003e \u003cp\u003e405.3 Sample Connections 35\u003c\/p\u003e \u003cp\u003e405.4 Containers 35\u003c\/p\u003e \u003cp\u003e405.5 Sampling of High Boiling Materials 36\u003c\/p\u003e \u003cp\u003e405.6 Sampling of Intermediate Boiling Materials 37\u003c\/p\u003e \u003cp\u003e405.7 Sampling of Materials Having Boiling Points Below -50°F (-46°C) 40\u003c\/p\u003e \u003cp\u003e405.8 Leakage Check 41\u003c\/p\u003e \u003cp\u003e405.9 Labeling and Handling the Samples 41\u003c\/p\u003e \u003cp\u003e\u003cb\u003e500.0 TEST PROCEDURE 43\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e501.0 Preliminary 43\u003c\/p\u003e \u003cp\u003e502.0 Test Procedure for Maximum Hydraulic Throughput 43\u003c\/p\u003e \u003cp\u003e502.1 Flood Symptoms 44\u003c\/p\u003e \u003cp\u003e502.2 Performing Capacity Tests 45\u003c\/p\u003e \u003cp\u003e502.3 Optional Test Technique – Gamma Scanning 48\u003c\/p\u003e \u003cp\u003e503.0 Considerations Affecting Efficiency Test Procedure 48\u003c\/p\u003e \u003cp\u003e503.1 Rigorous Versus Shortcut Efficiency Tests 48\u003c\/p\u003e \u003cp\u003e503.2 Strategy of Efficiency Testing 49\u003c\/p\u003e \u003cp\u003e503.3 Early Preparation for Efficiency Tests 50\u003c\/p\u003e \u003cp\u003e503.4 Last-minute Preparations for Efficiency Tests 53\u003c\/p\u003e \u003cp\u003e503.5 Establishment of Steady State Conditions 55\u003c\/p\u003e \u003cp\u003e503.6 The Test Day 56\u003c\/p\u003e \u003cp\u003e503.7 Concluding Test 56\u003c\/p\u003e \u003cp\u003e\u003cb\u003e600.0 COMPUTATION OF RESULTS\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e601.0 Verification of Test Data and Simulation Models 58\u003c\/p\u003e \u003cp\u003e602.0 Material Balance 59\u003c\/p\u003e \u003cp\u003e602.1 End Effects 59\u003c\/p\u003e \u003cp\u003e603.0 Enthalpy Balance 59\u003c\/p\u003e \u003cp\u003e603.1 Overall Balance 59\u003c\/p\u003e \u003cp\u003e603.2 Internal Flow Rates 60\u003c\/p\u003e \u003cp\u003e604.0 Hydraulic Performance 60\u003c\/p\u003e \u003cp\u003e604.1 Trayed Column 60\u003c\/p\u003e \u003cp\u003e604.2 Packed Column 61\u003c\/p\u003e \u003cp\u003e605.0 Efficiency Performance 61\u003c\/p\u003e \u003cp\u003e605.1 Trayed Column 62\u003c\/p\u003e \u003cp\u003e605.2 Packed Column 69\u003c\/p\u003e \u003cp\u003e\u003cb\u003e700.0 INTERPRETATION OF RESULTS 76\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e701.0 Sources of Experimental Error 76\u003c\/p\u003e \u003cp\u003e701.1 Material and Enthalpy Balances 77\u003c\/p\u003e \u003cp\u003e702.0 Effects of Experimental Error 78\u003c\/p\u003e \u003cp\u003e703.0 Design versus Performance 78\u003c\/p\u003e \u003cp\u003e703.1 Mechanical\/Tower Equipment 78\u003c\/p\u003e \u003cp\u003e703.2 Process Conditions 78\u003c\/p\u003e \u003cp\u003e704.0 Hydraulic Performance 79\u003c\/p\u003e \u003cp\u003e704.1 Mechanical\/Tower Equipment 79\u003c\/p\u003e \u003cp\u003e704.2 Tray 79\u003c\/p\u003e \u003cp\u003e704.3 Packing 80\u003c\/p\u003e \u003cp\u003e704.4 Process Conditions 80\u003c\/p\u003e \u003cp\u003e705.0 Mass Transfer Performance 81\u003c\/p\u003e \u003cp\u003e705.1 Mechanical\/Tower Equipment 81\u003c\/p\u003e \u003cp\u003e705.2 Tray 81\u003c\/p\u003e \u003cp\u003e705.3 Packing 82\u003c\/p\u003e \u003cp\u003e705.4 Maldistribution 82\u003c\/p\u003e \u003cp\u003e705.5 Process 84\u003c\/p\u003e \u003cp\u003e706.0 Test Troubleshooting 85\u003c\/p\u003e \u003cp\u003e706.1 Analysis Procedure 85\u003c\/p\u003e \u003cp\u003e706.2 Sampling 85\u003c\/p\u003e \u003cp\u003e706.3 Equilibrium Data 85\u003c\/p\u003e \u003cp\u003e706.4 Temperature Measurements 85\u003c\/p\u003e \u003cp\u003e706.5 Heat and Material Balances 86\u003c\/p\u003e \u003cp\u003e706.6 Fluctuation of Process Conditions 86\u003c\/p\u003e \u003cp\u003e706.7 Pressure Drop Measurements 86\u003c\/p\u003e \u003cp\u003e706.8 Incorrect Prediction of Pressure Drop 86\u003c\/p\u003e \u003cp\u003e706.9 Errors in Assumptions in Modeling Mass Transfer 86\u003c\/p\u003e \u003cp\u003e706.10 Multicomponent Systems Deviate from Binary Data 87\u003c\/p\u003e \u003cp\u003e706.11 High Purity Separation 87\u003c\/p\u003e \u003cp\u003e706.12 Test and Design Conditions 87\u003c\/p\u003e \u003cp\u003e\u003cb\u003e800.0 APPENDIX 88\u003c\/b\u003e\u003c\/p\u003e \u003cp\u003e801.0 Notation 88\u003c\/p\u003e \u003cp\u003e801.1 Greek Symbols 90\u003c\/p\u003e \u003cp\u003e802.0 Sample Calculations 90\u003c\/p\u003e \u003cp\u003e802.1 General Analysis of Test Data 90\u003c\/p\u003e \u003cp\u003e802.2 Packed Column 91\u003c\/p\u003e \u003cp\u003e802.3 Trayed Column 107\u003c\/p\u003e \u003cp\u003e803.0 References 126\u003c\/p\u003e","brand":"John Wiley \u0026 Sons Inc","offers":[{"title":"Default Title","offer_id":49406896767319,"sku":"9781118627716","price":44.6,"currency_code":"GBP","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0817\/1739\/5799\/files\/9781118627716.jpg?v=1730497480","url":"https:\/\/bookcurl.com\/products\/aiche-equipment-testing-procedure-trayed-and-packed-columns-9781118627716","provider":"Book Curl","version":"1.0","type":"link"}